• Journal of dental hygiene science
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• v.18 no.1
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• pp.42-49
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• 2018

The computer-aided design/computer-aided manufacturing (CAD/CAM) system was introduced to shorten the production time of all-ceramic restorations and the number of patient visits. Among these types of ceramic for dental CAD/CAM, they have been processed into inlay, onlay, and crown shapes using leucite-reinforced glass-ceramics to improve strength. The purpose of this study was to observe the mechanical properties and microstructure of leucite-reinforced glass-ceramics for dental CAD/CAM. Two types of leucite-reinforced glass-ceramic blocks (IPS Empress CAD, Rosetta BM) were prepared with diameter of 13 mm and thickness of 1 mm. Biaxial flexural testing was conducted using a piston-on-three-ball method at a crosshead speed of 0.5 mm/min. Weibull statistics were used for the analysis of biaxial flexural strength. Fracture toughness was obtained using an indentation fracture method. Specimens were observed by field emission scanning electron microscopy to examine the microstructure of the leucite crystalline phase after acid etching with 0.5% hydrofluoric acid aqueous solution for 1 minute. The results of strength testing showed that IPS Empress CAD had a mean value of $158.1{\pm}8.6MPa$ and Rosetta BM of $172.3{\pm}8.3MPa$. The fracture toughness results showed that IPS Empress CAD had a mean value of $1.28{\pm}0.19MPa{\cdot}m^{1/2}$ and Rosetta BM of $1.38{\pm}0.12MPa{\cdot}m^{1/2}$. The Rosetta BM sample exhibited higher strength and fracture toughness. Moreover, the crystalline phase size and ratio were increased in the Rosetta BM sample. The above results are expected to elucidate the basic mechanical properties and crystal structure characteristics of IPS Empress CAD and Rosetta BM. Additionally, they will help develop leucite-reinforced glass-ceramic materials for CAD/CAM.

• Journal of the Korean Ceramic Society
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• v.33 no.3
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• pp.339-347
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• 1996

Mechanical properties(flexural strength hardness fracture toughness) of alumina ceramics were evaluated. Alumina products of four companies were selected and three of those were made in Korea and one of those was made in Japan. The large differences according to manufacturing companies had resulted from flexural strength and weibull modulus which had a wide ranges of 300 to 400 MPa and 5 to 15 respectively. Critical indenstation load which could be neglected the effect of elastic recovery was about 9.8N and Vickers' hardness were about 15 GPa. Fracture toughnesses were evaluated by IF and ISB method. It was more preferable to the average at one indentation load that fracture toughness were obtained from the slope of the relationship between indentation load and crack length in IF method and between indentation load and fracture load in ISB method and fracture toughness was about 4 MPa·m1/2.

• Journal of the Korea Concrete Institute
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• v.22 no.5
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• pp.651-658
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• 2010

Sixteen concrete mixes reinforced with hybrid steel-polybinyl alcohol (PVA) fibers and a control concrete mix with no fiber were tested in order to examine the effect of the micro and macro fibers on the slump and different mechanical properties of concrete. Main variables investigated were length and volume fraction of steel and PVA fibers. The measured mechanical properties of hybrid fiber reinforced concrete were analyzed using the fiber reinforcing index and compared with those recorded from monolithic steel or PVA fiber reinforced concrete. The initial slump of hybrid fiber reinforced concrete decreased with the increase of the aspect ratio and the volume fraction of fibers. In addition, splitting tensile strength, modui of rupture and elasticity, and flexural toughness index of concrete increased with the increase of the fiber reinforcement index. Modulus of rupture and flexural toughness index of hybrid fiber reinforced concrete were higher than those of monolithic fiber reinforced concrete, though the total volume fraction of hybrid fibers was lower than that of monolithic fiber. For enhancing the flexural toughness index of hybrid fiber reinforced concrete, using the steel fiber of 60 mm length was more effective than using the steel fibers combined with 60 mm and 30 mm lengths.

• Magazine of the Korea Concrete Institute
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• v.6 no.4
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• pp.141-152
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• 1994

The results of an experimental study on the development and the evaluation of lightweight and high strength composites utilizing by-products and calcium silicates for construction materials are presented in this paper. The composites using early strength portland cement, by-Products( f1y ash, silica fume), silica powder, quick lime, gypsum, A1 powder and fibers(PAN-derived CF, alkali-resistance GF) were prepared using various mixing conditions. As the test results show, PAN-derived CF and alkali-resistance GF were suitable for rein-forcing fiber of the composites. And the mechanical properties,such as compressive tensile flexural strength, and toughness of Lt. Wt. fiber reinforced calcium silicates cement comp-osites were improved by increasing the fly ash and silica fume contents, and fiber contents, especially by increasing fiber contents the toughness of the composites were remarkably in-creased. Also, compressive tensile flexural strength,and toughness of the composites rein-forcing PAN-derived CF were higher than those of the composites reinforcing alkali-resistance GF..

• Proceedings of the KSEEG Conference
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• 1999.04a
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• pp.233-235
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• 1999

• Polymer(Korea)
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• v.25 no.2
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• pp.246-253
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• 2001

Amino terminated PES-CTBN-PES triblock copolymer was synthesized from PES oligomer and commercial CTBN rubber (CTBN1300$\times$13), and molecular weight of the copolymer was controlled to be 15000 g/mole. The copolymer was utilized to toughen diglycidyl ether of bisphenol-A (DGEBA) epoxy resin which was cured with 4,4'-diaminodi-phenylsulfone (DDS) and subjected to the measurement of thermal properties, fracture toughness ( $K_{IC}$), flexural properties and solvent resistance. The properties were compared with those from the samples modified by CTBN/PES blends. The maximum loading of copolymer into the epoxy resin was 40 wt% without utilizing solvent, at which $K_{IC}$ fracture toughness of 2.21 MPa${\cdot}m^{0.5}$ was obtained without sacrificing flexural properties and chemical resistance. However, the epoxy resin modified with PES/CTBN blend exhibited much lower $K_{IC}$ and flexural properties compared to the epoxy resins toughened by PES-CTBN-PES copolymers.

• Advances in concrete construction
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• v.8 no.3
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• pp.207-215
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• 2019

Application of nanotechnology can be used to tailor made cementitious composites owing to small dimension and physical behaviour of resulting hydration products. Because of high aspect ratio and extremely high strength, carbon nanotubes (CNTs) are perfect reinforcing materials. Hence, there is a great prospect to use CNTs in developing new generation cementitious materials. In the present paper, a parametric study has been conducted on cementitious composites reinforced by two types of multi walled carbon nanotubes (MWCNTs) designated as Type I CNT (10-20 nm outer dia.) and Type II CNT (30-50 nm outer dia.) with various concentrations ranging from 0.1% to 0.5% by weight of cement. To evaluate important properties such as flexural strength, strain to failure, elastic modulus and modulus of toughness of the CNT admixed specimens at different curing periods, flexural bending tests were performed. Results show that composites with Type II CNTs gave more strength as compared to Type I CNTs. The highest increase in strength (flexural and compressive) is of the order of 22% and 33%, respectively, compared to control samples. Modulus of toughness at 28 days showed highest improvement of 265% for Type II 0.3% CNT composites. It is obvious that an optimum percentage of CNT could exists for composites to achieve suitable reinforcement behaviour and desired strength properties. Based on the parametric study, a tentative optimum CNT concentration (0.3% by weight of cement) has been proposed. Scanning electron microscope image shows perfect crack bridging mechanism; several of the CNTs were shown to act as crack arrestors across fine cracks along with some CNTs breakage.

• Magazine of the Korea Concrete Institute
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• v.11 no.2
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• pp.209-220
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• 1999

This paper is aimed to evaluate the effectiveness of flexural toughness of slab panel structures($60{\times}60{\times}10$) reinforced by steel fiber instead of wire mesh. Steel fiber used in this study is double hooked Dramix type fiber. And the fiber length is 60mm, diameter is 0.8mm, Various assessment methods of toughness index are used to estimate the proper effectiveness. In this experimental study, we find that Johnston, JCI-SF4 and EFNARC method are more effective to assess the flexural toughness of slab panels than the others. And the steel fiber is very effective alternative material to reinforce slab panel structures instead of wire mesh. Fiber volume fraction of 0.5~0.75% is more useful than the others in enhancing the post-peak energy absorption and toughness index by Johnston's $I_{5.5}$ assessment method. And the slab panels reinforcing with steel fiber are more resistant to crack propagation than wire mesh reinforcing slabs.

• Journal of the Korea institute for structural maintenance and inspection
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• v.19 no.4
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• pp.109-115
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• 2015

High performance fiber reinforced cementitious composite (HPFRCC) can provide high fracture energy absorption as well as high strength with high fiber volume fraction. The increased fracture energy helps resisting high frequency loadings, such as earthquake, impact or blast. This study investigates the flexural performance of slurry infiltrated fiber concrete (SIFCON), one of the important HPFRCC, with respect to varying fiber volume fraction. The maximum fiber volume fraction was 8.0 % and reduced to 6.0% by 0.5% and the maximum volume fraction is obtained by packing fibers with simple tapping by hands. The used fiber was a steel fiber with the length 30 mm and the diameter of 0.5 mm. The flexural strengths were 48.7 MPa at 8.0 % and 22.8 MPa at 6.0 %. The measured flexural strength is much higher compared to other cememtitious composite materials but decreased proportional to the fractions. This result implies that for SIFCON considered herein the reduced amount of steel fibers may affect its flexural performance in a negatively way. The flexural toughness, an index to represent the fracture energy absorption, also decreased with the reduced fiber amount.

• Proceedings of the Korea Concrete Institute Conference
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• 2003.11a
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• pp.629-634
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• 2003

The cement-based composites have relatively low tensile strength and toughness. The fiber addition is one of the most important ways of increasing the toughness of concrete. The steel fibers have been used conventionally in the shotcrete of tunnel lining. Recently, the structural synthetic fibers were developed and used frequently in some actual tunnel shotcreting in foreign countries. There are so many method to evaluate a toughness; ASTM, JCI, EFNARC, etc. But these methods contain a few defects. So most researchers are studying to develope a new toughness evaluation method. A RTA is one of these methods. The purpose of this study is to explore the strength and toughness characteristic of the fiber reinforced concrete panel according to the geometry; diameter, thickness. The result were compared with those of steel fiber reinforced concrete.