• Title/Summary/Keyword: FE technique

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다양한 조건에서의 $Ba_{1-x}K_xFe_2As_2$ 박막 제조 (Fabrication of $Ba_{1-x}K_xFe_2As_2$ Thin Films in Various Conditions)

  • 이남훈;정순길;강원남
    • Progress in Superconductivity
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    • 제12권1호
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    • pp.32-35
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    • 2010
  • Potassium doped $BaFe_2As_2$ superconducting thin films by using an ex situ pulsed laser deposition technique were fabricated in various conditions to find out an optimal growth condition. Controlled conditions were annealing temperature, annealing time, and mass of potassium. The $Ba_{1-x}K_xFe_2As_2$ thin films which has most good quality is fabricated at a condition of annealing temperature at $700^{\circ}C$, annealing time of 60 minutes, and 0.6 g of potassium lumps. In this condition we were able to fabricate good quality films with high transition temperature of ~ 39 K.

정전 마이크로 액츄에이터의 자동 CAE 평가 (Automated CAE Evaluation of Electrostatic Micro Actuator)

  • Lee, Joon-Seong
    • 한국정밀공학회:학술대회논문집
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    • 한국정밀공학회 1996년도 추계학술대회 논문집
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    • pp.711-715
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    • 1996
  • This paper describes an automated computer-aided engineering (CAE) system for micromachines whose size range 10 to 10$^3$${\mu}{\textrm}{m}$. An automatic finite element mesh generation technique, which is based on the fuzzy knowledge processing and computational geometry techniques, is incorporated into the system, together with one of commercial finite clement (FE) analysis codes, MARC, and one of commercial solid modelers, Designbase. The system allows a geometry model of concern to be a automatically converted to different FE models, depending on physical phenomena to be analyzed, i.e. electrostatic analysis, stress analysis, modal analysis and so on. The FE analysis models are then exported to the FE analysis code, and then analyses are performed. This system is successfully applied to an electrostatic micro actuator.

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X-선 회절법에 의한 철-질소 화합물층의 ε과 γ'상 분율 해석 (Fraction Analysis of ε and γ'-iron Nitride in Compound Layer Using X-ray Diffraction)

  • 김윤기
    • 한국재료학회지
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    • 제16권2호
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    • pp.85-91
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    • 2006
  • The fraction of $\varepsilon\;and\;\gamma$'-iron nitride in compound layer is predicted by x-ray diffraction using direct comparison method. The validity of formulation models was checked by comparing calculated results with metallographic analysis of iron nitride compound layer grown on steel S45C by gas nitriding. The fraction of $\varepsilon$ calculated by the three phase model, porous-$Fe_3N$/ dense-$Fe_3N$/ mixed layer with $Fe_3N\;and\;Fe_4N$, is 80 percent of that analyzed by etching technique. The $\varepsilon$ fraction predicted by mixed layer model is 122 percent of that measured by microscope.

금속 나노와이어의 제조와 특성 (Metal nano-wire fabrication and properties)

  • 보보무로드 함라쿠로프;김인수
    • 한국소성가공학회:학술대회논문집
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    • 한국소성가공학회 2009년도 춘계학술대회 논문집
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    • pp.432-434
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    • 2009
  • Metal nano-wire arrays on Cu-coated seed layers were fabricated by aqueous solution method using sulfate bath at room temperature. The seed layers were coated on Anodic aluminum oxide (AAO) bottom substrates by electrochemical deposition technique, length and diameter of metal nano-wires were dominated by controlling the deposition parameters, such as deposition potential and time, electrolyte temperature. Anodic aluminum oxide (AAO) was used as a template to prepare highly ordered Ni, Fe, Co and Cu multilayer magnetic nano-wire arrays. This template was fabricated with two-step anodizing method, using dissimilar solutions for Al anodizing. The pore of anodic aluminum oxide templates were perfectly hexagonal arranged pore domains. The ordered Ni, Fe, Co and Cu systems nano-wire arrays were characterized by Field Emission Scanning Electron Microscopy (FE-SEM) and Vibrating Sample Magnetometer (VSM). The ordered Ni, Fe, Co and Cu systems nano-wires had different preferred orientation. In addition, these nano-wires showed different magnetization properties under the electrodepositing conditions.

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마모입자 분석기술을 이용한 초음속 항공기 엔진의 상태 예측에 관한 연구 (A Study on the Prediction of Engine Condition of Supersonic Aircraft through the Wear Debris Monitoring Technique)

  • 정병학;정동윤
    • Tribology and Lubricants
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    • 제13권2호
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    • pp.82-88
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    • 1997
  • This paper describes an empirical equation which can be used to predict the engine condition of supersonic aircraft. The equation, which is derived from the trend analysis of JOAP data, represents the concentration of Fe particles in the engine oil. The result of the trend analysis shows that the concentration of Fe particles is a function of running time of engine oil. Meanwhile the slope of Fe concentration is a function of running time of engine. Threfore, the empirical equation was derived as $w=a(t_e).t_o+b$. However, the equation could not enough to diagnose the damaged part of engine quantitatively. To make up for the weak points of the equation, qualitative analysis was carried out. For that purpose wear debris were collected from the abnormal engine and analyzed by EDS to detect the damaged parts of engine.

Thermodynamic Properties of $NiFe_2O_4-NiFe_2O_4$ Spinel Solid Solution

  • 박봉훈;김동수
    • Bulletin of the Korean Chemical Society
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    • 제20권8호
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    • pp.939-942
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    • 1999
  • The tie lines delineating ion-exchange equilibria between NiFe2O4-NiCr2O4 spinel solid solution and Fe2O3-Cr2O3 corundum solid solution were determined at 900, 1000, and 1200 ℃ by electron microprobe and energy dispersive X-ray analysis of oxide phases, using the flux growth technique. Activities of the spinel components were calculated from the tie lines, assuming Temkin's ideal mixing in the corundum solid solution. The spinel phase could be expressed by a regular solution with negative deviations from ideality. The Gibbs free energies of mixing for spinel solid solution were discussed in terms of the cation distribution model, based on site preference energies and assuming random mixing on both tetrahedral and octahedral sites.

THE CONTROL OF PERMITTIVITY IN THE Ni-Zn FERRITE ABSORBER

  • Cho, S.B.;Oh, J.H.
    • 한국자기학회지
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    • 제5권5호
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    • pp.730-734
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    • 1995
  • The variation of magnetic permeability and dielectric constant and their relationship with microwave absorbing properties are investigated in sintered Ni-Zn ferrite. Toroid specimens of ${(Ni_{0.5}Zn_{0.5}O)}_{1-y}{(Fe_{2}O_{3})}_{1+y}$ ferrites are prepared by conventional ceramic processing technique. The large change in magnetic permeability is observed by the variation of excess $Fe_{2}O_{3}$ in the Ni-Zn ferrites. The more the iron-excess from y=0.04 to y=0.12, the lower value of both $\mu_{r}'$ and $\mu_{r}"$ is observed. However dielectric permittivity increases with the increase of the increase of the excess $Fe_{2}O_{3}$. The control of permittivity is realized by nitrogen sintering atmosphere and excess $Fe_{2}O_{3}$ respectively.

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Analysis of CRUD Flake Applied to Abnormal High Beam Current by Shielded-EPMA

  • Jung, Y.H.;Baik, S.J.;Ahn, S.B.
    • Corrosion Science and Technology
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    • 제17권6호
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    • pp.265-271
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    • 2018
  • CRUD specimens, scraped from twice-burned fuel cladding in the Korean Nuclear Power Plant, were analyzed using Shielded-EPMA. The principal elements of the CRUD were identified as Ni and Fe, at an approximate ratio of 1.3 Ni/Fe. To investigate the morphology and composition of the pure metallic materials in the CRUD, coolant impurities must be removed. This can be accomplished by increasing the EPMA current to an abnormally high intensity until the impurities are melted. Normally, EPMA applications are performed at conditions of 20 kV voltage and 20 nA current. But in our study, the applied current was increased up to 1200 nA, over time increments ranging from 5 to 30 seconds. This technique was performed by opening an adjustable aperture for the gun alignment. Results showed impurities contained in the CRUD material disappeared and pure metal materials, e.g., Ni and Fe, remained. This method presents an innovative way to analyze CRUD.

초전형 적외선 센서용 P(VDF/TrFE) 막의 분극에 따른 유전특성의 변화 (Dielectric characteristics with poling of P(VDF/TrFE) films for pyroelectric infrared sensor)

  • 권성렬;김영우;배승춘;박성근;김기완
    • 센서학회지
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    • 제9권1호
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    • pp.9-14
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    • 2000
  • 스핀 코팅 방법으로 제조된 P(VDF/TrFE) 막의 유전적 특성을 조사하였다. 막의 결정성과 막질을 개선하기 위해 스핀 코팅 후에 3 단계에 걸친 열처리 공정을 하였다. 상부전극을 마스크로 사용하는 간단한 P(VDF/TrFE) 막의 식각공정과 조건을 확립하였다. 분극을 여러 단계에 걸쳐 하는 정확한 분극공정을 실현하였다. 스핀코팅으로 제조된 막의 두께는 용액농도 10 wt%, 스핀속도 3000 rpm, 스핀시간 30초에서 $1.87\;{\mu}m$였다. 제조된 P(VDF/TrFE) 막의 유전상수와 유전손실을 측정하였다. 1 kHz의 주파수에서 분극전 P(VDF/TrFE) 막의 유전상수는 13.5, 유전 손실은 0.042로 나타났으며 분극후 각각 11.5, 0.037로 나타났다.

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A Form-finding Technique for Three-dimensional Spatial Structures

  • Lee, Sang Jin
    • Architectural research
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    • 제15권4호
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    • pp.207-214
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    • 2013
  • A form-finding technique is proposed for three-dimensional spatial structures. Two-step discrete finite element (FE) mesh generator based on computer aided geometric design (CAGD) is introduced and used to control the shape of three-dimensional spatial structures. Mathematical programming technique is adopted to search new forms (or shapes) of spatial structures. For this purpose, the strain energy is introduced as the objective function to be minimized and the initial volume (or the initial weight) is considered as constraint function. Numerical examples are carried out to test the capability of the proposed form-finding techniques and provided as benchmark tests.