• Title/Summary/Keyword: Gel bead

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Fluidized Bed Drying Effect on the Aerogel Powder Synthesis

  • Hong, Seong-Hoon;Lee, Dong-Kyu;Oh, Chang-Sup;Kim, Yong-Ha
    • Journal of Energy Engineering
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    • v.21 no.1
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    • pp.43-46
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    • 2012
  • A fluidized bed drying approach was utilized to the synthesis of water glass based silica aerogel powders. The effects of the fluidized bed drying conditions such as the superficial velocity and temperature of hot air and bead size as well as bead/wet-gel ratio, on the physical properties such as tapping density and productivity of the aerogel powders were systematically investigated. The experimental results showed that the amount of beads mixed with wet-gels in the fluidized bed column has the most profound impact on the fluidization efficiency, greatly enhancing the yield of the aerogel powders up to 98% with a proper bead/wet-gel weight ratio as compared to 72% without using beads. No significant change was observed in the tapping density over a wide range of the fluidized drying condition. Consequently the fluidized bed drying approach shows a good promise as an alternative route for the large-scale production of the aerogel powders.

Immobilization of Microorganisms - Part 1. Preparation of Immobilized Lactobacillus bulgaricus - (미생물(微生物) 고정화(圖定化)에 관한 연구(硏究) - 제1보(第1報). Lactobacillus 균(菌)의 고정화조건(圖定化條件) -)

  • Lee, Kang-Heup
    • Applied Biological Chemistry
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    • v.24 no.2
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    • pp.149-152
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    • 1981
  • The immobilization of Lactobacillus bulgaricus was investigated by various method, e.g. by use of polyacrylamide gel and Al-, Ca-, Fe- or Mg-alginate beads, and the most active immobilized cells were obtained by entrapment in a Ca-alginate beads. These immobilized microbial cells, when introduced into 4.5% lactose solution and whey solution showed maximum relative activity of 28% or lactose solution and 18% for whey solution as measured against the native microbial reference standard (100).

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Characterization of Titania plate and Nano Titania Coated Beads for Photoelectrocatalytic system(PECS) (광전자촉매 시스템(PECS)에 사용할 광촉매 금속판과 비드의 특성고찰)

  • Do, Young-Woong;Ha, Jin-Wook
    • Proceedings of the KAIS Fall Conference
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    • 2008.11a
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    • pp.354-357
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    • 2008
  • 본 연구는 광전자촉매 시스템(PECS) 적용을 위하여 광촉매 금속판과 코팅비드를 제조하여 특성을 고찰하였다. 광촉매 물질의 회수가 용이하고, 실용화하기 위하여 티타늄 금속판을 $400^{\circ}C$에서 $700^{\circ}C$까지 $50^{\circ}C$에서 $100^{\circ}C$간격으로 토치를 사용하여 산화처리 하였으며, 비드의 경우 alumina, glass, silica gel beads에 TTIP([Ti$(OC_3H_7)_4$], Aldrich)을 전구체로 사용하여, 유동층 화학기상증착공정(Fluidized Bed Chemical Vapor Deposition, FB-CVD)으로 박막코팅을 하였다. 광촉매 금속판의 경우 산화처리 후 외관상태와 성분분석 시 최적조건은 $400^{\circ}C{\sim}500^{\circ}C$ 60분간 토치로 산화하였을 때였으며, 광촉매 코팅비드의 경우 silica gel beads가 본연의 다공구조를 나타내며 박막코팅이 되어, 상대적으로 alumina, glass beads에 비해 반응표면적이 크게 나타났다.

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Modeling the effect of mass transfer on the kinetics of fructo-oligosaccharide production by immobilized cells (고정화 세포에 의한 Fructo-oligosaccharides 생산 반응메카니즘에서 물질전달 영향에 대한 수학적 모델)

  • 윤종원;전영중이민규송승구
    • KSBB Journal
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    • v.8 no.3
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    • pp.266-271
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    • 1993
  • The effective diffusion coefficients of glucose, sucrose and fructo-oligosaccharides in Ca-alginate gel beads at high concentration of sucrose solutions were investigated at $50^{\circ}C$. A mathematical model for the kinetics of fructo-oligosaccharide production using immobilized cells was proposed and compared with experimental results varying the bead size, the substrate concentration and the bead ratio. Very low values of diffusion coefficients ranging $1.2-7.6\times10^{-7}\textrm{cm}^2$/sec were obtained, and the predicted results were in good agreement with experimental ones in all cases tested.

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Immobilized Condition of Suchwowces cerevisiae for Ethanol Production from Persimmon Juice. (감 즙으로부터 에탄을 생산을 위한 Saccharomyces cerevisiae의 고정화 조건)

  • 이상원;손미예;서권일
    • Food Science and Preservation
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    • v.6 no.2
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    • pp.221-227
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    • 1999
  • The immobilized culture system of Saccharomyces cerevisiae was examined to improve the efficiency of vinegar production from persimmon juice. Optimum concentration of Na-alginate for the immobilization was 2%. When the 1eakage of yeast from get beads was checked by turbidity of culture medium with varying concentration of Na-alginate from 1 to 4%, turbidity of culture medium increased from 8 hrs of cultivation with 1% Na-alginate concentration showing optical density of 0.82 at 20 hrs. However, the increase in turbidity of culture medium was slow with 2-4% Na-alginate showing optical density of 0.55-0.58 at 20 hrs. Microscopical analysis of gel matrix showed that the immobilized yeast was grown well regardless of Na-alginate concentration. Optimum size of gel bead and amount of inoculation were 2-3 m and 33mg, respectively. For ethanol production aerobic cultivation for 121hrs using cohen plug followed by anaerobic cultivation using silicon plug equipped with a check valve was the most effective.

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Adsorption of Heavy Metal Ions(Cadmium etc.) using Chitosan Bead (Chitosan Bead를 이용한 Cd등의 중금속 이온의 흡착제거)

  • 권성환;김기환;장문석;유재근
    • Journal of environmental and Sanitary engineering
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    • v.11 no.3
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    • pp.21-27
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    • 1996
  • Chitosan is a natural polyelectrolytic compound. Researches of adsorption capacity using chitosan have been doing actively. We prepared bead type gel, simple modifier of chitosan, And then experimented adsorption test of heavy metals (Cd etc) using it. According to the result adsorption capacity of chitosan bead was five times higher than chitosan powder. Removal rate of cadmium resulted 90% over in the test that initial concentration of Cd was 100mg/L and bead dosage was 6g/100mL. Adsorption type of heavy metals was similar to general adsorption curve. And optical pH range was 4 - 10 in the adsorption test. In the experiments of other heavy metals (Pb, Zn, Cu, Mn) adsorption types had two stages, highly removal rate-stage at the short time (20minutes) and then slow rate-stage at the after. And removal efficiency at the variable pH ranges revealed relatively good.

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A Study on the Photocatalytic Degradation of VOC over TiO2 Coated on Glass Bead (산화티탄 광촉매를 이용한 VOC 가스 처리효과에 관한 연구)

  • Yun, Seok-Yeong;No, Jun-Hyeong;Park, Sun-Je;Lee, Seung-Ho
    • Korean Journal of Materials Research
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    • v.10 no.5
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    • pp.328-334
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    • 2000
  • The photocatalyst of $TiO_2$coated on glass bead was prepared from sol-gel method to remove the VOC (vola-tile organic compounds) by the photocatalytic reaction. The coated films were characterized by X-ray diffraction(XRD), specific surface area(BET), and scanning electron microscopy observation (SEM), The gas-phase photocatalytic degradation of trichloroethylene(TCE) and benzene with coated titanium dioxide on glass beads was in-vestigated using a fixed bed reactor. The degradation was calculated by the concentration difference with the retained on the reactor with aid of gas chromatography. At steady state, conversion yields were obtained for 80% of trichloroeth-vlene in 400 ppmv concentration and 65% on benzene in the range of concentration from 50 to 300 ppmv, respectively.

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Removal of Cadmium Ion (Cd2+) by Pseudomonas aeruginosa Immobilized in Ca-Alginate Gel Beads in Packed-Bed Column Reactor (충전층 반응기내에서 고정된 Pseudomonas aeruginosa에 의한 Cd2+의 제거)

  • Choi, Kwang Soo;Kim, Chul Kyung
    • Clean Technology
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    • v.8 no.4
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    • pp.217-222
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    • 2002
  • The effects of initial cadmium ion concentrations (50, 100, 200, 300ppm), and feeding velocities (30, 45, 60mL/hr) on the removal ratio of cadmium ion by Pseudomonas aeruginosa ATCC 27853 immobilized in Ca-alginate gel beads in a packed-bed column reactor were investigated at operating temperature $37^{\circ}C$. The removal ratio of cadmium ion with variable initial concentration was decreased in the following order : 50ppm > 100ppm > 200ppm > 300ppm. The optimum removal conditions of cadmium ion by Pseudomonas aeruginosa ATCC 27853 were initial concentration 50ppm, feeding velocity 30mL/hr.

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Photocatalytic Degradation of Benzene in the Gas Phase using TiO2 Coated on Ceramic and Glass Beads (세라믹과 유리에 코팅한 TiO2 광촉매를 이용한 가스상 벤젠의 제거)

  • 손현석;양원호;김현용;이소진;박종래;조경덕
    • Journal of Korean Society for Atmospheric Environment
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    • v.19 no.1
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    • pp.57-66
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    • 2003
  • TiO$_2$ sol was prepared by sol-gel method, and this sol was coated in ceramic and glass bead by dip-coating method. The coated catalyst was applied to degrade benzene in the gas phase by exposing to UV -lamp (365 nm) in a batch reactor. The removal efficiency of the benzene was compared by changing various conditions such as the kind of chemical additives, the coating beads (ceramic and glass), solution pH, the initial concentration of TiO$_2$ sol, UV intensity, and benzene concentration. The physical structure of TiO$_2$ sol used in this study was found to be pu-rely anatase type from XRD analysis. The results showed that ceramic bead was effective as the coating agent rath-er than glass bead. The significant change in the benzene removal efficiency of benzene did not occur with chang-ing coating frequency and the initial concentration of TiO$_2$ sol. The removal efficiency of benzene increased with increasing UV intensity, and with acidic treatment of TiO$_2$-coated ceramic bead.

Estimating the Viability of Bifidobacterium longum in Ca-Alginate Beads Against Simulated Gastroenteric Juices

  • Lee, Ki-Yong;Kim, Ji-Youn;Lee, Yoon-Jong;Choi, Eon-Ho;Shin, Dong-Hoon;Heo, Tae-Ryeon
    • Journal of Microbiology and Biotechnology
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    • v.11 no.1
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    • pp.97-105
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    • 2001
  • The viability of Bifidobacterium longum KCTC 3128, entrapped in calcium alginate beds in simulated gastroenteric juices (gastric and bile salt solution), was tested to evaluate the influences of several parameters (gel concentration, bead size, and initial cell number). The death rate of B. longum in beads after being sequentially exposed to simulated gastric juices and bile salt solution decreased propertionally with increasing both the alginate gel concentration and bead size. The number of initial cell loading in beads affected the numbers of survivors after being exposed to these solutions, while the death rate of the viable cells were not affected. From the results obtained, the influence of entrapment parameters on the survival of bifidobacteria was quantitatively and systematically evaluated by using a mathematical method.

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