• 한국재료학회:학술대회논문집
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• 한국재료학회 2002년도 추계학술발표강연 및 논문개요집
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• pp.176-176
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• 2002

• 한국재료학회:학술대회논문집
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• 한국재료학회 2002년도 추계학술발표강연 및 논문개요집
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• pp.180-180
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• 2002

• 한국전기전자재료학회논문지
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• 제15권1호
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• pp.46-55
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• 2002

10mo1% Gd$_2$O$_3$ doped CeO$_2$ fine powders were synthesized by the oxalate coprecipitation method. The characteristics and sintering behavior of fine powders were investigated. The oxalate precipitates had the specific surface area of 150$m^2$/g, and appeared to be fine and spherical primary particles with a size of approximately 5.5nm. The decomposition of the precipitates occurred from a temperature around 30$0^{\circ}C$ and it was completed below 40$0^{\circ}C$, resulted in the formation of the oxide. The calcination temperature of the fine powders was suitable at 77$0^{\circ}C$. By introducing fine powders washed with alcohol and ball-milling process after calcination, the sintered body was possible to attain the value of 97% of the theoretical density at low temperature of 130$0^{\circ}C$

• 한국세라믹학회지
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• 제44권12호
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• pp.690-695
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• 2007

Scandia stabilized zirconia (ScSZ) is adapted for electrolyte material of solid oxide fuel cell (SOFC) because of its high ionic conductivity and chemical stability. ScMnSZ1 powder having a composition of $((ZrO_2)_{0.89}(Sc_2O_3)_{0.1}(MnO_2)_{0.01})$ is synthesized by ultrasonic spray pyrolysis (USP) method. Porous ScMnSZ1 powder is obtained by using a pore forming agent. Microstructure and morphology, particle size distribution of porous powder synthesized with 3wt% pore forming agent are investigated. Sintered ScMnSZ1 sample with ground fine powder are also investigated their microstructure and electrical conductivity. The electrical conductivity of sintered ScMnSZ1 samples with ground fine powder was 0.082 S/cm, 0.127 S/cm and 0.249 S/cm at $750^{\circ}C$, $800^{\circ}C$ and $900^{\circ}C$, respectively.

• 한국세라믹학회지
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• 제13권1호
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• pp.25-29
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• 1976

The properties vary with quality of ferric-oxide that is major material of ferrites. In this point of view, a manufacturing method of pure and homogeneous fine ferric oxide is very important. The characters of this study are as follows: 1) Ferric oxide was made from waste pickling liquor of steel. 2) The crude ferric-oxide that is made by roasting the pickling liquor was dissolved in 20% HCI solution and then produced ferric chloride is purified by ethyl ether extraction. 3) The methanol solution of purified ferric chloride was sprayed into the refractory tube with compressed air and propane gas and then ignited leading to the ferric-oxide powder. 4) The produced oxide powder was introduced to the scrubber type vessel throught cooling system in order to collect the powder. 5) Crystalline phase of the powder was identified by X-ray diffraction and particle size, crystalline shape of the powder were investigated by settling method and electron microscope and the effects of concentration of ferric chloride in methanol on grain size were discussed. Results were obtained as fellows: 1) Total impurity in the ferric oxide produced from waste pickling liquor was 3.7%. 2) The solubilityof crude ferric oxide that was made from waste pickling liquor in HCI solution increased with the HCI concentration and reached to saturation range at 15% HCI concentration. 3) Extraction of FeCl3 increased with HCI concentration which is solvent. 4) Alpha ferric oxide obtained was very fine crystalline particles, the mean crystalline grain increased with the concentration of ferric chloride, and mean grain size distributed from 3.5$\mu$(at 0.5mole/l) to 0.5$\mu$(at 0.05mole/l).

• 한국분말재료학회지
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• 제22권4호
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• pp.266-270
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• 2015

The synthesis of NiTi alloy powders by hydrogen reduction and dehydrogenation process of NiO and $TiH_2$ powder mixtures is investigated. Mixtures of NiO and $TiH_2$ powders are prepared by simple mixing for 1 h or ball milling for 24 h. Simple-mixed mixture shows that fine NiO particles are homogeneously coated on the surface of $TiH_2$ powders, whereas ball milled one exhibits the morphology with mixing of fine NiO and $TiH_2$ particles. Thermogravimetric analysis in hydrogen atmosphere reveals that the NiO and $TiH_2$ phase are changed to metallic Ni and Ti in the temperature range of 260 to $290^{\circ}C$ and 553 to $639^{\circ}C$, respectively. In the simple-mixed powders by heat-up to $700^{\circ}C$, agglomerates with solid particles and solidified liquid phase are observed, and the size of agglomerates is increased at $1000^{\circ}C$. From the XRD analysis, the presence of liquid phase is explained by the formation and melting of $NiTi_2$ inter-metallic compound due to an exothermic reaction between Ni and Ti. The simple-mixed powders, heated to $1000^{\circ}C$, lead to the formation of NiTi phase but additional Ni-, Ti-rich and Ti-oxide phases. In contrast, the microstructure of ball-milled powders is characterized by the neck-grown particles, forming $Ni_3Ti$, Ti-oxide and unreacted Ni phase.

• 한국조리학회지
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• 제18권3호
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• pp.191-205
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• 2012

식생활이 다양화되고 편의화 됨에 따라 쌀 소비량은 지속적인 감소 추세를 보이고 있다. 국내의 쌀 소비를 촉진시키고 쌀 수급 불균형을 해소하기 위해서는 주식으로서의 쌀 외에 쌀 가공식품 개발이 필요하다. 그 중에서 술을 이용한 쌀 소비는 다른 쌀 가공식품에 비해 높은 부가가치성을 지니므로 더욱 주목된다. 본 연구는 쌀 품종과 입도의 가공특성을 달리하여 탁주를 제조한 다음 품온, 당도, 알코올 함량, 산도, 아미노산가, pH, 색도 및 관능 등의 품질특성을 살펴본 것이다. 먼저 안다, 하이아미, 추청 세 품종의 쌀가루를 이용하여 무증자법으로 탁주를 제조한 다음 입도별 품질특성을 비교하였다. 모든 탁주 술덧의 품온은 담금 2일 후 최고 온도에 도달하였다. 품종에 따른 차이는 산도와 관능 평가에서만 나타났다. 산도의 경우 안다, 추청, 하이아미 순으로 높게 나타났고, 관능 평가는 추청이 가장 높게 나타났다. 입도별로는 알코올 함량과 산도는 중분쇄 쌀가루 탁주에서 높게 나타났고 담금 직후의 품온, 당도, 아미노산가, pH, 색도, 관능은 초미세 쌀가루 탁주에서 더 높게 나타났다. 본 연구의 결과 쌀 품종과 입도를 달리하여 제조한 무증자 탁주는 추청 초미세 쌀가루로 담그는 것이 효율적인 것으로 판단된다.

• 자원리싸이클링
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• 제18권1호
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• pp.38-43
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• 2009

본 고에서는 현행 고순도 폴리실리콘 제조공정에서 부산물로 발생하고 있는 실리콘 미세분말을 경제적인 가격에 태양전지급 원료로 재이용하고자 실리콘 미세분말의 무점결제 성형공정에 대한 연구를 수행하였다. 폴리실리콘 미세분말의 평균 크기는 $7.8{\mu}m$였으며, 주요 불순물은 표면 산화물과 수분이었다. 표면 산화물을 제거하기 위한 HF수용액-에탄올 혼합용액을 이용한 전처리공정을 행함으로써 폴리실리콘 분말의 성형성 그리고 성형체의 밀도 및 강도를 향상시킬 수 있었다. 진공 중에서 성형하는 경우 성형체 회수율이 20%증가하였다. 폴리실리콘 미세 분말은 공정 부산물 상태에서는 태양전지용 원료로 사용되기에 적합한 순도가 아니었지만, 건식 열처리를 행함으로써 태양전지급 이상의 순도를 확보할 수 있었다.

• Geomechanics and Engineering
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• 제28권6호
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• pp.547-557
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• 2022

Dune sands are poorly graded collapsible soils lacking fines. This experimental study explored the technical feasibility of sustainable invigoration of fine waste materials to improve the geotechnical properties of dune sand. The fine waste considered in this study is fine marble waste. The fine waste powder was mixed with dune sand at different contents (5, 10,15, 20, 25, 50%), where the gradation, void ratio, compaction, and shear strength characteristics were assessed for each fine marble waste -dune sand blend. The geotechnical properties of the dune sand-fine marble waste mix delineated in this study reveal the enhancement in compaction and gradation characteristics of dune sand. According to the results, the binary mixture of dune sand with 20% of fine marble waste gives the highest maximum dry density and results in shear strength improvement. In addition, a numerical study is conducted for the practical application of the binary mix in the field and tested for an isolated shallow foundation. The elemental analysis of the fine marble waste confirms that the material is non-contaminated and can be employed for engineering applications. Furthermore, the numerical study elucidated that the shallow surface replacement of the site with the dune sand mixed with 20% fine marble waste gives optimal performance in terms of stress generation and settlement behavior of an isolated footing. For a sustainable mechanical performance of the fine marble waste mixed sand, an optimum dose of 20% fine marble waste is recommended, and some correlations are proposed. Thus, for improving dune sand's geotechnical characteristics, the addition of fine marble waste to the dune sand is an environment-friendly solution.

• 대한안전경영과학회지
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• 제24권4호
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• pp.117-124
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• 2022

This study collected powder extinguishers with 6-10 years of elapsed life from January 2012 to January 2017 in market, factory, and apartment areas to experiment with changes in fineness and to examine the characteristics of extinguishing power. First, in the case of ABC powder, 98.3 wt% of the 8-year market area and 98.6 wt% of the 10-year apartment complex were found to be inappropriate in the first, second, and third arithmetic average analysis of the powder extinguisher from 6 to 10 years. That is, the fine distribution and size of the powder extinguishing agent particles should be managed within an appropriate range. It is analyzed that the powder fire extinguisher may experience a change in the fineness of the powder depending on the external environment exposure, placement, management status, and age of use, resulting in a decrease in digestive power or inability to radiate. Second, the fire extinguisher cannot be used in the initial fire suppression depending on the place of deployment, the environment of deployment, the progress of the number of years of use, and maintenance, so it is necessary to strengthen the device that enables fire extinguisher maintenance and inspection. Third, in the manufacturing process, the charging method should also be reviewed in consideration of the conditions of the workplace, the humid season, and the rainy environment.