• Transactions of the Korean Society of Mechanical Engineers A
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• v.33 no.11
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• pp.1274-1278
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• 2009

Fracture characteristics for plate and dome shapes of glass filled ceramics using shock tube were carried out. Glass filled ceramics have been considered as a promising candidate material for the dome port cover of air breathing engine. This part of the air breathing engine has an important role as separated membrane between combustion and external air, and needs the frangible characteristics that the particles of fractured glass filled ceramics should not affect the internal components of combustion. The objectives of this study are to evaluate the fracture pressures for various thicknesses and diameters of shock impact area. Also fracture phenomena of separated membrane using a shock tube compare with analytical method. The experimental apparatus consists of a driver, a driven section and a dump tank. The used material is glass filled ceramic made from Corning company. Specimens have the thickness of 3, 4.5 and 6mm. It is expected that the results obtained from this study can be used in the basic data for the dome port cover design of an air breathing engine.

• Journal of the Korean Ceramic Society
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• v.29 no.12
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• pp.956-962
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• 1992

The predominant sintering mechanisms of low firing temperature ceramic substrate which consists of borosilicate glass containing alumina as a filler are the rearrangement of alumina particles and the viscous flow of glass powders. In this system, sintering condition depends on the volume ratio of alumina to glass and on the particle size. When the substrate contains about 35 vol% alumina filler and the average alumina particle size is 4 $\mu\textrm{m}$, the best firing condition is obtained at the temperature range of 900∼1000$^{\circ}C$. The extensive rearrangement behavior occurs at these conditions, and the optimum sintering condition is attained by smaller size of glass particles, too. The formation of cristobalite during sintering causes the difference of thermal expansion coefficient between the substrate and Si chip. This phenomenon degradates the capacity of Si chip. Therefore, the crystallization should be prevented. In the alumina filled borosilicate glass system, the crystallization does not occur. This effect may have some relation with aluminum ions in alumina. For aluminum ions diffuse into glass matrix during sintering, functiong as network former.

• Journal of the Microelectronics and Packaging Society
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• v.6 no.1
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• pp.11-21
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• 1999

For microelectronic packaging application, the crystallizable glass powder in CaO-$A1_2O_3-SiO_2-B_2O_3$system was mixed with various amounts of alumina inclusions (\approx 4 $\mu \textrm{m}$), and its sintering behavior, crystallization behavior, and dielectric constant were examined in terms of vol% of alumina and the reaction between the alumina and the glass. Sintering of the CASB glass powder alone at $900^{\circ}C$ resulted in full densification (99.5%). Sintering of alumina-filled composite at $900^{\circ}C$ also resulted in a substantial denslfication higher than 97% of theoretical density, In this case, the maximum volume percent of alumina should be less than 40%. XRD analysis revealed that there was a partial dissolution of alumina into the glass. This alumina dissolution, however, did not show the particle growth and shape accommodation. Therefore, the sintering of both the pure glans and the alumina-filled composite was mainly achieved by the viscous flow and the redistribution of the glass. Alumina dissolution accelerated the crystallization initiation time at $1000^{\circ}C$ and hindered the densification of the glass. Dielectric constants of both the alumina-filled glass and the glass-ceramic composites were increased with increasing alumina content and followed rule of mixture. In case of the glass-ceramic matrix composites showed relatively lower dielectric constant than the glass matrix composite. Furthermore, as alumina content increased, crystallization behavior of the glass was changed due to the reaction between the glass and the alumina. As alumina reacted with the glass matrix, the major crystallized phase was shifted from wollastonite to gehlenite. In this system, alumina dissolution strongly depended on the particle size: When the particle size of alumina was increased to 15 $\mu\textrm{m}$, no sign of dissolution was observed and the major crystallized phase was wollastonite.

• Proceedings of the Korean Society of Propulsion Engineers Conference
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• 2009.05a
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• pp.103-106
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• 2009

Fracture characteristics of plate shape using shock tube for glass filled ceramics was carried out. Glass filled ceramics have been considered as a promising candidate material for the dome port cover of air breathing engine. This part of the air breathing engine has an important role separating solid and liquid fuel, and needs the frangible characteristics that the fracture of a part should not affect the internal components of combustion. The objectives of this study are to evaluate the fracture pressures for various thicknesses and diameters of shock impact area. Also fracture phenomena of separated membrane using a shock tube are observed. The experimental apparatus of shock tube consists of a driver, a driven section and a dump tank. The used material is glass filled ceramic made from Corning company. Specimens are used 3, 4.5 and 6mm thickness. Also diameters of shock wave area are chosen 70, 60 and 50 mm. It is expected that the results obtained from this study can be used in the basic data for the dome port cover design of an air breathing engine.

• Proceedings of the Korean Society of Propulsion Engineers Conference
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• 2004.10a
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• pp.223-226
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• 2004

The objectives of this study are to evaluate mechanical properties of glass ceramic for dome port cover material o( the ramjet. Candidate material for dome port cover of the ramjet is selected the machinable glass ceramic(MACOR glass-filled ceramic, Corning Glass Works, code 9658). Static and dynamic fracture toughness tests were performed to evaluate the apparent fracture toughness of notched specimen.

• Journal of the Korean Ceramic Society
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• v.40 no.8
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• pp.735-738
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• 2003

The PTFE composites for the microwave printed circuit board were prepared using woven glass fiber. The dielectric constant of the PTFE composites with oven glass fiber tended to decrease with an increase of immersion time, and was saturated at 3 times immersion. It resulted from the fact that fine powders of PTFE filled up at the pore and bend of woven glass fiber sufficiently. As the immersion time increased, the propagation velocity increased due to the reduction of dielectric constant.

• Proceedings of the Korean Society of Propulsion Engineers Conference
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• v.y2005m4
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• pp.112-115
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• 2005

The objectives of this study are to evaluate the dynamic fracture toughness of advance glass ceramics(MACOR glass-filled ceramic, Corning Glass Works) for dome port cover of the ramjet. Static and dynamic fracture toughness tests are performed using strain gage method in the variation of notch radii.

• Proceedings of the Korean Institute of Electrical and Electronic Material Engineers Conference
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• 2003.07b
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• pp.611-615
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• 2003

The crystalline and dielectric properties on $Al_2O_3$ filled glass frit ($CaO-Al_2O_3-SiO_2-MgO-B_2O_3$) with admixtures of $TiO_2$ have been investigated. The dielectric constant value of $7.5{\sim}7.8$, quality factor value of 700 were obtained for glass frit : $Al_2O_3$ (50 : 50 wt%) ceramics. As the amount of $TiO_2$ increased, temperature coefficient of dielectric constant were decreased.

• Journal of the Korean Ceramic Society
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• v.35 no.9
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• pp.939-944
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• 1998

The formation microstructure and properties of novel ceramic composite materials by active filler con-trolled polymer pyrolysis were investigated. Polymethlsiloxane filled with W is of particular interested be-cause of the formation of ceramic bonded hard materials (WC-$W_{2}C$-$S_{1}OC$) for wear resistant applications. Highly metal-filled polymer suspensions were prepared and their conversion to ceramic composites by an-nealing in $N_{2}C$ atmosphere at 1000-$1600^{\circ}C$ were studied. Dimensional change porosity and phase distribution (filler network) were analyzed and correlated to the resulting material properties. Microcrystalline com-posites with the filler reaction products embedded to the resulting material properties. Microcrystalline com-posites with the filler reaction products embedded in a silicon oxycarbide glass matrix were produced. De-pending on the pyrolysis conditions ceramic composites with a density up to 95 TD% a hardness of 7-8.8GPa Yong's modulus of 220-230 GPa a fracture toughness of 6-6.8$MPam^{1/2}$ and a flexual strength of 380-470 MPa were obtained.

• Journal of the Korean Ceramic Society
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• v.35 no.7
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• pp.706-714
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• 1998

The MgO-{{{{ { {Al }_{2 }O }_{3 } }}-{{{{ { {SiO }_{2 } }_{ } }}system containing alumina powder was fabricated sintered at various temperature and analyzed in order to study the sintering mechanism and crystallization characteristics. The specimen composed of glass powder with average particle size of 8.27 $\mu\textrm{m}$ and 0-40 vol% alumina powder were sint-ered for 3 hrs at the temperature between 850$^{\circ}C$ and 1350$^{\circ}C$ The sintering mechanism consists of the redis-tribution of particles occuring at 750$^{\circ}C$ and the viscous flow at 850∼950$^{\circ}C$. The degree of crystallization and sintering temperatue were dependent upon the ratio of glass/alumina. The second phase from the reaction between glass and alumina was not observed which was confirmed by XRD and properties analysis. The density dielectric constant and specific resistivity of specimen were 2.30∼3.26g/cm2 5.8∼7.38 at 1 GHz density dielectric constant and specific resistivity of specimen were 2.30∼3.26g/cm3 5.8∼7.38 at 1GHz and 1.23∼4.70${\times}$107 $\Omega$$.$m respectively.