• 제목/요약/키워드: FE experiment

검색결과 968건 처리시간 0.041초

재사용이 가능한 나노복합재료 Fe3O4-ACCS-Ag의 제조 및 항균 특성 평가 (Investigation of Synthesis and Antibacterial Properties of a Magnetically Reusable Fe3O4-ACCS-Ag Nanocomposite)

  • 심재홍;김해원;김진원;서영석;오세강;조민;박정희;오병택
    • 한국지하수토양환경학회지:지하수토양환경
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    • 제20권3호
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    • pp.25-33
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    • 2015
  • In this study, Fe3O4-ACCS-Ag nanoparticles (NPs) were successfully synthesized using silica extracted from corn cob ash. The synthesized Fe3O4-ACCS-Ag NPs were characterized using X-ray diffraction (XRD), scanning electron microscopyenergy dispersive X-ray spectroscopy (SEM-EDX), transmission electron microscopy (TEM) and fourier transform infrared spectroscopy (FTIR). In addition, the potential application of Fe3O4-ACCS-Ag NPs as an antibacterial material in water disinfection was investigated using Escherichia coli ATCC 8739 as model bacteria. The antibacterial activity of synthesized composite material showed 99.9% antibacterial effect within 20 min for the tested bacteria. From this experiment, the synthesized Fe3O4-ACCS-Ag nanocomposites also hold magnetic properties and could be easily recovered from the water solution for its reuse. The reused nanocomposites presented the decreasing antibacterial efficiencies with the reuse cycle but the composite used three times still killed 90% of bacteria in 20 min.

고사리 뿌리의 채취시기에 따른 전분 추출수율과 이화학적 특성 (Root Starch Yield and Physio-Chemical Characteristics of Bracken (Pteridium aquilinum Kuhn) according to Harvesting Time)

  • 문정섭;염규생;안송희;기세현;정동춘
    • 한국자원식물학회:학술대회논문집
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    • 한국자원식물학회 2020년도 추계국제학술대회
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    • pp.74-74
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    • 2020
  • 고사리(Pteridium aquilinum Kuhn)는 고사리 속(Pteridium spp.)에 속하는 양치식물의 총칭으로서 우리나라에는 22과 70속 272종이 분포되어 있는 것으로 보고되었다. 고사리의 어린 순에는 가식부 100g 당 칼슘 15.0mg, 칼륨 185.0mg 등이 함유되어 있으며 골다공증, 심혈관 질환 등에 효과가 있고 식이섬유로 인해 변비 예방에도 유용한 것으로 알려져 있다. 우리나라의 고사리 재배면적은 2019년 기준 5,349ha 수준을 보이고 있으며 전체 산채류 재배면적에서 26%의 비중을 차지하고 있으나 재배면적의 증가에 따라 고사리 재배의 부가가치를 높일수 있는 방안이 요구되고 있는 실정으로 그 중 고사리 뿌리에서 추출한 전분은 중국 및 일본 등지에서 면류나 제과용으로 이용되고 있어 고사리 재배의 부가가치를 향상시킬 수 있는 방안으로 기대되고 있다. 본 연구에서는 고사리 뿌리의 채취시기에 따른 뿌리 전분의 생산성과 이화학적 특성을 조사하기 위해 2020년 3월 26일부터 10월 28일 까지 5회에 걸쳐 뿌리를 수확하여 세척한 후 고무망치로 파쇄하고 수침 방법을 이용해 추출한 전분의 추출수율과 이화학적 특성을 조사하였다. 채취시기별 고사리 뿌리의 생산성은 7월 27일 수확에서 3,783.3kg/10a로 유의하게 높은 수량을 보였다. 파쇄한 고사리 뿌리를 24시간 sodium metabisulfite 0.4% V/W 용액에 수침하여 전분을 추출한 후 24시간 간격으로 3회에 걸쳐 진탕, 침전과 세척의 과정을 거친 후 조사한 전분 추출 수율은 3월 26일 수확한 뿌리에서 7.6%로 가장 높았고 7월 27일과 9월 24일 채취한 경우에서는 전분이 검출되지 않았으며 10월 28일에는 4.9%의 유의하게 낮았다. 추출한 전분의 색도분석에서 L값은 채취시기가 늦어질수록 높아지는 경향을 보였고 a, b값은 낮아지는 경향을 보여 전분의 색도가 향상되는 경향을 보였으며, 신속점도측정기로 조사한 전분의 호화특성에서는 채취시기가 늦어질수록 전분의 최고점도는 높아졌으나 최저점도 및 최종점도는 낮아지는 경향을 나타냈다. 전분의 무기물 함량은 3월 26일과 5월 25일 채취하는 경우 Fe > Ca > Mg > K > P의 순으로 함량이 높았으나 10월 28일 채취한 경우에서는 Fe와 Ca이 감소되고 K 함량은 증가하여 Ca > Fe > Mg > K > P의 순으로 무기물 함량이 높게 나타났다.

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유산균과 효모균 배양액 함유 액비 시용이 크리핑 벤트그래스의 생육에 미치는 영향 (Effect of Liquid Fertilizer Contained Medium of Lactobacillus sp. and Saccharomyces sp. on Growth of Creeping Bentgrass)

  • 김영선;함선규;이상진
    • 아시안잔디학회지
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    • 제24권2호
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    • pp.138-144
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    • 2010
  • 본연구는효모균(Saccharomyces sp.)과유산균(Lactobacillus sp.)을 포함하는 미생물배양액에 기능성성분이 포함하는 기능성비료의 시비가 크리핑벤트그래스의 잔디품질과 생육에 미치는 영향에 대해 조사하였다. 처리구는 비료의 종류에 따라 무처리구(NF), 대조구(CF), 미생물배양액(MO; CF+MO),철 함유 미생물배양액(MO-Fe; CF+MO-Fe), 그리고 황함유 미생물배양액(MO-S; CF+MO-S)였다. 시험 전후 토양분석결과, pH는 시험 후에 전보다 모든 처리구에서 약간 증가하였고, 시험 종료 후 처리구간의 토양화학성은 비슷하여 공시비료의 시비는 토양환경에 거의영향을 미치지않았다. 잔디생육 조사결과, 엽색지수와 엽록소지수는 무처리구와 비교할 때, 관행구와 처리구에서 높았고, 관행구와 처리구들 사이에는 조사시기별 변화경향은 비슷하나 MO처리구에서 약간 높게 나타났다. 잔디뿌리는 MO와 MO-Fe에서 더 길었다. 잔디의 지상부와 지하부 생육을 조사결과, 지상부에서는 MO와 MO-S가, 지하부에서는 MO와 MO-S가 관행구보다 높았으며, MO처리가 NF와 CF보다 각각 26%와 6%증가하여 MO처리가 잔디생육에 가장 효과적이었다. T/R ratio는 모두 무처리구보다 증가였으나 처리구별 차이는 나타나지 않았다. 잔디 지상부 지하부의 무기성분함량을 CF와 비교할 때, 지상부에서는 CF보다 MO, MO-Fe 및 MO-S 처리구에서 질소와 인 함량 증가하였고, 지하부에서는 인 함량이 증가하였다. 본 연구 결과, 유산균과 효모균의 처리는 크리핑벤트그래스의 뿌리생육과 양분흡수를 촉진하여 잔디품질과 성장을 향상시키는 잔디성장촉진 기능이 있는 비료임을 알 수 있었다.

공액 사슬을 갖는 철 화합물의 전기화학적 특성 (Electrochemical Properties of Diiron Complexes wish Conjugated Chains)

  • 정민철
    • 한국전기전자재료학회논문지
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    • 제15권6호
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    • pp.511-517
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    • 2002
  • The complex 1 $([Cp*Fe(CO)_2]_2-(\mu-CH=CH-CH=CH))$ which have butadiene as a bridge were synthesized from $Cp*(CO)_2FeK$ and cis-3,4-dichlorocyclobutene. The derivatives of complex 1 where one or two carbonyl groups are replaced by phosphine ligands have been prepared by photochemical substitution. The new derivatives $([Cp*Fe(L)_2]_2-(\mu-CH=CH-CH=CH))$ where L = $(Ph_2PCH_2CH_2PPh_2)$ and $([Cp*Fe(CO)(L)]_2-(\mu-CH=CH-CH=CH))$ where L : $PPh_3$ have been characterized from $^^1H-$, $^^13C-$,$^^31P-NMR$ and elemental analysis. Obtained complexes have been studied in electrochemical experiment and UV/VIS-near-IR. The mixed-valence radical cation forms of complex 2, 3 species were found to be delocalized as the Class III. Based on the separation of the waves ($\triangle E$ : 0.470 ~ 0.605 V), the efficiency of electronic communication between two metal centers of cation species leading to stabilization relative to neutral species. The phosphine-substitute complexes (2, 3) displays two reversible oxidation waves and oxidation state of metal centers-dependent color change, electrochromism, was observed from yellow to orange and deep blue in methylene chloride.

The first of its kind metallicity map of the Large Magellanic Cloud

  • Choudhury, Samyaday;Subramaniam, Annapurni;Cole, Andrew A.
    • 천문학회보
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    • 제41권2호
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    • pp.30.1-30.1
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    • 2016
  • We have estimated a metallicity map of the Large Magellanic Cloud (LMC) using the Magellanic Cloud Photometric Survey (MCPS) and Optical Gravitational Lensing Experiment (OGLE III) photometric data. This is a first of its kind, high-spatial resolution map of metallicity up to a radius of $4^{\circ}-5^{\circ}$, derived using large area photometric data and calibrated using spectroscopic data of Red Giant Branch (RGB) stars. The RGB is identified in the V, (V - I) colour- magnitude diagrams of small subregions of varying sizes in both data sets. The slope of the RGB is used as an indicator of the mean metallicity of a subregion, and it is calibrated to metallicity using spectroscopic data for field and cluster red giants in selected subregions. The mean metallicity of the LMC is found to be [Fe/H] = -0.37 dex (${\sigma}[Fe/H]=0.12$) from MCPS data, and [Fe/H] = -0.39 dex (${\sigma}[Fe/H]=0.10$) from OGLE III data. The bar is found to have an uniform and higher metallicity compared to the disk, and is indicative of an active bar in the past. Both the data sets suggest a shallow radial metallicity gradient up to a radius of 4 kpc ($-0.049{\pm}0.002$ dex kpc-1 to $-0.066{\pm}0.006$ dex kpc-1). This metallicity gradient of the LMC disk, though shallow, resembles the gradient seen in spiral galaxies, and similar to that found in our Galaxy.

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Finite element analysis of shear-deficient RC beams strengthened with CFRP strips/sheets

  • Lee, H.K.;Ha, S.K.;Afzal, M.
    • Structural Engineering and Mechanics
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    • 제30권2호
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    • pp.247-261
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    • 2008
  • Performance of shear-deficient reinforced concrete (RC) beams strengthened with carbon fiber-reinforced polymer (CFRP) strips/sheets is analyzed through numerical simulations on four-point bending tests. The numerical simulations are carried out using the finite element (FE) program ABAQUS. A micromechanics-based constitutive model (Liang et al. 2006) is implemented into the FE program ABAQUS to model CFRP strips/sheets. The predicted results are compared with experiment data (Khalifa and Nanni 2002) to assess the accuracy of the proposed FE analysis approach. A series of numerical tests are conducted to investigate the influence of stirrup lay-ups on the shear strengthening performance of the CFRP strips/sheets, to illustrate the influence of the damage parameters on the microcrack density evolution in concrete, and to investigate the shear and flexural strengthening performance of CFRP strips/ sheets. It has been shown that the proposed FE analysis approach is suitable for the performance prediction of RC beams strengthened with CFRP strips/sheets.

Preparation and Electromagnetic Properties of an Electromagnetic Wave Absorber

  • Sun, Chang;Sun, Kangning;Pang, Laixue;Liu, Jian
    • Journal of Magnetics
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    • 제21권1호
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    • pp.61-64
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    • 2016
  • In this study, we report the as-prepared MgO-doped $BaFe_{12}O_{19}$, which was prepared by calcination technique and high-energy ball milling process, as an electromagnetic wave absorber. The phase analysis of $BaFe_{12}O_{19}$ and the as-prepared MgO-doped $BaFe_{12}O_{19}$ was detected utilizing X-ray Diffractometer (XRD). The microstructure was characterized using Scanning Electron Microscope (SEM). By means of the transmission/reflection coaxial line method, the electromagnetic properties and microwave absorbing properties of the as-prepared electromagnetic wave absorber were studied. It is found that the electromagnetic wave absorber has a minimum reflection loss value of -41 dB at 4.27 GHz with a matching thickness of 2.6 mm. The experiment results revealed that the as-prepared electromagnetic wave absorber could find potential applications in many military as well as commercial industries.

Periodicity Dependence of Magnetic Anisotropy and Magnetization of FeCo Heterostructure

  • Kim, Miyoung
    • Journal of Magnetics
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    • 제21권1호
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    • pp.6-11
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    • 2016
  • The magnetic anisotropy energy (MAE) and the saturation magnetization $B_s$ of (110) $Fe_nCo_n$ heterostructures with n = 1, 2, and 3 are investigated in first-principles within the density functional theory by using the precise full-potential linearized augmented plane wave (FLAPW) method. We compare the results employing two different exchange correlation potentials, that is, the local density approximation (LDA) and the generalized gradient approximation (GGA), and include the spin-orbit coupling interaction of the valence states in the second variational way. The MAE is found to be enhanced significantly compared to those of bulk Fe and Co and the magnetic easy axis is in-plane in agreement with experiment. Also the MAE exhibits the in-plane angle dependence with a two-fold anisotropy showing that the $[1{\overline{I}}0]$ direction is the most favored spin direction. We found that as the periodicity increases, (i) the saturation magnetization $B_s$ decreases due to the reduced magnetic moment of Fe far from the interface, (ii) the strength of in-plane preference of spin direction increases yielding enhancement of MAE, and (iii) the volume anisotropy coefficient decreases because the volume increase outdo the MAE enhancement.

980MPa급 초고장력 강판의 자동차 프런트 사이드 멤버 부품 성형에 관한 연구 (A Study on the Forming of Automotive Front Side Member Part with Ultra High Strength Steel of DP980)

  • 차승훈;이상곤;고대철;김병민
    • 소성∙가공
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    • 제18권1호
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    • pp.39-44
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    • 2009
  • This paper is concerned with forming technology of an automotive front side member part with ultra high strength steel sheet of DP980. The forming technology considered in this paper is the draw & form type, which installs the upper pad and lower pad to produce the complicated shape of ultra high strength steel sheet. In order to produce sound product, comparison between form type and draw & form type and between draw type and draw & form type are investigated by FE-analysis. FE-analysis is carried out with commercial sheet metal forming analysis S/W, DYNAFORM. It was shown from FE-analysis that the draw & form type satisfied the required specifications such as the dimensional accuracy and soundness of automotive front side member part. The effectiveness of the analytical result was verified by the experiment. From this investigation, the draw & form type is proved to be able to supply useful forming technology in forming ultra high strength steel.

기계적 합금화에 의한 나노구조 Fe-Co 합금분말의 제조 및 자성특성 (Fabrication of Nanostructured Fe-Co powders by Mechanical Alloying and Their Magnetic Properties)

  • 정진영
    • 한국분말재료학회지
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    • 제6권1호
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    • pp.27-35
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    • 1999
  • A study was made on the fabrication of nanostructured Fe-Co powders by mechanical alloying and their magnetic properties. Microstrural development during the process of MA was inverstigated by means of X-ray diffraction, differential thermal analyzer, scanning electron microscopy and transmission electron microscopy. The magnetic properties of NS Fe-Co powders were evaluated through the measurements of the saturation magnetization $(M_s)$ as well as the coercivity $(H_c)$. The average grain size calculated from line braodening in XRD peak was about 10nm or less and confirmed by TEM. In this experiment, two different milling methods (cycle opertion and conventional milling) were used. Cycle operation had an advantage over the conventional milling method in that more refined powders can be obtained. Solid state alloying of the components was confirmed from both the change of the saturation magnetization and the change of lattice parameter with Co contentration. Maxium $M_s$ was obtained at the composition of 30at.%Co. Relatively high coercivities of 10~150e were obtained for the compositions investigated, and this seems to be due to the high amount of internal strain introduced during milling.