• Title/Summary/Keyword: Gas detector

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Rapid Measurement of VOC Using an Analysis of Soil-Gas (Soil-Gas의 분석을 이용한 휘발성 유기화합물 오염도 신속측정)

  • 김희경;조성용;황경엽
    • Journal of Korea Soil Environment Society
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    • v.3 no.1
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    • pp.3-9
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    • 1998
  • This paper presents soil-gas surveying technique to delineate an area contaminated with volatile organic compounds, which are common solvents and constituents of gasoline. The sampling method of soil-gas surveying is 1) grab sampling, which actively takes sample using a pump, or 2) passive sampling, which takes sample through diffusion in a trap filled with absorbent. The grab sampling shows the level of contamination at a certain location at a certain time, while the passive sampling shows the change in the contamination at a certain location. The analysis of soil gas can be performed with 1) a small portable detectors such as PID (photoionization detector) or FID (flame-ionization detector) to measure the total hydrocarbon in the soil gas, 2) a gas detector tube, which is filled with indicator reagents and changes its color with concentrations of the gas of interest, or 3) a portable GC (gas chromatograph), which can analyze different compounds simultaneously. The soil-gas surveying technique is a much less expensive method to investigate area contaminated volatile organic compounds and thus can be used as a screening tool to identify an area, which needs to be further investigated.

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Hybrid Operational Concept with Chemical Detection UAV and Stand-off Chemical Detector for Toxic Chemical Cloud Detection (화학오염운 탐지를 위한 접촉식 화학탐지기를 탑재한 무인기와 원거리 화학탐지기의 복합 운용개념 고찰)

  • Lee, Myeongjae;Chong, Eugene;Jeong, Young-Su;Lee, Jae-Hwan;Nam, Hyunwoo;Park, Myung-Kyu
    • Journal of the Korea Institute of Military Science and Technology
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    • v.23 no.3
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    • pp.302-309
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    • 2020
  • Early-detection and monitoring of toxic chemical gas cloud with chemical detector is essential for reducing the number of casualties. Conventional method for chemical detection and reconnaissance has the limitation in approaching to chemically contaminated site and prompt understanding for the situation. Stand-off detector can detect and identify the chemical gas at a long distance but it cannot know exact distance and position. Chemical detection UAV is an emerging platform for its high mobility and operation safety. In this study, we have conducted chemical gas cloud detection with the stand-off chemical detector and the chemical detection UAV. DMMP vapor was generated in the area where the cloud can be detected through the field of view(FOV) of stand-off chemical detector. Monitoring the vapor cloud with standoff detector, the chemical detection UAV moved back and forth at the area DMMP vapor being generated to detect the chemical contamination. The hybrid detection system with standoff cloud detection and point detection by chemical sensors with UAV seems to be very efficient as a new concept of chemical detection.

X-ray properties measurement of Flat panel Digital X-ray gas detector (평판형 디지털 엑스레이 가스 검출기의 엑스선 특성 측정기술에 관한 연구)

  • Yoon, Min-Seok;Cho, Sung-Ho;Oh, Kyung-Min;Jung, Suk-Hee;Nam, Sang-Hee;Park, Ji-Goon
    • Journal of the Korean Society of Radiology
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    • v.3 no.1
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    • pp.17-21
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    • 2009
  • The Recently, large area matrix-addressed image detectors are investigated for X-ray imaging with medical diagnostic and other applications. In this paper, a new flat panel gas detector for diagnostic X-ray imaging is proposed, and its characteristics are investigated. The research of flat panel gas detector is not exist at all. Because of difficulty to inject gas against to atmospheric pressure. So almost gas detector made by chamber shape. We made flat panel sample by display technique. (ex: PDP, Fed, etc.) The experimental measurements, the transparent electrodes, dielectric layer, and the MgO protection layer were formed in front glass. And, the X-ray phosphor layer and address electrodes are formed in the rare glass. The dark current, the x-ray sensitivity and linearity as a function of electric field were measured to investigate the electrical properties. From the results, the stabilized dark current density and the significant x-ray sensitivity were obtained. And the good linearity as a function of exposure dose was showed in wide diagnostic energy range. These results means that the passive matrix-addressed flat panel gas detector can be used for digital x-ray imaging.

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폐기물 매립지 토양에서의 PCBs 분석법

  • Lee Jeong-Hwa;Jeon Chi-Wan;Jeong Yeong-Uk
    • Proceedings of the Korean Society of Soil and Groundwater Environment Conference
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    • 2005.04a
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    • pp.199-201
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    • 2005
  • This paper describes a simple procedure for the quantitative analysis of 7 PCBs (polychlorinated biphenyls) in soils on the waste reclaimed land, The procedure involved sample clean up using silicagel column, acetonitrile partition and sulfuric acid procedures. The instrumental technique is applied GC/PDD(gas chromatography/pulsed discharge detector) and GC/ECD(gas chromatography/electron capture detector). Concentration of $sub-{\mu}g/g$ level was attainable with 20g soils on the waste reclaimed land.

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A Study for Measurements of In-Cylinder Residual Gas Fraction using Fast Response FID in an SI Engine (스파크점화기관에서 고속응답 FID를 이용한 실린더내 잔류가스량 측정에 관한 연구)

  • 송해박;조한승;이종화;이귀영
    • Transactions of the Korean Society of Automotive Engineers
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    • v.6 no.1
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    • pp.80-89
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    • 1998
  • The residual gas in an spark-ignition engine is one of important factors on emissions and performance such as combustion stability. With high residual gas fractions, flame speed and maximum combustion temperature are decreased and these are deeply related with combustion stability especially at idle and NOx emission at relatively high engine load. Therefore, there is a need to characterize the residual gas fraction as a function of the engine operating load. Therefore, there is a need to characterize the residual gas fraction as a function of the engine operating parameters. In the present study, the quantitative measurement technique of residual gas fraction was studied by using Fast Response Flame Ionization Detector(FRFID). The measuring technique and model for estimation of residual gas fraction were reported in this paper. By the assuming that the raw signal from FRFID saturates with the same slope for firing and misfiring cycle, in-cylinder hydrocarbon(HC) concentration can be estimated. Residual gas fraction can be obtained from the in-cylinder HC concentration measured at firing and motoring condition. The developed measurement and calibration procedure were applied to the limited engine operating and design condition such as intake manifold pressure and valve overlap. The results show relevant trends by comparing those from previous studies.

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A Basic Study for the Performance Evaluation of a Raman LiDAR Detector for Detecting Hydrogen Gas (수소 가스 검출용 라만 라이다 측정기의 성능 평가를 위한 기초 연구)

  • WONBO CHO;YUNKYU LIM;YANGKYUN KIM;BYOUNGJIK PARK
    • Transactions of the Korean hydrogen and new energy society
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    • v.34 no.2
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    • pp.205-211
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    • 2023
  • Hydrogen gas is light and diffuses very quickly. Therefore, when a leakage accident occurs, the damage is great, so a technology that can quickly measure the leakage in the air at a long distance is needed. In order to develop hydrogen gas leaked in the atmosphere in a non-contact manner, an experiment was performed to measure hydrogen gas using a lidar technology using the Raman effect. Hydrogen Raman signals were detected using a UV LED light source, which is a Raman light source, and a spectrometer in the ultraviolet region including an optical filter in the 400-430 nm band. To develop this, a Raman lidar optical structure was designed to measure the hydrogen Raman signal at a certain distance, and the hydrogen Raman spectrum was confirmed using a standard gas to evaluate the performance of this optical structure. The linearity was found to be 0.99 using hydrogen standard gas (10, 50, 100, 500, 1,000 ppm). Accordingly, a Raman lidar capable of measuring hydrogen gas rapidly diffusing in the air in an open state was developed to improve the limitations of existing hydrogen sensors.

Comparison of Solid Phase Microextraction-Gas Chromatograph/Pulsed Flame Photometric Detector (SPME-GC/PFPD) and Static Headspace-Gas Chromatograph/Pulsed Flame Photometric Detector (SH-GC/PEPD) for the Analysis of Sulfur-Containing Compounds (Solid phase microextraction-gas chromatograph/pulsed flame photometric detector(SPME-GC/PFPD)와 static headspace-gas chromatograph/pulsed flame photometric detector(SH-GC/PEPD)를 이용한 황 함유 화합물들의 분석 방법 비교)

  • Yang, Ji-Yeon;Kim, Young-Suk
    • Korean Journal of Food Science and Technology
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    • v.37 no.5
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    • pp.695-701
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    • 2005
  • Efficient method was established for analysis of sulfur-containing compounds, including dimethyl disulfide, dimethyl trisulfide, 3-methyl thiophene, allyl mercaptan, 2-methyl-3-furanthiol, and methional. Sulfur-containing compounds were extracted through solid phase microextraction (SPME) or static headspace extraction (SH), and quantified using gas chromatograph equipped with pulsed flame photometric detector. All sulfur compounds, except ally mercaptan, showed higher detection response when dissolved in hexane than in dichloromethane. Linear range was $10^2-10^4$. Dimethyl trisulfide showed lowest limit of detection (LOD) value of 15.2 ppt, and methional highest of 70.5 ppb. Highest extraction efficiency for sulfur-containing compounds, particularly polar and small molecular weight compounds, was observed in 75mm carboxen/polydimethylsiloxane fiber, followed by 65mm polydimethylsiloxane/divinylbenzene and 100mm polydimethylsiloxane. Compared to SPME, less sulfur-containing compounds could be analyzed by SH, mainly due to its low extraction efficiency, although lower amount of artifacts were formed during sample preparation.

Analysis of Benzophenone in Sediment and Soil by Gas Chromatography/Mass Spectrometry (기체크로마토그래피/질량분석기에 의한 저질 및 토양시료 중 벤조페논의 분석법 연구)

  • 권오승;김은영;류재천
    • Environmental Analysis Health and Toxicology
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    • v.16 no.3
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    • pp.121-126
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    • 2001
  • Analytical method of benzophenone (BP) in sediment and soil was developed by gas chromatography/mass selective detector/selected ion monitoring (GC/MSD/SIM). The ultrasonic extraction of US EPA (method 3550B) method and liquid-liquid extraction for sediment and soil samples were used for the analysis of BP from sediment and soil. BP was extracted with n-hexane. Organic layer was washed with 5% sodium chloride solution. 1∼2 l of the concentrated solution of organic layer was applied to GC/MSD. The retention time of BP peak was 11.10 min. Recovery (%) of BP by ultrasonication from sediment and soil samples was 96.0∼100.6% and 40.0∼83.0%, respectively. Recovery of BP by liquid-liquid extraction was 51∼59% in soil samples. The detection limit of BP in sediment and soil samples were determined to 0.1 ng/g.

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Gas Detector for Hydrogen Dissolved in Transformer Oil

  • Seo Ho-Joon;Hwang Kyu-Hyun;Rhie Dong-Hee
    • KIEE International Transactions on Electrophysics and Applications
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    • v.5C no.2
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    • pp.72-75
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    • 2005
  • In oil-filled equipment such as transformers, partial discharge or local overheating will precede a final shutdown. Accompanied with such problems is a decomposition of insulating material into gases, which are dissolved into the transformer oil. The gases dissolved in oil can be separated with some membranes based on the differences in permeability of membranes to different gases. This paper discuss the permeability characteristics of several membranes for separation hydrogen gas in oil. With result of this paper, it may become possible to detect fault-related gases from transformer oil and predict incipient failures in the