• Proceedings of the Korean Vacuum Society Conference
• /
• 2016.02a
• /
• pp.153-153
• /
• 2016

Polyoxymethylene copolymer (POM-C) is an attractive and widely used engineering thermoplastic across many industrial sectors owing to outstanding physical, mechanical, self-lubricating and chemical properties. In this research work, the POM-C blocks were irradiated with 1 MeV electron beam energy in five doses (100, 200, 300, 500 and 700 KGy) in vacuum condition at room temperature. The tribological and physico-chemical properties of electron beam irradiated POM-C blocks have been analyzed using Pin on disk tribometer, Raman spectroscopy, SEM-EDS, Optical microscopy, 3D Nano surface profiler system and Contact angle analyzer. Electron beam irradiation at a dose of 100 kGy resulted in a decrease of the friction coefficient and wear loss of POM-C block due to well suited cross-linking, carbonization, free radicals formation and energetic electrons-atoms collisions (physical interaction). It also shows lowest surface roughness and highest water contact angle among all unirradiated and irradiated POM-C blocks. The irradiation doses at 200, 300, 500 and 700 kGy resulted in increase of the friction coefficient as compared to unirradiated POM-C block due to severe chain scission, chemical and physical structural degradation. The electron beam irradiation transferred the wear of unirradiated POM-C block from the abrasive wear, adhesive wear and scraping to mild scraping for the 1 MeV, 100 kGy irradiated POM-C block which is concluded from SEM-EDS and Optical microscopic observations. The degree of improvement for tribological attribute relies on the electron beam irradiation condition (energy and dose rate).

• Tribology and Lubricants
• /
• v.33 no.5
• /
• pp.220-227
• /
• 2017

In this work, carbon nanotube and nano-size alumina particle are exploited as additive for lubrication experiment. We used pin-on-disk type tribometer to investigate the tribological characteristics of lubricants with respect to additives and rotational speed. We conducted more than 15 trials of tribotests for two hours for each specimen to obtain stable and accurate frictional force and to create measurable wear track on the substrate. We conducted tests at the boundary/mixed lubrication regime to evaluate the influence of additives on the tribological characteristics. We found that the friction coefficient decreased as the rotational speed increased and as additives were added. In particular, the reduction of friction by adding additives was more significant at low rotational speed than at high rotational speed. We speculate that the additives helped to separate and protect the two contacting surfaces at low speed, while the influence of additives was not significant at high speed since sufficiently thick lubricant film was formed. The wear of the substrate was also reduced by adding additives to the lubricant. However, in contrast to friction, the amount of wear at high rotational speed was less when alumina particles were added to the lubricant than the amount of wear at low speed. We speculate that the increased wear at low rotational speed is as a result of the intermittent abrasive wear caused by alumina particles with uneven shape, while the reduced wear at high speed is as a result of sufficient film thickness which prevented the abrasive wear.

• Tribology and Lubricants
• /
• v.38 no.1
• /
• pp.15-21
• /
• 2022

Diamond reinforced Cr-based coating has been proposed as wear-resistant materials. In this study, the friction and wear characteristics of diamond reinforced Cr-based coating are experimentally assessed. The experiments are performed using a pin-on-reciprocating plate tribo-tester under various normal forces with boundary lubrication. The stainless-steel ball is used as a counter material. Prior to the experiments, mechanical properties such as elastic modulus and hardness are determined using nanoscale instrumented indentation. The hardness of the specimen is further determined using a Vickers hardness tester. The specimens before and after the experiments are carefully observed using a confocal microscope to understand the wear characteristics. In addition, the wear volume and wear rate of the specimens are determined based on the confocal microscope data. The results show that the friction coefficients are 0.096-0.100 under 20-40 N normal forces. Furthermore, the wear rates of the diamond reinforced Cr-based coating and the stainless steel ball under 20-40 N normal forces are found to be 12.8 × 10^-8 mm³/(Nm)-15.5 × 10^-8 mm³/(Nm) and 1.9 × 10^-8 mm³/(Nm)-3.9 × 10^-8 mm³/(Nm), respectively. However, the effect of the normal force on wear rates is not clearly observed, which may be associated with the flattening of the ball. The results of the study may be useful for the tribological applicability of diamond reinforced Cr-based coating as wear-resistant materials.

• Proceedings of the Korean Society of Tribologists and Lubrication Engineers Conference
• /
• 1999.06a
• /
• pp.14-19
• /
• 1999

In order to evaluate the effect of Nb on wear properties of high speed steel by powder metallurgy(PM-HSS), niobium-alloyed PM-HSS have been prepared by adding 0%, 1%, 3% and 5%Nb to PM-HSS of 6%W-5%Mo-4%Cr-5%V-5%Co presented in the previous paper. Sliding wear test have been conducted in various sliding speed conditions under the constant pressure using a pin-on-disc type machine. The results of this study shows that the wear resistance of PM-HSS has been increased by the addition of Nb in the range of experimental sliding speed. However, the amount of Nb shows to be unimportant parameter for the improvement of the wear resistance. It may be due to the thermal stability of carbide and high temperature properties of matrix by adding Nb comparing to the case of no addition.

• Tribology and Lubricants
• /
• v.19 no.3
• /
• pp.151-158
• /
• 2003

In metal cutting at the tool-chip interface, friction generates considerable amount of heat. Thus, the knowledge of wear properties of cutting tool material in high temperature has been as one of important factors in need of clarification. The authors presented the wear properties of 5%Co-5%V-1%Nb high speed steel, fabricated by powder metallurgy, in room temperature in previous articles. The objective of this paper is to clarify the effects of temperature on its wear properties. Wear tests in sliding conditions under various temperatures have been conducted using the pin-on-disc type wear test machine. The results indicate that the wear properties of 5%Co-5%V-1%Nb high speed steel in high temperature as well as in room temperature are excellent. It may be deduced that the oxide layer formed on worn surface at high temperature is stable enough to prevent wear due to the high temperature strength of its matrix.

• Tribology and Lubricants
• /
• v.23 no.6
• /
• pp.318-322
• /
• 2007

The wear characteristics in supre-A dental material have been investigated. The wear tests were performed by using pin-on-disk wear tester at room temperature. Vickers hardness and fracture toughness measurement of dental materials were preformed. Microscopic observations on worn surfaces of specimens were conducted by SEM. The friction coefficient of supper-A material was investigated according to weight and slinging velocity. The hardness of supper-A material was a half of the enamel of natural teeth.

• Proceedings of the Korean Society of Tribologists and Lubrication Engineers Conference
• /
• 2000.06a
• /
• pp.76-83
• /
• 2000

Boundary lubrication condition arises in most lubricated systems, especially during motion reversals and start up phase of operation. In this work electric contact resistance variations with respect to sliding conditions under lubrication is investigated The motivation was to improve the understanding of the contact condition in the boundary lubrication regime. It is shown that electrical contact resistance is sensitive to sliding speed and surface condition of the specimens. Also, phenomena such as run-in during the initial phase of sliding and lubricant pile up near the sliding pin could be observed. The results of this work will aid in better understanding of the metal to metal contact condition in lubricated systems.

• Tribology and Lubricants
• /
• v.15 no.3
• /
• pp.265-271
• /
• 1999

Wherever there are rotating equipment and contact between surface, there is wear and the generation of wear particles. The particles contained in the lubricating oil carry detailed and important information about the condition monitoring of the machine. This information may be deduced from particle shape, composition, size distribution, and concentration. Therefore, This paper was undertaken to Ferrography system of wear debris generated from lubricated moving machine surface. The lubricating wear test was performed under different experimental conditions using the Falex wear test of Pin and V-Block type by Ti(C, N) coated. It was shown from the test results that wear particle concentration (WPC) and wear severity Index( $I_{S}$), size distribution in normal and abnormal wear have come out all the higher value by increases sliding friction time. Wear shape is observed on the Ferrogram it was discovered a thin leaf wear debris as well as ball and plate type wear particles. This kind of large wear shape have an important effect not only metals damage, but also seizure phenomenon.

• Proceedings of the Materials Research Society of Korea Conference
• /
• 2003.03a
• /
• pp.28-28
• /
• 2003

고온가압소결(Hot Pressing) 된 다이아몬드 공구용 Co-Fe, Co-Ni계 금속본드의 상온 건식 미끄럼 마멸시험을 행하고, 조성에 따른 각 본드의 마멸 특성을 비교하고 마멸 기구를 규명하였다. 미끄럼 마멸시험은 pin-on-disk 형태의 마멸시험기를 사용하여 각 조성의 성분, 적용하중 그리고 마멸상대재를 변수로 상온, 대기 중에서 실시되었다. 마멸속도는 마멸시험 전후의 시편의 무게 감량을 이론밀도와 거리로 나누어 계산되었다. 마멸기구의 규명을 위하여 시험된 시편의 마멸면과 마멸단면을 SEM과 EDS를 이용하여 분석하였다. 시험 결과 Co-Fe system의 경우 그 마멸속도는 마멸상대재의 영향보다는 Fe 첨가에 따른 시편의 미세조직과 기계적 성질의 차이에 따라 크게 변화하였다. 그러나 Co-Ni system의 마멸속도는 마멸 상대재에 따라 크게 변화하는 것이 관찰되었다. $Al_2$O$_3$를 상대재로 마멸된 경우에는 마멸속도가 시편/상대재 접촉면에서 형성되는 산화층의 영향을 크게 받았고, glass bead(83% SiO$_2$)를 상대재로 한 경우에는 시편의 경도와 마멸속도는 서로 반비례하였다.

• Journal of the Korean institute of surface engineering
• /
• v.29 no.1
• /
• pp.26-35
• /
• 1996

The Ni-SiC composite plating was performed in a Watt nickel solution and the wear resistance of the composite layer was studied on a pin-on-flat type wear tester. The volume losses and friction coefficients were measured. It was found that the quantity of SiC powder in the composite layers was affected by SiC concentration, pH, temperature, and agitation speed in the Watt nickel solution. The hardness and wear resistance of the coatings increased with SiC content. The quantity of SiC powder in the coating from a nickel sulfamate solution is larger than that of the Watt nickel solution, because the amount of nickel ions absorbed on the SiC powder in the nickel sulfamate solution is greater than that in the Watt's solution.