• 제목/요약/키워드: Fine microstructure

검색결과 737건 처리시간 0.032초

규산질미분말혼합시멘트계도포방수재료가 습윤환경하의 콘크리트의 미세조직에 미치는 영향 (Effect of Siliceous Slury Coating on Microstructure of Concrete under Damp Environment)

  • 오상근
    • 한국콘크리트학회:학술대회논문집
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    • 한국콘크리트학회 1992년도 가을 학술발표회 논문집
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    • pp.1-4
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    • 1992
  • This paper deals with the effect of siliceous slurry coating on concrete microstructure under damp environment. This material is mixed inorganic powder consisted of silica, cement and fine sand and water. Water pressure was given on the coated surface of concrete. for estimation on effect of siliceous slurry coating, microstructure of coated concrete was observed through SEM, and chemical components of crystals were analyzed with X-ray diffraction and EDX. A number of needle and fibrous crystals were produced in microstructure. And based on X-ray diffraction and EDX, needle crystal mainly consist of Al, Si, and Ca, and it is concluded to be ettringite. Fibrous crystals consist of Ca and Si, and it to be calcium silicate hydrate.

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The Effect of La-silicon Oxynitride on the Densification of ${Si_3}{N_4}$ Ceramics by Spark Plasma Sintering

  • Cho, Kyeong-Sik;Kim, Sungjin;Beak, Sung-Ho;Park, Heon-Jin;Lee, June-Gunn
    • 한국세라믹학회지
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    • 제38권8호
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    • pp.687-692
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    • 2001
  • Silicon nitride-La-silicon oxynitride ceramics were fabricated by Spark Plasma Sintering (SPS). The density, crystalline phase and microstructure were compared with those obtained by Hot Pressing (HP). The full density was achieved within 40 min by spark plasma sintering at 1$650^{\circ}C$, whereas the same result was required by hot pressing with a dwell time of 500 min at higher temperature. There were some differences in the microstructure and second phases in the sintered ceramics, which are attributed to the rapid densification in the spark plasma sintering. The fine and acicular grain microstructure appeared in spark plasma sintering.

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급냉응고 AI-20Si-5Fe-2Ni 합금의 조직, 경도 및 마모특성에 관한 연구 (A Study on the characteristics of microstructure, hardness and wear of rapidly solidified AI-20Si-5Fe-2Ni materials)

  • 이상용;이정환;이영선;신평우
    • 한국소성가공학회:학술대회논문집
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    • 한국소성가공학회 1996년도 추계학술대회논문집
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    • pp.157-165
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    • 1996
  • Characteristics of microstructure, hardness and wear of two AI-20Si-5Fe-2Ni materials produced by powder metallurgy and spray forming respectively were studied at temperatures up to 560$^{\circ}C$. Above 300$^{\circ}C$, the microstructure of powder processed alloy became inhomogenous, whereas the spray formed alloy showed homogeneous microstructures. Hardness of both alloys was increased between 300$^{\circ}C$~490$^{\circ}C$ in both alloy. It was interpreted that increase in hardness was mainly related to the formation of stable and fine intermetallic phase from metastable one. It was showed that hoogenity of microstructure in the rapidliy soldified affected directly wear property.

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콘크리트 기공 솔루션에서의 열간 압연 및 열 기계 처리 철근의 부식 특성 (Corrosion Characteristics of hot rolled and thermo-mechanically treated steel rebar in concrete pore solution)

  • 이한승;싱 지텐드라 쿠마르
    • 한국건축시공학회:학술대회논문집
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    • 한국건축시공학회 2018년도 춘계 학술논문 발표대회
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    • pp.202-203
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    • 2018
  • Chemistry and microstructure of steel reinforcement bars play an important role to control the corrosion in concrete environments. In present study, we have chosen two different microstructure of steel rebars produced from companies and assessed their corrosion characteristics in simulated concrete pore (SCP) solution with prolonged exposure periods. Hot rolled steel rebar showed more corrosion resistance compare to thermo-mechanically treated (TMT) one. The growth of passive is greater in hot rolled (A) than TMT (B) due to orientation of microstructure. TMT steel rebar exhibit distorted microstructure with many micro cells which enhances the galvanic coupling and induce the deterioration while on the other hand hot rolled rebars exhibit fine grain boundary which responsible in growth of uniform, adherent and protective passive film resultant improved impedance was observed.

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Effects of Sintering Additives on the Microstructure Development in Silicon Oxynitride Ceramics

  • Kim, Joosun;Chen, I-Wei
    • The Korean Journal of Ceramics
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    • 제6권3호
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    • pp.224-228
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    • 2000
  • Using a small amount of additives and amorphous Si₂N₂O powders, O-SiAlON ceramics have been hot-pressed and its microstructure and mechanical properties were investigated. Scandium oxide was demonstrated to be an effective densification additive for O-SiAlON. Amorphous Si₂N₂O was densified at relatively low temperatures and a microstructure with acicular grains was developed. Fine grains found in materials obtained from amorphous powders suggest that nucleation and crystallization of O-SiAlOH is relatively easy compared with the Si₃N₄-SiO₂reaction.

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고강도-고인성 라인파이프강 개발 동향 (Developing Trend of High Strength and Good Toughness Linepipe Steel)

  • 유장용;강기봉
    • 대한기계학회:학술대회논문집
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    • 대한기계학회 2004년도 춘계학술대회
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    • pp.216-221
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    • 2004
  • Linepipe steels with a low carbon acicular ferrite microstructure have been recently developed to accommodate the current transportation condition of the gas and oil industry, and they are finally applied to West- East pipeline project in China. By adopting acicular microstructure, both better formability and better toughness could be obtained due to low yield ratio and fine grained microstructure. Mechanical properties of pipe are not greatly different from those of base plates or hot coils with a microstructure of acicular ferrite. Merits of introducing higher strength steels are well known, i.e., reducing the gauge of pipe and the material cost, increasing the welding speed and decreasing construction cost because of reducing the construction period. Threfore, gas and oil industry has required higher strength steel than APIX70 grade steel. Under this background, API-X80 steel has been developed and shall be applied to the several projects. In this paper, developing stage of API-X80 steel is also presented and discussed.

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Hybrid Microstructure and Mechanical Properties of HRS Processed SUS316L and Titanium Materials

  • Fujiwara, Hiroshi;Ohta, Koichi;Noro, Atsushi;Ameyama, Kei
    • 한국분말야금학회:학술대회논문집
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    • 한국분말야금학회 2006년도 Extended Abstracts of 2006 POWDER METALLURGY World Congress Part 1
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    • pp.540-541
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    • 2006
  • SUS316L stainless steel, commercial pure Titanium and Ti-6Al-4V alloy powders applied by Mechanical Milling (MM) process are sintered by Hot Roll Sintering (HRS) process. Microstructure and mechanical properties of those HRS materials is investigated. The microstructures of materials produced by HRS process consist of fine grains and work-hardened structure, that is, the hybrid microstructure. Tensile test of the HRS material demonstrated the good mechanical properties. These results show that the HRS process is very effective to the improvement of mechanical properties in the SUS316L stainless steel, commercial pure Titanium and Ti-6Al-4V alloy.

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Austempered Ductile Iron(A.D.I.)의 기계적 성질과 현미경 조직검사 (Mechanical Properties and Microstructure Examinations on Austempered Ductile Irons)

  • 이승석
    • 열처리공학회지
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    • 제3권1호
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    • pp.25-33
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    • 1990
  • Recently developed austempered ductile irons(A.D.I.) have good mechanical properties. However it is still needed to examine the relationships between microstructures related to banitic reaction and the mechanical properties. From the mechanical tests such as impact test, hardness test, tensile test, and the microstructure observations, we concluded that the good mechanical properties of A.D.I. came from the fine banitic ferrite structure formed during the first stage of the austempering reaction.

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급속응고한 Al-Mg 합금의 미세조직 및 인장특성에 미치는 첨가원소의 영향 (Effects of Alloying Elements on the Microstructure and Tensile Properties of Rapidly Solidified Al-Mg Alloys)

  • 박현호;박종성;김명호
    • 한국주조공학회지
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    • 제17권4호
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    • pp.356-364
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    • 1997
  • In order to study effects of Cu and Be on the microstructure and tensile properties of rapidly solidified Al-Mg alloys, Al-Mg-Cu-Be alloys have been rapidly solidified by inert gas atomization process. Microstructure of rapidly solidified Al-Mg-Cu-Be powders exhibited refinement and good dispersion of Be particles as increasing of solidification rate. Solidification rate of atomized powders was estimated to be about $5{\times}10^{3{\circ}}C/s$. Inert gas atomized Al-Mg-Cu-Be powders were hot-processed by vacuum hot pressing at $450^{\circ}C$ under 100 MPa and hot extruded with reduction ratio in area of 25: 1 at $450^{\circ}C$. The extruded Al-Mg-Cu-Be powders consisted of recrystallized fine Al grains and homogeneously dispersed fine Be particles, and exhibited improved tensile properties with increase in Cu content. $Al_2CuMg$ compounds precipitated in grain and grain boundaries of Al-Mg-Cu-Be alloys with aging heat treatment after solution treatment. Hardness and tensile properties were improved by increasing Cu content and Be addition. Compared with extruded Al-Mg-Cu powders, the extruded Al-Mg-Cu-Be powders exhibited finer recrystallized grains and improved tensile properties by dispersion hardening of Be and subgrain boundaries pinned by fine Be particles. After aging treatment, hardness and tensile properties were improved due to restricted precipitation by increasing of dislocation density around Be particles in matrix.

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Ferromagnetic Resonance Studies of Ultrathin Co Layers in Co/Ag Multilayers

  • Dubowik, J.
    • Journal of Magnetics
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    • 제4권3호
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    • pp.92-97
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    • 1999
  • A relationship between microstructure and ferromagnetic resonance of Co/Ag multilayers has been studied in as-deposited and annealed multilayers iwth ultrathin (dCo < 1 nm) Co layers. Depending on the nominal thickness of Co Co/Ag multilayers represent a system of fine magnetic particles (dCo < 0.4 nm) or discontionuous layered structure (dCo/0.5 nm). FMR data has been interpreted in the framework of a odel of interacting fine particles exhibiting superparamagnetic behavior. Changes in the FMR spectra upon annealing have been attributed to the growth of the Co particles and to a transition from the fcc to hcp atomic structure of the highly (111) textured Co particles.

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