• 제목/요약/키워드: Extraction methods

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화학적 추출법에 따른 (구)장항제련소 주변 토양의 중금속 오염특성 분석과 식물 전이 가능량 예측 (Study on Heavy Metal Contamination Characteristics and Plant Bioavailability for Soils in the Janghang Smelter Area)

  • 정슬기;안진성;김영진;김건하;최상일;남경필
    • 한국지하수토양환경학회지:지하수토양환경
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    • 제16권1호
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    • pp.42-50
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    • 2011
  • Potential risk of heavy metals to various receptors including humans depends on the bioavailability of the heavy metals in soil. In this study, the heavy metal extraction methods using 0.1N HCl and aqua regia were compared with the Tessier's sequential extraction method to assess whether these two methods can be used to determine the plant-available heavy metal concentrations. The contamination characteristics of copper (Cu), cadmium (Cd), lead (Pb), and arsenic (As) found in soils collected from 75 sites around the closed Janghang smelter were analyzed by extracting heavy metals using 0.1 N HCl, aqua regia, and the Tessier's sequential extraction method. The portion of metals bioavailable to plants is considered as the sum of the fraction 1 (exchangeable) and the fraction 2 (carbonates binding) of the Tessier's 5-step sequential extraction method, which were determined to be 3.1 ${\pm}$ 3.82, 0.6 ${\pm}$ 0.15, 20.6 ${\pm}$ 18.78, and 7.0 ${\pm}$ 6.48 mg/kg for Cu, Cd, Pb, and As, respectively, in this study. When the extraction using aqua regia and the Tessier's extraction method were compared, the extracted Cu and Pb concentrations did not show significant differences, whereas the extracted Cd and As concentrations showed significant differences. These results indicate that the portion of Cd and As in the fraction 5 of the Tessier's sequential extraction can not be extracted using aqua regia. Using aqua regia, which is the official test method, higher concentrations of Cu, Cd, Pb and As were extracted than the sum of the fraction 1 and 2. The results show that only 9, 40, 39 and 10% of Cu, Cd, Pb and As using aqua regia can be uptaken by plants (i.e., plant-available). Using 0.1N HCl, the portion of Cd equivalent to about 66% the fraction 1 could be extracted, while, with Pb, the portion of the fraction 1 and about 90% of the fraction 2 could be extracted. With As, the portion equivalent to the fraction 1, 2 and 79% of the fraction 3 was extracted, while with Cu, the portion equivalent to the fraction 1, 2, 3 and 20% of the fraction 4 was extracted using 0.1N HCl.

Comparative Study of Knowledge Extraction on the Industrial Applications

  • Woo, Young-Kwang;Bae, Hyeon;Kim, Sung-Shin;Woo, Kwang-Bang
    • 제어로봇시스템학회:학술대회논문집
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    • 제어로봇시스템학회 2003년도 ICCAS
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    • pp.1338-1343
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    • 2003
  • Data is the expression of the language or numerical values that show some characteristics. And information is extracted from data for the specific purposes. The knowledge is utilized as information to construct rules that recognize patterns and make decisions. Today, knowledge extraction and application of the knowledge are broadly accomplished to improve the comprehension and to elevate the performance of systems in several industrial fields. The knowledge extraction could be achieved by some steps that include the knowledge acquisition, expression, and implementation. Such extracted knowledge can be drawn by rules. Clustering (CU, input space partition (ISP), neuro-fuzzy (NF), neural network (NN), extension matrix (EM), etc. are employed for expression the knowledge by rules. In this paper, the various approaches of the knowledge extraction are examined by categories that separate the methods by the applied industrial fields. Also, the several test data and the experimental results are compared and analysed based upon the applied techniques that include CL, ISP, NF, NN, EM, and so on.

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Determination of nickel and cadmium in fish, canned tuna, black tea, and human urine samples after extraction by a novel quinoline thioacetamide functionalized magnetite/graphene oxide nanocomposite

  • Naghibzadeh, Leila;Manoochehri, Mahboobeh
    • Carbon letters
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    • 제26권
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    • pp.43-50
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    • 2018
  • In this research, a novel and efficient quinoline thioacetamide functionalized magnetic graphene oxide composite ($GO@Fe_3O_4@QTA$) was synthesized and utilized for dispersive magnetic solid phase preconcentration of Cd(II) and Ni(II) ions in urine and various food samples. A number of diverse methods were employed for characterization of the new nanosorbent. The design of experiments approach and response surface methodology were applied to monitor and find the parameters that affect the extraction performance. After sorption and elution steps, the concentrations of target analytes were measured by employing FAAS. The highest extraction performance was achieved under the following experimental conditions: pH, 5.8; sorption time, 6.0 min; $GO@Fe_3O_4@QTA$ amount, 17 mg; 2.4 mL $1.1mol\;L^{-l}$ $HNO_3$ solution as the eluent and elution time, 13.0 min. The detection limit is 0.02 and $0.2ng\;mL^{-1}$ for Cd(II), and Ni(II) ions, respectively. The accuracy of the new method was investigated by analyzing two certified reference materials (sea food mix, Seronorm LOT NO 2525 urine powder). The interfering study revealed that there are no interferences from commonly occurring ions on the extractability of target ions. Finally, the new method was satisfactorily employed for rapid extraction and determination of target ions in urine and various food samples.

매복지치 발치 시 발생한 합병증 양상에 대한 후향적 연구 (Complications of impacted third molar extraction: retrospective study)

  • 황정국;김경욱
    • Journal of the Korean Association of Oral and Maxillofacial Surgeons
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    • 제36권2호
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    • pp.119-124
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    • 2010
  • Introduction: Surgical extraction of third molar is one of the most frequently performed procedures in oral and maxillofacial surgery unit as the impacted wisdom teeth could cause various complications. Even though, however, extraction of the impacted wisdom teeth is an obligation for the reason of possible complication even for general practitioners, it has been avoided. Various factors concerning surgical extraction of impacted third molar are considered: general condition of patients, relationship with relative anatomies, aspects of impaction, surgeon's skill. Materials and Methods: The consideration and crossing analysis of these factors with 2,463 patients who visit Dankook University dental hospital to extract those impacted third molar. Results: 1. Gender doesn't affect. 2. Medical problems have more complications. 3. There are more complications in high difficulty index (DI) impacted teeth. 4. When inferior alveolar canal overlap mandibular third molar, complication rate is 26.92%. 5. The most common complication was swelling and pain. 6. There is no statistical difference between the incidence of complication and surgeon's experience. Conclusion: In regard to these results, it seems that clinical or radiological examination can predict potential complications of wisdom teeth, and it is helpful to bear in mind the fact.

표고버섯 배양액으로부터 단백다당류의 추출 및 정제 방법 (Extraction and Separation of Protein-bound Polysaccharide by Lentinus edodes)

  • 박경숙;이별나
    • 한국식품영양학회지
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    • 제10권4호
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    • pp.503-508
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    • 1997
  • L. edodes의 배양액 및 균사체로부터 항암작용이 있는 단백 다당류의 추출 및 정제방법에 관한 실험을 실시하였다. 단백다당류 추출에서 비이온성 계명 활성제인 2% Triton X-100 용액으로 추출할 경우 상온에서 추출하여도 통상의 10$0^{\circ}C$ 열수 추출을 통해 얻을 수 있는 것보다 수율이 높았다. 그러나 계명활성제 용액에 4N NaCl을 첨가하여 추출하면 ethanol 침전과정에서 단백다당류의 침전물을 얻을 수 없었다. 열수 추출에 있어서 추출 온도는 10$0^{\circ}C$가 효과적이고 추출 시간은 4시간 정도면 충분하였다. 열수 추출 결과 ethanol 침전 및 동결건조를 통하여 얻어진 조단백 다당류의 정제 실험에서는 alumina를 충전제로 하는 gel filtration보다 sephadex에 의한 gel filtration 또는 DEAE-cellulose, DEAE-sephadex를 이용한 ion exchange chromatography가 보다 효과적이다.

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Emotion recognition from speech using Gammatone auditory filterbank

  • 레바부이;이영구;이승룡
    • 한국정보과학회:학술대회논문집
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    • 한국정보과학회 2011년도 한국컴퓨터종합학술대회논문집 Vol.38 No.1(A)
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    • pp.255-258
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    • 2011
  • An application of Gammatone auditory filterbank for emotion recognition from speech is described in this paper. Gammatone filterbank is a bank of Gammatone filters which are used as a preprocessing stage before applying feature extraction methods to get the most relevant features for emotion recognition from speech. In the feature extraction step, the energy value of output signal of each filter is computed and combined with other of all filters to produce a feature vector for the learning step. A feature vector is estimated in a short time period of input speech signal to take the advantage of dependence on time domain. Finally, in the learning step, Hidden Markov Model (HMM) is used to create a model for each emotion class and recognize a particular input emotional speech. In the experiment, feature extraction based on Gammatone filterbank (GTF) shows the better outcomes in comparison with features based on Mel-Frequency Cepstral Coefficient (MFCC) which is a well-known feature extraction for speech recognition as well as emotion recognition from speech.

A Two-stage Process for Increasing the Yield of Prebiotic-rich Extract from Pinus densiflora

  • Jung, Ji Young;Yang, Jae-Kyung
    • Journal of the Korean Wood Science and Technology
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    • 제46권4호
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    • pp.380-392
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    • 2018
  • The importance of polysaccharides is increasing globally due to their role as a significant source of dietary prebiotics in the human diet. In the present study, in order to maximize the yield of crude polysaccharides from Pinus densiflora, response surface methodology (RSM) was used to optimize a two-stage extraction process consisting of steam explosion and water extraction. Three independent main variables, namely, the severity factor (Ro) for the steam explosion process, the water extraction temperature ($^{\circ}C$), and the ratio of water to raw material (v/w), were studied with respect to prebiotic sugar content. A Box-Behnken design was created on the basis of the results of these single-factor tests. The experimental data were fitted to a second-order polynomial equation for multiple regression analysis and examined using the appropriate statistical methods. The data showed that both the severity factor (Ro) and the ratio of water to material (v/w) had significant effects on the prebiotic sugar content. The optimal conditions for the two-stage process were as follows: a severity factor (Ro) of 3.86, a water extraction temperature of $89.66^{\circ}C$, and a ratio of water to material (v/w) of 39.20. Under these conditions, the prebiotic sugar content in the extract was 332.45 mg/g.

Age, extraction rate and jaw surgery rate in Korean orthodontic clinics and small dental hospitals

  • Jung, Min-Ho
    • 대한치과교정학회지
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    • 제42권2호
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    • pp.80-86
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    • 2012
  • Objective: This study aimed to investigate the current data regarding age, sex, and Angle Classification of Korean orthodontic patients and influence of these factors on the tendency to undergo extraction and orthognathic surgery. Methods: The recent trends of Korean orthodontic patients were assessed using questionnaire survey. The questionnaires were e-mailed to orthodontists who met the study criteria; 58% of the orthodontists opened the e-mails, and 27.7% replied to the e-mails. In all, the medical records of 11,340 patients who underwent orthodontic treatment at private clinics and small dental hospitals in Korea were analyzed. Results: The percentage of female patients in the study sample was 69.6%, and the average age of the patients was 19.87 years. The percentage of patients who were older than 19 years was 50.2%. Class II and Class III malocclusions were noted in 33.6% and 23.6% of patients, respectively. Extraction and orthognathic surgery were performed in 60.4% and 6.9% of patients, respectively. Conclusions: The results showed that there were a high percentage of adult, Class II malocclusion and extraction patients in private practices and small dental hospitals during the study period. Further, a relatively high proportion of adult patients opted to undergo orthognathic surgery.

Comparison of safety and analgesic efficacy of diclofenac sodium with etodolac after surgical extraction of third molars: a randomized, double-blind, double-dummy, parallel-group study

  • Vaghela, Jitendra H.;Shah, Jigna H.;Patel, Jaladhi H.;Purohit, Bhargav M.
    • Journal of Dental Anesthesia and Pain Medicine
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    • 제20권1호
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    • pp.19-27
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    • 2020
  • Background: Surgical extraction of third molars is associated with postoperative pain and swelling at the extraction site. Pain is commonly managed using non-steroidal anti-inflammatory drugs (NSAIDs). Postoperative pain is usually moderate to severe in the first 12 h postoperatively and lasts for 3-5 days. However, with NSAIDs, these symptoms usually subside within 24 h. Diclofenac sodium and etodolac are NSAIDs, more selectively cyclooxygenase-2 inhibitors, with good analgesic efficacies. Methods: We compared the safety and analgesic efficacy of diclofenac sodium with etodolac peroral after surgical extraction of third molars in a double-blind, double-dummy, parallel-group study. The subjective pain improvement and pain relief after 2, 6, 24, 48, and 72 h using the visual analogue scale were measured as the study outcome. Results: Etodolac was equivalent to diclofenac sodium in pain alleviation at all postoperative time periods. No significant differences were found between diclofenac sodium and etodolac groups (P > 0.05). Both study medications were well tolerated and safe with mild adverse effects in only a few participants. Conclusion: Diclofenac sodium and etodolac are comparable in terms of analgesic efficacy and safety after surgical removal of third molars.

A TWO-STAGE SOURCE EXTRACTION ALGORITHM FOR TEMPORALLY CORRELATED SIGNALS BASED ON ICA-R

  • Zhang, Hongjuan;Shi, Zhenwei;Guo, Chonghui;Feng, Enmin
    • Journal of applied mathematics & informatics
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    • 제26권5_6호
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    • pp.1149-1159
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    • 2008
  • Blind source extraction (BSE) is a special class of blind source separation (BSS) methods, which only extracts one or a subset of the sources at a time. Based on the time delay of the desired signal, a simple but important extraction algorithm (simplified " BC algorithm")was presented by Barros and Cichocki. However, the performance of this method is not satisfying in some cases for which it only carries out the constrained minimization of the mean squared error. To overcome these drawbacks, ICA with reference (ICA-R) based approach, which considers the higher-order statistics of sources, is added as the second stage for further source extraction. Specifically, BC algorithm is exploited to roughly extract the desired signal. Then the extracted signal in the first stage, as the reference signal of ICA-R method, is further used to extract the desired sources as cleanly as possible. Simulations on synthetic data and real-world data show its validity and usefulness.

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