• The Journal of Internal Korean Medicine
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• v.40 no.6
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• pp.1112-1121
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• 2019

Objectives: FDY003 is a raw material for medicine consisting of a natural product that is expected to have the advantages of low side effects and high efficacy. In this study, we predict the efficacy and the standardization of the drug by method validation of anticipated index compounds and the measurement of antioxidant activity. Methods: FDY003 is prepared by extracting and purifying 70% of ethyl alcohol (EtOH). The method validation of cordycepin and chlorogenic acid was determined by high-performance liquid chromatography-photo diode array (HPLC-PDA) and the content of FDY003 was calculated. In order to monitor the biological activity of FDY003, antioxidant activity was measured by 1,1-diphenyl-2-picrylhydrazyl (DPPH), 2,2-azino bis (3-ethylbenzothiazoline-6-sulfonic acid) (ABTS), and ferric-reducing antioxidant power (FRAP). The equivalent values of antioxidants such as trolox, ascorbic acid, gallic acid, and caffeic acid were measured by ABTS and FRAP. Results: Chlorogenic acid and cordycepin were both found suitable for method validation in HPLC and FDY003 containing 9.92±0.50 and 17.97±0.27 ㎍/g, respectively. In DPPH, the electron donating ability (EDA) value of FDY003 was increased in a concentration dependent manner. FDY003 confirmed antioxidant activity by ABTS and FRAP. Conclusions: FDY003 contains certain components including cordycepin and chlorogenic acid and has antioxidant ability by various mechanisms. Therefore, it is expected that FDY003 is capable of various physiological activities including anti-cancer activity.

• Journal of the Korean Society of Clothing and Textiles
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• v.10 no.1
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• pp.105-111
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• 1986

본 연구에서는 연신정도가 다른 완전배향사(FDY)와 부분배향사(POY)를 열처리시켜 내부구조변화를 유도한 후 염색성을 연구하였고, 염색성과의 관련성을 위해 결정화도 및 복굴절룰을 조사하였다. 열처리는 silicone oil속에서 정장상태로 실시하였으며, 시료의 염색은 Disperse Yellow 42를 이용해 무한염욕상태에서 실시하였다. 그리고, DMF를 이용해 염료를 추출시킨후 spectrophotometer 로 염료흡착량을 측정하였다. 결정화도는 밀도-결정화도 관계식으로 구하였으며, 복굴전률은 편광현미경으로 시료의 두께와 retardation을 측정한 후 계산하였다. FDY와 POY 필라멘트사의 염색성은 열처리시 감소하였으며 POY의 염색성이 FDY보다 우수했다. 결정화도는 열처리시 증가하였으며 열처리되지 않은 POY가 열처리되지 않은 FDY에 비해 낮은 값을 나타냈다. 복굴절률은 열처리시 증가하였으며 열처리되지 않은 POY가 열처리되지 않은 FDY에 비해 낮은 값을 나타냈다. 열처리후에도 POY가 FDY보다 낮은 복굴절률을 나타낸 반면 결정화도는 열처리된 POY가 열처리된 FDY와 비슷한 값을 나타냈다. 염색성은 결정화도와 배향도에 부적인 상관관계 즉 결정화도와 배향도가 증가함에 따라 염색성은 감소하는 관계를 시사했다.

• Textile Coloration and Finishing
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• v.16 no.6
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• pp.35-43
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• 2004

This study surveys the physical properties of ATY produced with FDY and POY. ATY is made with 70d Nylon FDY and 80d Nylon POY using AIKI air jet texturing machines, respectively. The processing parameters such as air pressure and yam speed are varied, and air pressure is varied ranging with 8.5bar, l0.5bar and 1l.5bar, and yarn speed is varied ranging with 400m/mim, 450m/mim, and 500m/min. The various physical properties of ATY made by POY and FDY denier, wet shrinkage, dry shrinkage, tensile properties, thermal stress and instability are measured and discussed with air pressure and yam speed. The shrinkage simulation of ATY is performed for analysing the process shrinkage on the dyeing and finishing processes.

• Journal of the Korean Society of Clothing and Textiles
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• v.13 no.1 s.29
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• pp.43-47
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• 1989

The microstructural changes of nylon 6 UDY, POY and FDY were compared after free-annealing through crystallinity, birefringence, and melting behavior analyses. Free-annealing was done at various temperatures $(120^{\circ}C\;,140^{\circ}C,\;160^{\circ}C,\;180^{\circ}C,\;200^{\circ}C)$ and times (15 min., 30 min., 60 min.) using vaccum oven. Crystallinity was measured by the density gradient column technique and birefringence was measured using a Nikon polarizing microscope with a quartz wedge and Senarmont compensator. Melting behavior was investigated on the basis of DSC melting corves. Crystallinites of specimens increased as the treatment temperature and time increased. Birefringence of UDY increased after annealing and increased as the treatment temperature increased. On the other hand, those of POY and FDY decreased after annealing. Especially, the changes of crystallinity and birefringence of treated POY were particularly lower than those of treated UDY and FDY. Melting peaks of untreated UDY, POY and FDY were different in the position and the shape, but little change was seen in melting peaks in spite of increasing the annealing temperature and time. UDY and FDY showed single melting peaks in all the specimens. But POY showed double melting peaks, which means the coexistences of crystals with different thermal properties.

• Bulletin of the Korean Chemical Society
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• v.31 no.11
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• pp.3252-3258
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• 2010

In this study, the effects of the various parameters of spinning and drawing processes on the properties of polyester full drawn yarn (FDY) prepared by steam processing during high-speed spinning were investigated using several techniques. The wet shrinkage ratio of the FDY was able to be manipulated by controlling the temperature and draw ratio. The FDY made using the steam high speed spinning technique exhibited identical properties (such as tenacity, elongation, and wet shrinkage ratio) to that of regular FDY, made using the spin-draw process. FDY prepared using the steam process during high-speed spinning showed excellent dyeability. The dye pick-up of the polyester yarn spun at high-speed spinning was found to be improved when dyed under an atmospheric pressure of $100^{\circ}C$. This result was the same as regular FDY dyed under a high pressure of $130^{\circ}C$.

• Textile Coloration and Finishing
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• v.25 no.3
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• pp.223-231
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• 2013

This research has a main focus on providing fundamental data for on-the-spot industrial fields by comparing and contrasting physical properties of fluffy spun-like material. The fluffy spun-like yarn is developed as fluffy yarn similar to natural spun-like yarn by treating polyester(FDY and + type shaped DTY) with ATY machine. In this experiment, using ATY machine for raw material texturing, we produced two fluffy yarns: (i) + type shaped(50d/36f, DTY) as core yarn and 100d/192f FDY as effect yarn[ATY(D)], (ii) FDY(75/36) as core yarn and 100d/192f FDY [ATY(F)] as effect yarn. After producing thous yarns, we twisted them with 500T/M, 700T/M, 1000T/M, respectively. produced yarns through this process were used as the samples for this experiment. Even though the shrinkage of fluffy yarn ATY(F) and ATY(D) becomes high as treated temperature rises and treated time lengthens, it is more affected by treated temperature then by treated time. In this experiment, produced fluffy yarn[ATY(D)] shows a little high values for temperature, but almost same values for higher temperatures. When we compare ATY(F) with ATY(D) fluffy yarn shows more natural fluffy yarn surface structure like natural cotton. The shrinkage of 700T/M twisted ATY(D) fluffy yarn show about 11% under treated temperature $180^{\circ}C$ and treated time 30min, and about 7% under $120^{\circ}C$ and 30min, respectively. But the shrinkage of 1000T/M fluffy yarn shoes about 9% and 6% under same conditions. Regarding treated time, tenacity and initial modulus of ATY(D) fluffy yarn rise high until 30min, but do not show much increase above 30min. Regarding treated temperature, tenacity and initial modulus of it rise high aboyer $140^{\circ}C$.

• Journal of the Korean Society of Clothing and Textiles
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• v.11 no.3 s.25
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• pp.33-40
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• 1987

PET FDY was heat set at various temperatures and times and the microstructural changes was investigated through crystallinity, birefringence and melting behavior analyses. Crystallinity of heat set PET increased as the treatment temperature and time increased. Birefringence also increased as temperature and time increased. The melting behavior of heat set PET was as follows: In most cases, PET showed double melting peaks. As temperature and time increased, form II crystal became sharp and increased in size, and form I crystal decreased in size. The slower the heating rate, the higher the programmed heating effect during DSC analysis.