• 대한전기학회:학술대회논문집
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• 대한전기학회 2002년도 하계학술대회 논문집 B
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• pp.688-690
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• 2002

The quench current characteristics of the superconducting solenoids with large diameter were experimentally investigated. Three solenoids with the inside diameter of 450mm were fabricated and tested for various winding tensions and epoxy impregnation conditions. The highest quench current was obtained in the solenoid impregnated with epoxy after wound with winding tension of 20 percents. Although the training effect in the solenoid appeared after epoxy impregnation, The quench current of solenoid impregnated with epoxy was higher than that before impregnation. The test results and discussions were presented.

• 대한전기학회논문지:전기기기및에너지변환시스템부문B
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• 제53권6호
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• pp.368-371
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• 2004

The quench current characteristics of the superconducting solenoids with large diameter were experimentally investigated. Three solenoids with inside diameter of 450mm were fabricated with different tensions and different types of epoxy applications. The quench current of each solenoid was measured according to the various ramping rates of current. The highest quench current was obtained in the solenoid impregnated with epoxy after winding with tension of 20 percents of the yield strength of the superconducting wire. It was found that the quench currents were almost independent of the ramp rate of current. From the results, although the training effect in the solenoid appeared with epoxy impregnation, the quench current of solenoid impregnated with epoxy was higher than that without epoxy impregnated The test results are presented and discussed.

• Transactions on Electrical and Electronic Materials
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• 제13권4호
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• pp.200-203
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• 2012

Epoxy/mica composite was synthesized, in order to use it as an impregnation resin in a vacuum pressure impregnation (VPI) process, for manufacturing a high voltage rotary machine. The average particle size of the mica was 5~7 ${\mu}m$ and its content was 0, 20, 30 and 40 wt%. A plasticizer or a low molecular aliphatic epoxy was also used, to decrease the viscosity of the composite. The AC electrical breakdown strength was estimated in sphere-to-sphere electrodes, and the electrical breakdown data were estimated by Weibull statistical analysis. The electrical breakdown strength became higher with the addition of mica; and that of the system with 20 wt% mica was highest. The electrical breakdown strength of the system with an aliphatic epoxy was higher than that of the system with a, plasticizer.

• 한국초전도ㆍ저온공학회논문지
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• 제7권1호
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• pp.42-46
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• 2005

The resistive type high temperature superconducting fault current limiter (HTSFCL) limits the fault current using the resistance generated by fault current. The generated resistance by fault current makes large pulse power which makes the operation of HTSFCL unstable. So, the cryogenic cooling system of the resistive type HTSFCL must diffuse and eliminate the pulse energy very quickly. Although the best way is to make wide direct contact area between HTS winding and coolant as much as possible, HTS winding also needs the impregnation layer which fixes and protects it from electromagnetic force. This paper deals with the thermal conductivity and dielectric strength of some epoxy compounds for the impregnation of high temperature superconducting (HTS) winding in liquid nitrogen. The measured data can be used in the optimal design of impregnation for HTS winding. Aluminar filling increased the thermal conductivity of epoxy compounds. Hardener also affected the thermal and electric characteristic of epoxy compounds.

• 한국산업융합학회 논문집
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• 제25권3호
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• pp.461-466
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• 2022

Epoxy resins are widely used in various industrial fields. However, they suffer from brittleness, an issue that must be addressed for further applications. To solve this problem, additional fillers are needed to improve the mechanical and thermal properties of the resins; zirconia is one such filler. However, it has been reported that aggregation may occur in the epoxy composites as the amount of zirconia increases, preventing enhancement of the mechanical strength of the epoxy composites. Herein, to reduce the aggregation, zirconia was well dispersed on halloysite nanotubes (HNTs), which have high thermal and mechanical strength, by a conventional wet impregnation method using zirconyl chloride octahydrate as a precursor. The mechanical and thermal strengths of the epoxy composites with The zirconia impregnated HNTs (Zr/HNT) were investigated. Zr/HNT were characterized by Scanning electron microscope (SEM), transmittance electron microscopy (TEM), X-ray diffraction (XRD) and X-ray photoelectron spectroscopy. The thermal strength of the epoxy composites was studied by thermomechanical analysis (TMA) and the mechanical strength of the epoxy composites (flexural strength) was studied by using a universal testing machine (UTM). The mechanical and thermal strengths of the epoxy complex with Zr/HNT were improved compared to those of the epoxy complex with HNT, and also increased as the content of Zr/HNT increased.

• Korean Chemical Engineering Research
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• 제59권4호
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• pp.521-531
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• 2021

진공가압함침공정(Vacuum Pressure Impregnation, VPI)은 발전기, 전동기 등 대형 회전기에 사용되는 고정자 권선에 에폭시 계열의 레진을 코팅시켜 물성을 강화하는 공정이다. VPI 공정 중 진공과 가압과정에서 에폭시 레진의 기화에 의해 레진 가스가 발생하고, 함침공정이 끝나고 경화를 위해 탱크 개방 시 레진 가스가 제거되지 않고 탱크 밖으로 유출된다. 유출된 레진 가스가 작업장 전체에 확산 시 화재, 폭발 및 호흡기 문제와 같은 안전 환경 문제가 있으므로 공정 내 레진 가스 배출시스템이 필요하다. 따라서, 본 연구에서는 VPI 공정에서 발생한 레진 가스를 배출하는 시스템을 설계하기 위해 전산유체역학(Computational Fluid Dynamics, CFD)을 이용하여 공기 유입구·배출구의 위치에 따른 배출효율에 대한 사례연구를 진행하였다. 본 연구의 최적의 배출시스템을 활용 시 1,800초 이내 90%이상의 레진 가스를 배출할 수 있으며, 레진 가스의 폭발하한계(Low Explosive Limit, LEL)이하로 레진 가스의 분율을 낮출 수 있었다.

• 한국세라믹학회지
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• 제37권8호
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• pp.760-767
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• 2000

Recently, the protection of construction is demanded with environmental pollution. These protect modes are use of concrete admixture, coat of protective polymer and impregnate of surface with chemicals etc. The most widely used impregnation is economical and effective. The define of Impregnation for construction protect is reacted in and consolidated substrate after absorbed. The impregnation agents are Polyesters, Acrylic monomers, Epoxy and Silicone derivatives. Commonly, because the Silane has good water repellency and environmental advantages that it widely used to water proofing agents, dampproofing agents and absorption reducer for concrete of bridges. When application of Silane, it occurs pollution and harmfulness as included organic solvent. The manufactures have tired to emulsification of Silane for the reducing of the defects. The Silane emulsion is vary unstable and does not stored long periods, and it is diminished in good properties with internal reaction. In this study we tried to emulsification of Silane for effectiveness improvement and reduce pollution and hazard and discussed properties variation of emulsion. The Silane emulsions are achieved emulsifying with W/O and O/W type surfactants. It used 0.24% PVA as protective colloid and stable phase is creamy. The creamy Silane emulsion performance as the penetration depth and water absorption rate are above 4 mm and below 0.1. It stable about 6 month at room temperature.

• Composites Research
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• 제30권6호
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• pp.365-370
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• 2017

탄소섬유 강화 열가소성 수지 복합재료(Carbon fiber reinforced thermoplastic composites; CFRTPs)의 물성은 다양한 요인들에 영향을 받는다. 그 중에서도 탄소섬유 표면에 Sizing되어 있는 에폭시(Epoxy) 층은 열가소성 수지와 상호 작용(Interaction)이 없어 매우 취약한 계면을 형성하며, 열가소성 수지의 높은 용융 점도(Melting viscosity)는 탄소섬유 다발(Bundle) 사이로 함침(Impregnation)이 어려워 탄소섬유 강화 복합재료 내부에 기공(Void)를 형성한다. 이와 같이 탄소섬유와 열가소성 수지 간의 낮은 계면전단강도(Interfacial shear strength)은 탄소섬유강화 열가소성 복합재료(Carbon fiber reinforced thermoplastic composites; CFRTPs)의 기계적 물성을 저하시키는 가장 중요한 요인 중 하나이다. 따라서, 본 연구에서는 열가소성 수지와의 상호작용이 없는 탄소섬유 표면의 에폭시 층을 열풍을 통해 제거하고, 열가소성 수지의 점도를 낮춰 함침도를 향상시키기 위해서 용액형 열가소성 수지를 제조하여 탄소섬유 표면에 Sizing 처리 함으로써 CFRTPs의 물성을 향상시켰다. CFRTPs의 층간전단강도(Interlaminar shear strength; ILSS) 및 굽힘 강도(Flexural strength)를 통해 이를 검증하였으며, 수지의 함침도는 기공률(Void content)의 계산을 통해 분석하였다.

• 한국전기전자재료학회:학술대회논문집
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• 한국전기전자재료학회 2006년도 하계학술대회 논문집 Vol.7
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• pp.247-248
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• 2006

Bulk YBCO 초전도체는 top-seeded melt-growth 방법으로 제조되었다. YBCO bulk는 Epoxy resin과 $AgNO_3$를 보강해 초전도체의 기계적 강도를 향상하고자 하였다. Epoxy resin은 보강 재료인 STYCAST 2850-FT와 경화제인 CATALYST 24LV 를 100:5 비율로 혼합하여 제조한 후 mould에 넣고 $66^{\circ}C$에서 2시간 열처리 하였다 (rotary pump로 진공 분위기 조성). $AgNO_3$는 $350^{\circ}C$에서 2시간, $450^{\circ}C$에서 1시간 열처리 하여 Ag와 $NO_3$의 분리 후 YBCO bulk에 Ag가 보강되도록 하였다. Epoxy resin 과 분리된 Ag는 YBCO bluk의 crack과 void에 침투되는 것을 SEM과 광학현미경을 통해 관찰할 수 있었다. Three point bending test를 이용하여 보강 전후의 YBCO bulk의 기계적 강도를 측정하였다. 보강 후의 YBCO bluk의 기계적 강도는 보강 전에 비해 향상된 결과를 확인할 수 있었고, Epoxy resin과 $AgNO_3$를 보강한 YBCO는 기계적 강도 향상에 높은 신뢰성을 보이고 있다.

• Composites Research
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• 제24권2호
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• pp.30-37
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• 2011

에폭시 수지와 유리섬유직물 간의 젖음성을 분석하였다. 에폭시 수지와 산무수물 경화제의 혼합비는 당량비 1:0.5, 1:1, 1:1.2로 하였고, 촉매는 혼합된 수지의 0.lwt%로 첨가하였다. DSC 경화거동분석 결과 이 혼합 수지는 상온에서 함침이 가능하였다. 혼합 수지에 대해 유리평판에 놓여진 유리섬유직물 위에 수지 한 액적(방울)을 투하 후 시간에 따른 접촉각 변화를 측정하였다, 또한, 일정량의 에폭시 수지 액적을 투하시켜 시간에 따른 젖음면적 변화를 측정하였다, 접촉각, 액적높이, 순수 젖음면적, 젖음계수를 측정함으로써 유리섬유직물에 대한 에폭시 수지의 젖음성을 비교 평가하였다. 그 결과 당량비 1:1.2에서 유리섬유직물에 대한 젖음성이 가장 우수하였다.