• Proceedings of the Korean Society of Precision Engineering Conference
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• 2012.05a
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• pp.725-726
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• 2012

• Proceedings of the Korean Society for Technology of Plasticity Conference
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• 2008.10a
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• pp.66-70
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• 2008

In this study, the formability of AZ31B magnesium alloy sheets was investigated by the analytical and experimental approaches. Tensile tests and limit dome height tests were rallied out at several temperatures between $25^{\circ}C$ and $300^{\circ}C$ to obtain the mechanical properties and forming limit diagram (FLD). The FLD-based criterion considering the strain-path and the blank temperature was used to predict the forming limit in a deep-drawing process of cross-shaped cup by finite element analysis. This criterion proved to be very useful in determining the optimal process conditions such as blank shape, punch velocity, minimum comer radius, fillet size, and so on, through the comparison between FEA and experimental data. In particular, the temperature of each tool that provided the best formability of the blank was determined by coupled temperature-deformation analyses. A practical method that can greatly reduce the forming time by increasing the punch speed during the forming process was suggested.

• Transactions of Materials Processing
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• v.17 no.7
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• pp.501-506
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• 2008

In this study, a forming magnesium alloy circular cup was simulated accounting for heat transfer at elevated temperatures. In order to predict the failure of magnesium alloy sheet during simulation, the forming limit diagram, which is used in sheet metal forming analysis to determine the criterion for failure, was investigated. For the failure prediction in the simulation accounting for heat transfer, the forming limit diagram for a temperature the same as the temperature of the blank element was used. The result of the simulation showed that the drawn depth increases with the increase of the die-holder temperature, and is in accord with the experimental results above the die-holder temperature of $150^{\circ}C$. The forming limit diagram provided a good guide for the failure prediction of warm forming simulation accounting for heat transfer. In addition, the effect of the tool shoulder radius on the drawn depth at various tool temperatures is verified using the simulation conditions which agreed with the experimental results.

• Composites Research
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• v.13 no.2
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• pp.81-90
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• 2000

For automotive applications, a sandwich sheet which was made of a 5182 aluminum alloy (AA5182) sheet and a polypropylene (PP) sheet, AA5182/PP/AA5182, has been developed. In order to evaluate its formability, the forming limit diagrams (FLD) of the 5182 aluminum alloy sheet with 0.2mm thickness and the sandwich sheet with 1.2mm thickness have been obtained based on the modified Marciniak-Kuczynski (M-K) theory. To account for the anisotropy of the sheet, Hill's 1948 yield function has been applied. The FLD of the sandwich sheet was predicted to be better than that of the AA5182 sheet, which was well confirmed by experiments.

• Journal of Food Hygiene and Safety
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• v.23 no.1
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• pp.26-30
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• 2008

Polycyclic Aromatic Hydrocarbons(PAHs) contamination arises from several source including processing of food(smoking, direct drying, cooking) and environmental contamination of air, water or soil. A red ginseng is produced by steaming the root followed by drying. The methodology involved extraction with n-hexane and washing with water, clean-up on Sep-Pak Florisil Cartridges and determination by HPLC/FLD. The mobile phase was a mixture of acetonitrile and water in 8:2 by the isocratic elution and the excitation wavelength of fluorescence detector was 294 nm and its emission wavelength was 404 nm. The average recovery was about 105% and the relative standard deviation was 0.5. The levels of benzopyrene in the selected red ginseng beverage samples were not detected.

• Food Science and Biotechnology
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• v.18 no.4
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• pp.978-984
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• 2009

An analytical method for the simultaneous determination of 9 quinolones (QNs) in porcine, chicken, and bovine muscles was developed and validated using liquid chromatography-fluorescence detector (LC-FLD). The samples were extracted using a liquid-liquid extraction (LLE) process. Chromatographic separation was achieved on a reverse phase $C_8$ column with a gradient elution using a mobile phase of 200 mM ammonium acetate buffer (pH 4.5) and acetonitrile (ACN). The proposed method was validated according to the Food and Drug Administration (FDA) guideline for bioanalytical assay procedures. Recoveries of QNs were 83.1-111.9% with relative standard deviations (RSDs) below 15%. Linearity within a range of 30-500 ${\mu}g/kg$ was obtained with the correlation coefficient ($R^2$) of 0.9967-0.9999. The limits of detection (LOD) were 1-16 ${\mu}g/kg$. These values were lower than the maximum residues limits (MRLs) established by the European Union (EU). The present method was successfully applied to determine QNs in edible muscles.

• Journal of fish pathology
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• v.26 no.1
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• pp.45-50
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• 2013

Enrofloxacin is one of the normally used flouroquinolones in mammalian and fish but its withdrawal time and studies were remain obscure. The residual contents of enrofloxacin in fish muscle were analyzed by using HPLC-FLD. More than 0.1 mg/kg of ENR was detected in muscle tissues and the residues were found over 1 year after treatment. The concentration of ENR in Paralichthys olivaceus was not affected by water temperature and lasted for an extended amount of time. The spike recoveries of ENR in the muscle tissue ranged from 78% to 85%. From this results, we need the prescription by veterinarian or aquatic organism disease inspector in ENR usage to assure safety of fish. Future research is required to determine the recommendation dose of ENR for side effects and safety.

• Transactions of the Korean Society of Mechanical Engineers A
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• v.31 no.8
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• pp.833-838
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• 2007

In tube hydroforming process, several defective products could be obtained such as bursting, wrinkling, folding, buckling. Because, especially, bursting is most frequently occurred failure among the well known failures, it is mostly important to predict the onset of bursting failure on tube hydroforming process. For most sheet metal forming processes, strain based forming limit diagram(FLD) is used often as a criteria to estimate the possibility of onset of the failures proposed above. However, FLD has a shortcoming that it is dependent on strain path while stress based diagram is independent on strain history. Generally, tube hydroforming consists of three main processes such as pre-bending, pre-forming, and hydroforming and it means that the strain histories of final products are nonlinear. Therefore, forming limit stress diagram(FLSD) is more suitable to predict forming limit for hydroforming parts. In this study, FLSD is applied to estimate bursting failure for an engine cradle of an automobile part. Consequently, it is proved that application of FLSD to predict forming limit is available for tube hydroforming parts.

• Proceedings of the Korean Society for Technology of Plasticity Conference
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• 2005.05a
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• pp.92-96
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• 2005

Among the failure modes which can be occurred in tube hydroforming such as wrinkling, bursting or buckling, the bursting by local instability under excessive tensile stresses is irrecoverable phenomenon. Thus, the accurate prediction of bursting condition plays an important role in producing the successfully hydroformed part without any defects. As the classical forming limit criteria, strain-based forming limit diagram has widely used to predict the failure in sheet metal forming. However, it is known that the FLD is extremely dependant on strain path throughout the forming process. Furthermore, the path-dependent limitation of FLD makes the application to hydroforming process, where strain path is no longer linear throughout forming process, more careful. In this work, stress-based forming limit diagram (FLSD), which is strain path-independent and more general, was applied to prediction of forming limit in tube hydroforming. Combined with the analytical FLSD determined from plastic instability theory, finite element analyses were carried out to find out Ihe state of stresses during hydroforming operation, and then FLSD is utilized as forming limit criterion. In addition, the approach is verified with a series of bulge tests in view of bursting pressure and shows a good agreement. Consequently, it is shown that the approach proposed in this paper will provide a feasible method to satisfy the increasing practical demands for judging the farming severity in hydroforming processes.

• Proceedings of the Korean Society for Technology of Plasticity Conference
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• 2005.05a
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• pp.249-252
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• 2005

Recently, as the industrial demand for small quantity batch production of sheet metal components, the application of dieless forming technology to production of these component rise with the advantages of the reduction in manufacturing cost and time. In dieless forming processes, the determination of moving path of tool plays an important role in producing successfully formed parts. In order to obtain the optimized moving path of tool avoiding forming failure, it is necessary to examine the forming limit of sheet material. Therefore, in this study, as the new criterion to evaluate the formability of sheet material in dieless forming processes FDD(feeding depth diagram) with respect to feeding depth and punch diameter is proposed. Thus, the FDD for the sheet materials of STS304 and Ti-grade2 were obtained from a series of FDT(feeding depth test). In addition the possibility of the application of FLD in judging forming severity in dieless forming processes was investigated by comparing the results of FE analyses based on FLD and experimental FDT.