• Tribology and Lubricants
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• 제13권4호
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• pp.60-65
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• 1997

The tungsten disulfide $(WS_2)$ solid lubricant was synthesized by two different reaction processes, i.e., the reaction between $CS_2$ gas phase and solid $WO_3$powder, and the vapour phase transport method of tungsten and sulfur in a high vacuum. The chemical and physical characteristics of synthesized $WS_2$powder were analyzed in terms of the average particle size, morphology, crystalline phase etc. in comparison with those of commercial $WS_2$powder. The solid $WO_3$ powder with the average size of 0.2 ${\mu}{\textrm}{m}$ was reacted with $CS_2$gas flowed with$N_2$or 96%$N_2{\times}4%H_2$forming gas for 36 h and 24 h at 90$0^{\circ}C$ respectively. $WS_2$ crystalline phase was then formed through the intermediate phase of .$W_{20}O_{58}$ In the case of vapour phase transport method, the 3.5 wt% iodine was added as a vapour transport reagent into the composition of tungsten and sulfur powders maintaining a constant molar ratio of W:S=1:2.2. The mixture was then heat treated at 85$0^{\circ}C$ for 2 weeks in vacuum. The reaction product obtained showed the average size of 12 ${\mu}{\textrm}{m}$ and the hexagonal plate shape of typical solid lubricant with 2H-$WS_2$crystalline phase.

• International Journal of Air-Conditioning and Refrigeration
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• 제6권
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• pp.56-66
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• 1998

The absorption process of water vapor in a liquid film is an important process in LiBr-Water absorption system. The composition of the gas phase, in which a non-absorbable gas is combined with the absorbate, influences the transport characteristics. In the present work, the absorption processes of water vapor into aqueous solutions of lithium bromide in the presence of non-absorbable gas are investigated. The continuity, momentum, energy and diffusion equations for the solution film and gas are formulated in integral forms and solved numerically. It is found that the mass transfer resistance in gas phase increases with the concentration of non-absorbable gas. However the primary resistance to mass transfer is in the liquid phase. As the concentration of non-absorbable gas in the absorbate increases, the interfacial temperature and concentration of absorbate in solution decrease, which results in the reduction of absorption rate. The reduction of mass transfer rate is found to be significant for the addition of a small amount of non-absorbable gas to the pure vapor, especially at the outlet of tube where the non-absorbable gas accumulates. At higher non-absorbable gas concentration, the decrease of absorption rate seems to be linear to the concentration of non-absorbable gas.

• 한국기계가공학회지
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• 제19권10호
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• pp.1-7
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• 2020

In this study, a multichannel gas-liquid microextraction system is designed by integrating the automatic elution of extraction line and multichannel gas-purging liquid phase microextraction. The system uses an injection pump and inert gas to push the extraction solvent to a sample bottle of a gas-phase color autosampler and then implements multichannel gas-liquid microextraction and gas chromatography-mass spectrometry. The system also employs a three-way integrated micro-high-temperature heater, syringe pump, and microflow controller to realize the simultaneous processing of multiple groups of samples, thus improving the sample pretreatment speed and reproducibility and reducing human error. Autoinjection experiments were implemented with polycyclic aromatic hydrocarbon standard samples. The experiments show that the average recovery rate of the system exceeds 70%, and the relative standard among the channels is less than 15%.

• 대한기계학회논문집
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• 제9권6호
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• pp.743-749
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• 1985

본 연구에서는 Gas Chromatograph를 사용하여 1,500㏄급 국산 소형 승용차 엔 진의 배기가스 성분을 분석하였다. 그리고 이를 통하여 배개가스 성분 분석에 Gas Chromatograph를 사용할 경우 아래와 같은 점에 유의한다면 배기가스 성분을 비교적 정확하게 측정할 수 있다는 것을 확인하였다.

• 한국항공우주학회지
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• 제37권1호
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• pp.1-16
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• 2009

최근 공학적으로 응용 범위가 넓은 액체-기체의 2상 유동장에 대한 전산 해석이 주목을 받고 있다. 본 연구에서는 밀도차가 큰 압축성 2상 유동장을 해석하기에 적합하도록 기존에 개발된 RoeM과 AUSMPW+ 공간 이산화 기법을 확장하였다. RoeM과 AUSMPW+에서 사용되는 충격파 포착항을 2상 혼합류의 상태방정식으로부터 새롭게 정의하여, 밀도와 음속이 상이한 두 유체에서도 정확성을 보장하면서 충격파 불안정성을 제거할 수 있도록 하였다. 개발된 2상 유동 RoeM과 AUSMPW+를 몇 가지 예제 문제에 적용하여 검증하였으며, 해석 결과는 두 수치기법이 일반적인 2상 유동에서도 충격파 안정적이며 정확한 특성을 갖는 것을 보여주었다.

• 한국재료학회지
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• 제12권6호
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• pp.427-430
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• 2002

Plasma nitrocarburizing treatment was performed for SCM 435 steel by using a plasma ion nitriding system. The effects of the variation of nitrogen and methan contents upon the hardened layer was investigated. Both the thickness of the compound layer and the amount of $\varepsilon$ phase in the compound layer increased with increasing nitrogen content. However, the thickness of the compound layer decreased due to unstable plasma for an atmosphere containing 90% $N_2$ gas content in the gas mixture. The amount of $\varepsilon$phase in the compound layer increased with increasing $CH_4$ gas content. For $CH_4$ gas content more than 2% in the gas mixture, the thickness of the compound layer decreased due to the formation of $\theta$ phase.

• 한국가스학회지
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• 제10권4호
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• pp.1-5
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• 2006

가스 소비의 급증으로 천연가스의 수송수단인 배관의 역할이 증가하고 있다. 일반적으로 배관으로 가스를 수송할 경우, 주로 컨덴세이트 형성에 기인하는 일부 액체가 관내에 형성되어 가스 산업현장에서 복잡한 조업 상의 문제점을 발생시킨다. 그러므로, 가스 컨덴세이트의 존재가 조업 효율에 미치는 영향을 예측할 수 있는 적절한 방법이 필요하다. 본 연구에서는 통합된 단상/2상 유동개념을 사용하여 가스 컨덴세이트의 발생 시작점과 그 발생량의 영향이 출구 압력에 미치는 영향을 분석할 수 있는 통계 모델을 개발하였다. 또한 컨덴세이트 발생 시작점 이후, 2상 유동지역에서 유동형태의 변화가 출구 압력에 미치는 영향도 분석되었다.

• 대한전기학회:학술대회논문집
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• 대한전기학회 2007년도 학술대회 논문집 전문대학교육위원
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• pp.88-92
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• 2007

In this paper, the basic experiment, electrolytic cell design and basic manufacturing have been made to interpret the characteristics of Hydrogen-Oxygen-Gas-Generator. As for the detailed matters, the data research on basic technology on Hydrogen-Oxygen-Gas and analysis on characteristics of Hydrogen-Oxygen-Gas from basic experiment. Also the experiment of characteristics and comparative evaluation between constant current source using IGBT converter from existing method and constant current source using new phase shift PWM control method converter. As results when it has injected constant DC current, we has compared Gas quantities by variable ripple frequencies using phase shift PWM control method converter. Therefore, in linear region, it has not different Gas quantities by constant DC current and by phase shift PWM control method converter. Also, it has increased Gas quantities wilder linear region when put ripple frequency at saturation region. Through, Gas quantities and input power, it has acquired higher input power per Gas quantities at put pulse curren. Therefore, when designing converter or inverter for electrolysis, which has ripple current.

• 한국추진공학회지
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• 제22권6호
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• pp.84-93
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• 2018

냉각제 분사조건이 변화할 때 혼합가스 사출시스템 (또는 가스-스팀 발사체계) 냉각효율 및 발사체 사출성능의 변화를 확인하기 위해 3차원 수치모사를 수행하였다. 선행연구를 참조하여 구축한 1차원 모델을 통해 3차원 단상(single-phase) 계산모델을 검증한 후, Discrete Phase Model을 활용하여 고온의 기체에 냉각제 분사를 모사한 이상(two-phase) 유동 계산을 수행하였다. 냉각제 유량과 분사구 개수를 각각 변화시키면서 계산을 수행한 결과, 분사구 개수를 증가시켰을 경우 냉각효율이 보다 개선되었다. 또한 분사조건에 따라 냉각제 액적 서로간의 coalescence 발생 빈도 및 공간분포 변화가 발생하여 액적의 직경이 달라졌고, 이는 냉각제 증발률에 영향을 미쳤다. 냉각제의 증발은 breech 내부의 온도를 감소시키는 반면에 압력감소를 억제하여 사출시스템 최적화 설계에 있어 중요한 요소임을 확인하였다.

• 한국안전학회지
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• 제9권3호
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• pp.67-73
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• 1994

The gas holdup and volumeteric liquid phase mass transfer coefficient with the variation of the concentration of CMC aqueous solution, gas velocity, diameter and area of the draught tube were investigated. As the results of the experiments, the gas holdup and volumetric liquid phase mass transfer coefficient decreased with decreasing the concentration of CMC aqueous solution, increased with increasing the gas velocity and increased with increasing the circulated area ratio of the draught tube.