• 제목/요약/키워드: Fe-based powder

검색결과 232건 처리시간 0.027초

Blended Elemental P/M Synthesis of Titanium Alloys and Titanium Alloy-based Particulate Composites

  • Hagiwara, Masuo;Emura, Satoshi
    • 한국분말야금학회:학술대회논문집
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    • 한국분말야금학회 2006년도 Extended Abstracts of 2006 POWDER METALLURGY World Congress Part2
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    • pp.1030-1031
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    • 2006
  • Titanium alloys and Titanium alloy-based particulate composites were synthesized using the blended elemental P/M route. First, processing conditions such as the fabrication of master alloy powder were investigated. Ti-6Al-4V, Ti-5Al-2.5Fe, Ti-6Al-2Sn-4Zr-2Mo, IMI685, IMI829, Timetal 1100 and Timetal 62S, and Ti-6Al-2Sn-4Zr-2Mo/ 10%TiB and Timetal 62S/10%TiB were then synthesized using the optimal processing conditions obtained. The microstructures and mechanical properties such as tensile strength and high cycle fatigue strength were evaluated.

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순수 타이타늄 기반 산화물분산강화 합금의 미세조직 및 기계적 특성 (Microstructure and Mechanical Properties of Oxide Dispersion Strengthened alloy Based on Commercially Pure Titanium)

  • 박태성;김정한
    • 한국분말재료학회지
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    • 제25권4호
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    • pp.327-330
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    • 2018
  • This study is conducted as a preliminary research to verify the feasibility of Ti-based Oxide dispersion strengthened (ODS) alloy. Pure-Ti powder is mixed with $Y_2O_3$ powder and subsequently, mechanically alloyed at $-150^{\circ}C$. The Ti-based ODS powder is hot-isostatically pressed and subsequently hot-rolled for recrystallization. The microstructure consists of elongated grains and Y excess fine particles. The oxide particle size is larger than that of the typical Fe-based ODS steel. Tensile test shows that the tensile ductility is approximately 25%, while the strength is significantly higher than that of pure Ti. The high-temperature hardness of the Ti-ODS alloy is also significantly higher than that of pure Ti at all temperatures, while being lower than that of Ti-6Al-4V. The dimple structure is well developed, and no evidence of cleavage fracture surface is observed in the fracture surface of the tensile specimen.

Friction and Wear Properties of Cu and Fe-based P/M Bearing Materials

  • Tufekci Kenan;Kurbanoglu Cahit;Durak Ertugrul;Tunay R. Fatih
    • Journal of Mechanical Science and Technology
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    • 제20권4호
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    • pp.513-521
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    • 2006
  • The performances of porous bearings under different operating conditions were experimentally investigated in this study. Material groups studied are 90%Cu + 10%Sn bronze and 1%C + % balance Fe iron-based self-lubricating P/M bearings at constant (85%) density. In the experiments, the variation of the coefficient of friction and wear ratio of those two different group materials for different sliding speeds, loads, and temperatures were investigated. As a result, the variation of the friction coefficient-temperature for both constant load, and constant sliding speed, friction coefficient-average bearing pressure, PV-wear loss and temperature-wear loss curves were plotted and compared with each other for two materials, separately. The test results showed that Cu-based bearings have better friction and wear properties than Fe-based bearings.

기계적 합금화하여 제조한 Fe-5Y2O3 합금분말의 나노산화물 석출거동 (A Precipitation Behavior of Nano-Oxide Particles in Mechanically Alloyed Fe-5Y2O3 Powders)

  • 김가언;노상훈;최지은;김영도;김태규
    • 한국분말재료학회지
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    • 제22권1호
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    • pp.46-51
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    • 2015
  • A precipitation behavior of nano-oxide particle in Fe-$5Y_2O_3$ alloy powders is studied. The mechanically alloyed Fe-$5Y_2O_3$ powders are pressed at $750^{\circ}C$ for 1h, $850^{\circ}C$ for 1h and $1150^{\circ}C$ for 1h, respectively. The results of Xray diffraction pattern analysis indicate that the $Y_2O_3$ diffraction peak disappear after mechanically alloying process, but $Y_2O_3$ and $YFe_2O_4$ complex oxide precipitates peak are observed in the powders pressed at $1150^{\circ}C$. The differential scanning calorimetry study results reveal that the formation of precipitates occur at around $1054^{\circ}C$. Based on the transmission electron microscopy analysis result, the oxide particles with a composition of Y-Fe-O are found in the Fe-$5Y_2O_3$ alloy powders pressed at 1150oC. It is thus conclude that the mechanically alloyed Fe-$5Y_2O_3$ powders have no precipitates and the oxide particles in the powders are formed by a high temperature heat-treatment.

Fe-Cr-Al 기 산화물 분산강화 합금의 미세조직에 미치는 분말제조 공정 영향 (Effect of Powder Synthesis Method on the Microstructure of Oxide Dispersion Strengthened Fe-Cr-Al Based Alloys)

  • 박성현;오승탁
    • 한국재료학회지
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    • 제27권9호
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    • pp.507-511
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    • 2017
  • An optimum route to fabricate oxide dispersion strengthened ferritic superalloy with desired microstructure was investigated. Two methods of high energy ball milling or polymeric additive solution route for developing a uniform dispersion of $Y_2O_3$ particles in Fe-Cr-Al-Ti alloy powders were compared on the basis of the resulting microstructures. Microstructural observation revealed that the crystalline size of Fe decreased with increases in milling time, to values of about 15-20 nm, and that an FeCr alloy phase was formed. SEM and TEM analyses of the alloy powders fabricated by solution route using yttrium nitrate and polyvinyl alcohol showed that the nano-sized Y-oxide particles were well distributed in the Fe based alloy powders. The prepared powders were sintered at 1000 and $1100^{\circ}C$ for 30 min in vacuum. The sintered specimen with heat treatment before spark plasma sintering at $1100^{\circ}C$ showed a more homogeneous microstructure. In the case of sintering at $1100^{\circ}C$, the alloys exhibited densified microstructure and the formation of large reaction phases due to oxidation of Al.

고압 가스 분무법을 이용한 Fe-Hf-B-Nb-P-C 연자성 분말 제조 및 특성 평가 (Investigation on Fe-Hf-B-Nb-P-C Soft Magnetic Powders Prepared by High-Pressure Gas Atomization)

  • 정재원;양동열;김기봉;이준홍;김영자;임태수;양상선;이민하;김휘준;김용진
    • 한국분말재료학회지
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    • 제23권5호
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    • pp.391-396
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    • 2016
  • In this study, ultra-fine soft-magnetic micro-powders are prepared by high-pressure gas atomization of an Fe-based alloy, Fe-Hf-B-Nb-P-C. Spherical powders are successfully obtained by disintegration of the alloy melts under high-pressure He or $N_2$ gas. The mean particle diameter of the obtained powders is $25.7{\mu}m$ and $42.1{\mu}m$ for He and $N_2$ gas, respectively. Their crystallographic structure is confirmed to be amorphous throughout the interior when the particle diameter is less than $45{\mu}m$. The prepared powders show excellent soft magnetic properties with a saturation magnetization of 164.5 emu/g and a coercivity of 9.0 Oe. Finally, a toroidal core is fabricated for measuring the magnetic permeability, and a ${\mu}_r$ of up to 78.5 is obtained. It is strongly believed that soft magnetic powders prepared by gas atomization will be beneficial in the fabrication of high-performance devices, including inductors and motors.

압흔하중식에 의한 금속소결분말체내에서의 밀도분포 예측 (Prediction of Density Distribution in Sintered Metal Powder Compacts by Indentation Force Equation)

  • 박종진
    • 한국분말재료학회지
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    • 제4권3호
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    • pp.188-195
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    • 1997
  • In most of sintered metal powder compacts, the sintered density distribution is controlled to be as high and uniform as possible to ensure the required mechanical properties. In general, the density distribution in the compacts is not uniform and not easy to measure. In the present study, a method for measuring the density distribution was developed, based on the indentation force equation by which the hardness and the relative density were related. The indentation force equation, expressed as a function of strength constant, workhardening coefficient and relative density, was obtained by finite element analysis of rigid-ball indentation on sintered powder metal compacts. The present method was verified by comparing the predicted density distribution in the sintered Fe-0.5%C-2%Cu compacts with that obtained by experiments, in which the density distribution was directly measured by machining the compacts from the outer surface progressively.

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천년초 열매 분말을 첨가하여 제조한 생면의 품질특성과 저장성 (Quality Characteristics and Storage Properties of Wet Noodle with Added Cheonnyuncho Fruit Powder)

  • 정복미
    • 한국식품조리과학회지
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    • 제26권6호
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    • pp.821-830
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    • 2010
  • This study was carried out to investigate the quality characteristics and storage of wet noodle with added Cheonnyuncho powder. Wet noodles were prepared at concentration of 1, 3, and 5%(w/w) of the fruit based on flour weight. Moisture content of the noodles with or without Cheonnyuncho powder was 34~36%. Ca, K, Mg, Fe, Mn and Zn contents of Cheonnyuncho noodle were increased at increasing concentrations of Cheonnyuncho powder. Cooked weight, volume, and water absorption decreased with increased fruit powder, whereas turbidity increased. For hunter's color values of noodles, L(lightness) and b(yellowness) values decreased with increasing concentration of Cheonnyuncho powder, whereas a(redness) value increased. For mechanical characteristics of the noodles, adhesiveness, cohesiveness, chewiness, elasticity, and brittleness of cooked noodle with Cheonnyuncho powder were lower than those of control. The pH of Cheonnyuncho noodle was lower than that of control during storage. Bacterial counts of wet noodle with 1% and 3% fruit powders were lower than those of the control and 5% fruit powder on the 8th day of storage at $5^{\circ}C$. From the sensory evaluation, texture, taste, and overall preference were not significantly different between the control and fruit group, but the color of 5% Cheonnyuncho noodle was significantly higher than that of control (p<0.05). In conclusion, the results of this study suggest that the addition of 1% and 3% Cheonnyuncho powder in combination with flour tended to improve antimicrobial effects during storage when compared to control.

PREPARATION AND PROPERTIES OF OIL-BASED MAGNETIC FLUIDS WITH THE SYNTHESIZED MAGNETITE

  • Jang, K.O.;Doh, S.W.;Cho, S.I.;Shon, H.J.;Hur, W.D.
    • 한국자기학회지
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    • 제5권5호
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    • pp.819-823
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    • 1995
  • The oil-based magnetic fluids were sysnthesized using ultra-fine $Fe_{3}O_{4}$ powder dispersed in hydrocarbon oil. To synthesize ultra-fine $Fe_{3}O_{4}$, we carried out the experiments varying the pH of reacting medium and the initial concentration of $Fe^{2+}$. We also investigated the amount of oleic acid to obtain a stable dispersion and the proper base oil of MF for loudspeaker application. The limits of adsorbed amount of oleic acid on the $Fe_{3}O_{4}$ surface were approximately 35~40 percents of the total magnetite weight. As the $Fe_{3}O_{4}$ content increased from 0.1g/cc to 0.6g/cc, the viscosity of oil-based magnetic fluid increased from 1,063cP to 1,828cP, and its saturation magnetization at 10kOe increased from 66G to 242G. When we tested the MF sample to a commercial speaker, improvements were noted.

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