• Title/Summary/Keyword: Gel-time

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Concentration of Fresh Gel from Aloe vera L. by Using Ultrafiltration Process (한외여과 공정에 의한 알로에 베라 겔 농축)

  • Baek, Jin-Hong;Kim, Sung-A;Lee, Shin-Young
    • KSBB Journal
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    • v.23 no.2
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    • pp.169-176
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    • 2008
  • The concentration of fresh gel from Aloe vera L. by using ulfrafiltration (UF) process was investigated and analyzed. The two membranes (organic and ceramic) with different molecular weight cut-off (MWCO) and modules (flat sheet and tubular) was used. Under optimum operation conditions, ceramic (zirconium dioxide) tubular membrane with MWCO of 50 kDa resulted in higher flux, less fouling, more turbid, higher total solid, higher polysaccharide and less aloin content. Optimum operation conditions were transmembrane pressure of 1.0 bar, feed velocity of 240 L/hr and temperature of $23^{\circ}C$. Volume concentration factor of aloe gel was 3.13 at permeate flux of $51.1\;L/m^2{\cdot}hr$ after processing time of 1.66 hr. Aloin in fresh aloe gel by UF process was effectively removed as permeate and bioactive polysaccharide content was 2.1 times higher than that of fresh aloe gel. These results allowed a very good level of concentration degree and polysaccharide content. Thus, ultrafiltration process of this study was suitable for the concentration of fresh aloe gel though the aloe concentrate showed both the viscosity decrease and partially separation of liquid layer during storage at $4^{\circ}C$.

Effective Positive Bias Recovery for Negative Bias Stressed sol-gel IGZO Thin-film Transistors (음 바이어스 스트레스를 받은 졸-겔 IGZO 박막 트랜지스터를 위한 효과적 양 바이어스 회복)

  • Kim, Do-Kyung;Bae, Jin-Hyuk
    • Journal of Sensor Science and Technology
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    • v.28 no.5
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    • pp.329-333
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    • 2019
  • Solution-processed oxide thin-film transistors (TFTs) have garnered great attention, owing to their many advantages, such as low-cost, large area available for fabrication, mechanical flexibility, and optical transparency. Negative bias stress (NBS)-induced instability of sol-gel IGZO TFTs is one of the biggest concerns arising in practical applications. Thus, understanding the bias stress effect on the electrical properties of sol-gel IGZO TFTs and proposing an effective recovery method for negative bias stressed TFTs is required. In this study, we investigated the variation of transfer characteristics and the corresponding electrical parameters of sol-gel IGZO TFTs caused by NBS and positive bias recovery (PBR). Furthermore, we proposed an effective PBR method for the recovery of negative bias stressed sol-gel IGZO TFTs. The threshold voltage and field-effect mobility were affected by NBS and PBR, while current on/off ratio and sub-threshold swing were not significantly affected. The transfer characteristic of negative bias stressed IGZO TFTs increased in the positive direction after applying PBR with a negative drain voltage, compared to PBR with a positive drain voltage or a drain voltage of 0 V. These results are expected to contribute to the reduction of recovery time of negative bias stressed sol-gel IGZO TFTs.

The Use of Polymer Gel for the Visualization of 3-D Dose Distribution in Brachytherapy Using Magnetic Resonance Imaging (방사선 근접치료에 있어서 핵자기공명영상을 이용한 3차원 방사선 선량분포도의 가시화를 위한 polymer 젤의 이용)

  • 강해진;조삼주;정은기;강승희;오영택;전미선;권수일
    • Progress in Medical Physics
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    • v.9 no.4
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    • pp.207-215
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    • 1998
  • There have been many radiation measurement methods so far among which film dosimetry, TLD, and ion chamber are the most frequently used methods. But this study describes a new radiation measurement method which uses polymer gel and magnetic resonance imaging(MRI). The objective of this study is to fabricate a polymer gel sensitive to radiation and to generate a dose to MRI contrast relationship, and to apply this results to the radiation measurement for the brachytherapy. To do this, 12 cm diameter cylindrical gel phantom was made, and the phantom was irradiated using the 30 mm diameter circular collimator which was used for radiosurgery. And this irradiated phantom was scanned with MRI. To find out the relationship between the radiation dose and the transversal relaxation time, an image processing software(IDL) was used. From this study it is found out that the radiation dose showed linear relationship to the transversal relaxation time of the gel up to 17 Gy($R^2$=0.993) and they had a different relationship above 17 Gy. The dose distributions were calculated using these results for the Ir-192 sources, one for the HDR afterloading system and the other for a 2 mCi seed source. And these calculated dose distributions were compared to the ones from the treatment planning computers. From this study the dose to the irradiated gel's transversal relaxation time relationship was examined, and this result was tried for the measurement of the brachytherapy.

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The Effect of Temperature and Exposure Time on UV-curing of Urethane Acrylate (UV 챔버 내부 온도 및 체류시간이 Urethane Acrylate의 경화속도에 미치는 영향)

  • Moon, Seung-Ho;Kim, Kwang-Hee;Kim, Jeong-Sik
    • Journal of the Korea Academia-Industrial cooperation Society
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    • v.13 no.9
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    • pp.3822-3826
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    • 2012
  • We have studied the effect of temperature and exposure time on the UV curing rate of Urethane Acrylate. UV dose has been modulated by changing the electric power, and temperature has been controled by coating rate and water temperature of the coating roll. Curing rate was evaluated by measuring gel fraction of the cured film. It has been found that effect of coating velocity on the gel fraction of the final film is predominant, but role of temperature of the UV chamber is negligible. These observations imply that exposure time of UV light is critical to have a fully cured film. To better understand the effect of design and operating condition of UV coater on the behavior of UV curing of Urethane Acrylate, we have also conducted heat-flux analysis of UV chamber.

The Anticoagulant Fraction from the Leaves of Diospyros Kaki L. Has an Antithrombotic Activity

  • Sa You Seon;Kim Soo-Jin;Choi Hye-Seon
    • Archives of Pharmacal Research
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    • v.28 no.6
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    • pp.667-674
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    • 2005
  • The leaves of Persimmon (Diospyros kaki L.) has long been used for tea in Korea since it was thought to be effective against hypertension. An anticoagulant fraction was purified through gel filtration G-100, hydrophobic, gel filtration G-150, and FPLC, Phenyl superpose column chromatographies. The purified fraction was homogenous and its Mr was estimated 10,000 Da by gel filtration and SDS-PAGE. The purified fraction was sensitive to treatment of subtilisin B, but not to heat and its activity was not changed after periodate oxidation, indicating that the activity was not due to carbohydrates. It delayed thrombin time (TT), activated partial thromboplastin time (APTT), and prothrombin time (PT) using human plasma. TT was more sensitive than APTT and PT, suggesting that the anticoagulant activity may be caused by a degradation or a defect of fibrin or thrombin. It did not cause the hydrolysis of fibrin after incubation. However, it inhibited thrombin-catalyzed fibrin formation with a competitive inhibition pattern. These results indicate that it may be an antithrombotic agent and that it is bound to fibrinogen binding sites of thrombin.

Explosion Characteristics by Different Sizes in the Wall Surface Shape of a Water Gel Barrier (Water Gel Barrier 표면형상의 크기에 따른 폭발특성)

  • Park, Dal-Jae;Kim, Nam-Il
    • Journal of the Korean Institute of Gas
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    • v.16 no.3
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    • pp.65-70
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    • 2012
  • Experimental investigations were carried out to examine the explosion characteristics by different sizes in the wall surface shape of a water gel barrier in an explosion chamber, 1,600 mm in length with a square cross-section of $100{\times}100\;mm^2$. The sizes in the wall surface shape were varied by using water gel barriers with a cross-section of $100{\times}200\;mm^2$ and its were varied in the bottom of the chamber away 300, 700 and 1,100 mm, respectively from the closed end of the chamber. The flame propagation images were photographed with a high speed camera and the pressure was recorded using a pressure transducer and a data acquisition system. It was found that as the size of the wall surface shape increased, the flame propagation process and the time taken to reach the maximum pressure were found to be faster. As a result, both the flame speed and the explosion overpressure increased as the size of the wall surface shape increased.

Preparation and Opticaa Properties of CuCl Nanocrystallites Dispersed Nonlinear Optical Glass by Sol-Gel Process (솔-젤법에 의한 CuCl 미세결정이 분산된 비선형 광학유리의 제조 및 광특성)

  • 송석표;한원택;김병호
    • Journal of the Korean Ceramic Society
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    • v.34 no.9
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    • pp.941-948
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    • 1997
  • CuCl nanocrystallites dispersed nonlinear optical silica and borosilicate glasses were fabricated by sol-gel process. CuCl powder was dissolved in TEOS(Si(OC2H5)4) and TMB((CH3O)3B), precursors of silica and borosilicate glasses, with ethanol, water and HCl, and precipitated through the heat treatment in the matrix glass. The optical properties of CuCl doped glasses were measured using the spectrophotometer at room temperature and low temperature(77K); Z1, 2 and Z3 exciton peaks from the absorption spectra, were observed at about 370 nm and 380 nm, respectively. The average radius of nanocrystallites, calculated from the blue shift of Z3 excitons, was measured according to annealing temperature and time. The precipitation temperature of CuCl nanocrystallites was decreased when boron was added to silica glass. Increase of annealing temperature and time made average radius of nanocrystallites saturated about 2 nm.

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Effects of Organic Substances in the Preparation of Porous Silica Glass by the Sol-Gel Process (졸겔법에 의한 다공성 실리카 유리의 합성에 있어서 유기물의 영향)

  • 최성일;신대용;한상목;이승범
    • Journal of the Korean Ceramic Society
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    • v.30 no.10
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    • pp.838-844
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    • 1993
  • To control the pore size of silcia gel, formamide (FA), N,N-dimethyl formamide (DMF), polyethylene glycol (PEG) and polyacrylic acid (PAA) were added in the sol-gel process from starting solution with tetramethyl orthosilicate (TMOS). The gels were characterized using porosimeter, TG-DTA and SEM. As a result, the more contents of FA and PAA was increased the more gelation time was decreased, also the more contents of DMF and PEG was increased the more gelling time was increased. The mean pore size of gels was larger in the order of PAA, DMF, FA and PEG. And the mean pore size of porous silica glass was 59.0$\AA$, 31.5$\AA$, 29.9$\AA$ and 29.0$\AA$, respectively, heated at 75$0^{\circ}C$/100$0^{\circ}C$.

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Shape-Stabilized Phase Change Materals : Frozen Gel from Polypropylene and n-Octadecane For Latent Heat Storage

  • Son, Tae-Won;Kim, Tae-Hun;Kim, Bong-Shik;Kim, Byung-Giu
    • Proceedings of the Polymer Society of Korea Conference
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    • 2006.10a
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    • pp.375-375
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    • 2006
  • The preparation methods are to be used as "melting method" and "absorption method", respectively. The reaction mixture in the reaction container was heating up the reaction mixture to $200^{\circ}C$ for 2 hour. The mixing time of lab scale preparation should be provided quit long, instead of the short working time in a compounder vessel. And The PP-PCM mixture in the reaction container was heating up the mixture around $60-80^{\circ}C$ for 2 hour. A melting method of frozen gel with 50/50 weight ratio of polypropylene-normal octadecane was prepared by adding PP chip and normal octadecane. An absorption method of frozen gel with 70/30 weight ratio of PP 4.8-normal n-octadecane was prepared by adding PP powder and normal octadecnae.

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Synthesis of barium hexaaluminate by sol - gel method (졸 - 겔법에 의한 바륨헥사알루미네이트 합성)

  • 백영순;김형진
    • Journal of the Korean Crystal Growth and Crystal Technology
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    • v.5 no.2
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    • pp.142-151
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    • 1995
  • Complex alkoxides were synthesized using metal alkoxide method and were then hydrolyzed to prepare the precursors using sol - gel method. Then, the precursors were calcined in order to make barium hexaaluminate. Factors affecting the material properties of the barium hexaaluminate precursors were studied and they are the kinds and amount of alcohols, and reaction time. In addition, in the course of hydrolysis, the effects of the amount of water, reaction temperature and aging time were also studied in terms of the specific surface area and average particle size of the barium hexaaluminates.

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