• Korean Journal of Materials Research
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• v.34 no.3
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• pp.138-143
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• 2024

Ni-CNT nanocomposites were synthesized via the electrical explosion of wire (EEW) in acetone and deionized (DI) water liquid conditions with different CNT compositions. The change in the shape and properties of the Ni-CNT nanopowders were determined based on the type of fluids and CNT compositions. In every case, the Ni nanopowder had a spherical shape and the CNT powder had a tube shape. However, the Ni-CNT nanopowders obtained in DI water exhibited irregular shapes due to the oxidation of Ni. Phase analysis also revealed the existence of nickel oxide when using DI water, as well as some unknown peaks with acetone, which may form due to the metastable phase of Ni. Magnetic properties were investigated using a Vibrating Sample Magnetometer (VSM) for all cases. Nanopowders prepared in DI water conditions had better magnetic properties than those in acetone, as evidenced by the simultaneous formation of super paramagnetic NiO peaks and ferromagnetic Ni peaks. The DI water (Ni:CNT = 1:0.3) sample revealed better magnetic results than the DI water (Ni-CNT = 1:0.5) because it had less CNT contents.

• Transactions of the Korean Society of Pressure Vessels and Piping
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• v.12 no.1
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• pp.93-100
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• 2016

Since the sodium-cooled fast reactor is operated in a hostile environment due to the use of liquid sodium as its coolant, advanced techniques for in-service inspection are required to periodically verify the integrity of the reactor. This paper presents the development of in-service inspection techniques for Proto-type Generation IV Sodium-cooled Fast Reactor. First, the 10 m long plate-type ultrasonic waveguide sensor has been developed for in-service inspection of reactor internals, and its feasibility was verified through several under-water and under-sodium experiments. Second, the combined inspection system for in-service inspection of ferromagnetic steam generator tubes has been developed. The remote field eddy current testing and magnetic flux leakage testing can be conducted simultaneously by using the developed inspection system, and the detectability was demonstrated through several damage detection experiments. Finally, the electro-magnetic acoustic transducer which can withstand high temperature and be installable in the remote operated vehicle has been developed for in-service inspection of the reactor vessel, and its detectability was investigated through damage detection experiments.