• 한국해안해양공학회지
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• 제19권4호
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• pp.355-360
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• 2007

본 논문에서는 수심이 일정한 수조에서의 비선형 천해파의 변형 과정에 대한 연구를 수행하였다. 파랑의 최초 쇄파에 대한 특성을 자세히 분석하고, 비선형파의 경사 및 퓨리에 스펙트럼을 산정하였다. 분석결과 스펙트럼의 진폭은 실용적으로 추산이 가능한 파랑 경사를 이용하여 표현할 수 있다.

• 음성과학
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• 제8권4호
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• pp.45-58
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• 2001

Modulated components of a speech signal are frequently used for speech coding, speech recognition, and speech synthesis. Time-frequency representation (TFR) reveals some information about instantaneous frequency, instantaneous bandwidth and boundary of each component of the considering speech signal. In many cases, the extraction of AM-FM components corresponding to instantaneous frequencies is difficult since the Fourier spectra of the components with time-varying instantaneous frequency are overlapped each other in Fourier frequency domain. In this paper, an efficient method decomposing speech signal into AM-FM components is proposed. A variable bandwidth filter is developed for the decomposition of speech signals with time-varying instantaneous frequencies. The variable bandwidth filter can extract AM-FM components of a speech signal whose TFRs are not overlapped in timefrequency domain. Also, amplitude and instantaneous frequency of the decomposed components are estimated by using Hilbert transform.

• Nuclear Engineering and Technology
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• 제49권3호
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• pp.534-540
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• 2017

The adsorption of uranium (VI) by calcium alginate beads was examined by batch experiments. The effects of environmental conditions on U (VI) adsorption were studied, including contact time, pH, initial concentration of U (VI), and temperature. The alginate beads were characterized by using scanning electron microscopy, transmission electron microscopy, X-ray photoelectron spectroscopy, and Fourier transform infrared spectroscopy. Fourier transform infrared spectra indicated that hydroxyl and alkoxy groups are present at the surface of the beads. The experimental results showed that the adsorption of U (VI) by alginate beads was strongly dependent on pH, the adsorption increased at pH 3~7, then decreased at pH 7~9. The adsorption reached equilibrium within 2 minutes. The adsorption kinetics of U (VI) onto alginate beads can be described by a pseudo first-order kinetic model. The adsorption isotherm can be described by the Redlich-Peterson model, and the maximum adsorption capacity was 237.15 mg/g. The sorption process is spontaneous and has an exothermic reaction.

• 분석과학
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• 제5권4호
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• pp.455-464
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• 1992

본 논문에서는 FT-IR 분광분석법을 이용하여 여러 가지 반응조건에서 기체상 silylation 반응에 의해 생성된 silylated layer의 depth를 비파괴적으로 정량하는 방법을 제안하였다. Silylated layer의 depth는 FT-IR 스펙트럼의 특성 봉우리들(Si-O-ph, Si-C, Si-H)의 흡광도를 바탕 스펙트럼 공제법으로 측정하여 SEM의 두께 측정치와 비교하여 정량하였다. FT-IR 분광분석법을 이용한 Silylated layer의 depth 분석은 비파괴적이고 정량적인 방법으로, 이 방법은 silylation process window를 설정하는 데 적합하다는 것을 알았다.

• 한국콘텐츠학회논문지
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• 제13권10호
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• pp.1-8
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• 2013

본 논문에서는 집적영상의 획득 과정에서 발생하는 기하학적 왜곡 중 투영 왜곡을 교정하는 방법을 제안한다. 제안된 방법에서는 집적영상의 스펙트럼 특성을 이용하여 왜곡 교정을 수행한다. 집적영상의 요소영상들이 대체로 주기적으로 반복됨에 따라 집적영상을 푸리에 변환하였을 경우 그 스펙트럼이 임펄스열로 나타난다. 반면, 왜곡이 존재하는 영상에서는 임펄스열이 뚜렷하게 나타나지 않는 특성이 있다. 따라서 집적영상의 푸리에 변환을 통해 얻어진 스펙트럼의 특성을 이용하여 투영 왜곡 파라미터를 찾아내고 이를 이용하여 교정하는 방법을 제안한다. 실험을 통하여 제안된 방법이 왜곡을 효과적으로 교정하는지 검증한다.

• 약학회지
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• 제47권6호
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• pp.461-468
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• 2003

A method is described for measuring clinically relevant levels of glucose in a pH 7.4 phosphate buffer by nearinfrared (NIR) absorption spectroscopy. Three types of NIR spectrometer, dispersive type, photo-diode array (PDA) type, and fourier transform (FT) type spectrometer were used and the performance was compared. Spectra were collected with a cuvette cell or quartz liquid fiber of 1 mm or 2 mm optical pathlength as transmittance method. Glucose absorption band appeared at second overtone, first overtone, and combination region for all systems. By use of the multivariate technigue of partial least squares (PLS) regression, glucose concentrations can be determined with a 16, 44, and 9.1 mg/d l standard error of prediction for dispersive type, photo-diode array type, and fourier transform type system, respectively. Sensitivity of spectrometer was evaluated by absorbance for the difference of 10 mg/d l glucose. Three absorption bands, second overtone, first overtone, and combination region were suited to three types systems, dispersive type, photo-diode array type, and fourier transform type systems, respectively. This investigation showed that three types NIR spectrometer were proper method for identification and quantitative analysis of glucose and possible for noninvasive blood glucose monitoring.

• IEIE Transactions on Smart Processing and Computing
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• 제6권4호
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• pp.246-252
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• 2017

Non-invasive and non-restrictive methods for measuring the physiological functions of the human body are useful for health care, security, and surveillance. In this paper, a new method that extracts human heartbeat information by utilizing ultra-wideband (UWB) impulse radar is proposed. The amplitude spectra of received radar pulses reflected from the human body are accumulated at specific time intervals, and chirp z-transform (CZT) is used to extract the heartbeat frequency from the amplitude spectra. The heartbeat frequency can be extracted with high-frequency resolution in the frequency band of the heartbeat of interest using CZT. Experimental results to verify the performance of the proposed method show that a highly accurate extraction of the heartbeat frequency is possible using this method.

• 한국조명전기설비학회:학술대회논문집
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• 한국조명전기설비학회 1999년도 학술대회논문집-국제 전기방전 및 플라즈마 심포지엄 Proceedings of 1999 KIIEE Annual Conference-International Symposium of Electrical Discharge and Plasma
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• pp.127-131
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• 1999

In this paper, using a wide-band AE sensor with the frequency range from 100[kHz], the frequency spectra of AE signals generated from the corona discharges of the needle-plane electrode was analyzed to determine the proper ultrasonic sensor. We also examined the relationship between the magnitude of corona discharge and the magnitude of AE signals in peak-to-peak value under the application of 60[Hz] AC high-voltage in oil. From these results, the main frequency spectra of AE signals emitted from the corona discharges of the needle-plane gap were found to be 130[kHz] by the fast fourier transform. The magnitude of AE signals was proportional to the magnitude of corona discharge and discharge current pulse with increasing the applied voltages. Also the detection of corona discharge point location by AE signals was found to be possible by using two sensors.

• Journal of Magnetics
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• 제19권2호
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• pp.101-105
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• 2014

In this work, Zinc ferrite nanoparticles have been prepared by various methods, conventional (ZC), mechanochemical processing (ZM) and Sol-Gel (ZS) method, to compare their structural and magnetic properties. The cation distribution obtained from XRD shows the degrees of inversions are 4%, 14.8%, and 16.4% from the normal $ZnFe_2O_4$ structure. Fourier transform infrared spectroscopy (FT-IR) confirms changes in cation distribution of $ZnFe_2O_4$ fabricated by sol-gel and mechanochemical processing. The $^{57}Fe$ M$\ddot{o}$ssbauer spectra of the samples were recorded at room temperature. The spectra exhibit a line broadening. The magnetic properties of the samples were studied by vibration sample magnetometer (VSM) at room temperature and the results show that the sample ZM has ferrimagnetic behaviour.

• Bulletin of the Korean Chemical Society
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• 제31권11호
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• pp.3151-3155
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• 2010

This study was performed to develop analytical methods to better understand the properties and reactivity of petroleum, which is a highly complex organic mixture, using high-resolution mass spectrometry and statistical analysis. Ten crude oil samples were analyzed using negative-mode electrospray ionization Fourier transform ion cyclotron resonance mass spectrometry (ESI FT-ICR MS). Clustering methods, including principle component analysis (PCA), hierarchical clustering analysis (HCA), and k-means clustering, were used to comparatively interpret the spectra. All the methods were consistent and showed that oxygen and sulfur-containing heteroatom species played important roles in clustering samples or peaks. The oxygen-containing samples had higher acidity than the other samples, and the clustering results were linked to properties of the crude oils. This study demonstrated that clustering methods provide a simple and effective way to interpret complex petroleomic data.