• 제목/요약/키워드: Elemental System

검색결과 306건 처리시간 0.029초

Synthesis of novel disperse dyes derived from phthalimide containning diester groups and their dyeing properties

  • Choi, Jae-Hong;Choi, Jong-Yun;Lee, Hyun-Young;Kwon, Oh-Tak
    • 한국염색가공학회:학술대회논문집
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    • 한국염색가공학회 2009년도 학술발표대회
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    • pp.45-46
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    • 2009
  • In this study, 12 azo disperse dyes based on phthalimide were synthesized including their precursors. The chemical structures of the dyes and the corresponding precursors were analyzed by the GC-MASS, $^1H$ NMR spectra and elemental analysis. The dyeability on PET, such as step dyeing and build-up properties and color fastness were examined using conventional exhaust dyeing procedures.

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기계적 합금화 방법에 의한 Cu-C계 복합금속분말의 제조 및 미세구조 제어 특성 (Synthesis and Microstructural Characterization of Cu-C Composite Metal Powder by Mechanical Alloying)

  • 이광민
    • 한국분말재료학회지
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    • 제4권1호
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    • pp.42-47
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    • 1997
  • It was investigated whether mechanical alloying (MA) processing could be more effective to the formation of metallic composite powder in Cu-C system. Elemental powder mixtures of Cu-70vo1.%C were mechanically alloyed with an attritor in an argon atmosphere and microstructural evolution was examined by X-ray diffraction analysis, scanning electron microscopy and transmission electron microscopy. It has been found that even with the high volume fraction of immiscible graphite in Cu-C system, the refinement with a few ten nanometer size as well as the highly uniform distribution of copper phases have been achieved by the MA processing.

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Chemical Speciation of Trace Metals in Natural Water by Ultrafiltration/Size Exclusion Chromatography/UV Absorption/ICP-MS

  • Haraguchi, Hiroki;Itoh, Akihide;Kimata, Chisen
    • 분석과학
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    • 제8권4호
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    • pp.405-410
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    • 1995
  • A study on elemental speciation of trace metals in lake water (Lake Biwa in Japan) has been carried out by a size exclusion chromatography (SEC) / inductively coupled plasma mass spectrometry (ICP-MS) system. Before analysis, the water sample was preconcentrated with a ultrafiltration technique, where the large molecules with molecular weight larger than 10,000 were concentrated. Then the preconcentrated water samples (500-1000 fold) were analyzed by a SEC/ICP-MS system. Most trace metals were found at the UV absorption peaks corresponding to the molecular weights of ca. 300,000 and 10,000-50,000, where trace metals were on-line detected by ICP-MS. The results suggest that many of trace metals exist as the large organic molecules-metal complexes in natural water.

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Analysis of Off-axis Integral Floating System Using Concave Mirror

  • Kim, Young Min;Jung, Kwang-Mo;Min, Sung-Wook
    • Journal of the Optical Society of Korea
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    • 제16권3호
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    • pp.270-276
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    • 2012
  • An off-axis integral floating system using a concave mirror is analyzed to resolve the image distortion incurred by the off-axis optical arrangement. The concave mirror can be adopted as the floating device to improve the optical efficiency. The image distortion due to the tilting axis of the concave mirror needs to be analyzed precisely to generate the pre-distortion image. In this paper, we calculate the image deformation in the off-axis structure of the concave mirror using the geometrical optics. Using the calculation results, the compensated elemental image can be generated for the pre-distortion integrated image, which can be projected to the floating 3D image without image distortion. The basic experiments of the off-axis integral floating are presented to prove and verify the proposal.

Isotopic Analysis of NUSIMEP-6 Uranium Particles using SEM-TIMS

  • Park, Jong-Ho;Park, Sujin;Song, Kyuseok
    • Mass Spectrometry Letters
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    • 제4권3호
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    • pp.51-54
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    • 2013
  • Isotopic analysis using thermal ionization mass spectrometry coupled with scanning electron microscopy (SEM-TIMS) was performed to determine the isotopic ratios of uranium contained in micro-particles in the 6th Nuclear Signatures Interlaboratory Measurement Evaluation Programme (NUSIMEP-6) sample. Elemental analysis by energy dispersive X-ray spectroscopy (EDS) was conducted on uranium-bearing mirco-particles, which were transferred to rhenium filaments for TIMS loading using a micromanipulation system in a SEM. A multi-ion-counter system was utilized to detect the ion signals of the four isotopes of uranium simultaneously. The isotope ratios of uranium corrected by bracketing using a reference material showed excellent agreement with the certified values. The measurement accuracy for $n(^{234}U)/n(^{238}U)$ and (b) $n(^{235}U)/n(^{238}U)$ was 10% and 1%, respectively, which met the requirements for qalification for the NetWork of Analytical Laboratories (NWAL).

Study of Three-dimensional Display System Based on Computer-generated Integral Photography

  • Lee, Byoung-Ho;Jung, Sung-Yong;Min, Sung-Wook;Park, Jae-Hyeung
    • Journal of the Optical Society of Korea
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    • 제5권2호
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    • pp.43-48
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    • 2001
  • A three-dimensional (3D) display system based on computer-generated integral photography (CGIP) is proposed and its feasibility is discussed. Instead of the pickup process in conventional If, the elemental images of imaginary objects are computer-generated. Using these images, we observed autostereoscopic 3D images in full color and full parallax. The lateral and depth resolutions of the integrated images are limited by some factors such as the image position, object thickness, the lens width, and the pixel size of display panel.

Study of Three-Dimensional Display System Based on Computer-Generated Integral Photography

  • Lee, Byoung-Ho;Jung, Sung-Young;Min, Sung-Wook;Park, Jae-Hyeung
    • Journal of the Optical Society of Korea
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    • 제5권3호
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    • pp.117-122
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    • 2001
  • A three-dimensional (3D) display system based on computer-generated integral photography (CGIP) is proposed and its feasibility is discussed. Instead of the pickup process in conventional IP, the elemental images of imaginary objects are computer-generated. Using these images, we observed autostereoscopic 3D images in full color and full parallax. The lateral and depth resolutions of the integrated images are limited by some factors such as the image position, object thickness, the lens width, and the pixel size of display panel.

완전시차 집적 영상 배경을 가지는 2D-3D 겸용 디스플레이 시스템 (2D-3D convertible display system having a background of full-parallax integral images)

  • 홍석표;신동학;김은수
    • 한국정보통신학회논문지
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    • 제13권2호
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    • pp.369-375
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    • 2009
  • 본 논문에서는 완전 시차 배경 영상을 가지는 새로운 형태의 2D-3D 겸용 디스플레이 시스템을 제안한다. 제안하는 시스템의 집적 영상 시스템과 기존의 2D 평면 디스플레이 구성이 되며, 3D 모드와 2D 모드에서 구동이 가능하다. 3D 모드에서는 집적 영상 기술을 이용하여 배경영상을 만들어서 주요 영상과 결합함으로써 3D 영상을 만든다. 2D 모드에서는 집적영상 시스템이 2D 평면 디스플레이의 백라이트 역할을 수행하고 2D 평면 디스플레이에 2D 영상이 표시된다. 제안하는 방법의 유용함을 보이기 위해서 기초 실험을 수행하고 성공적인 실험 결과를 보고한다.

자동차 에어컨 비정상과정 시뮬레이션 (Transient Simulation of an Automotive Air-Conditioning System)

  • 오상한;원성필
    • 설비공학논문집
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    • 제13권11호
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    • pp.1089-1096
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    • 2001
  • The cool-down performance after soaking is very important in an automotive air-conditioning system and is considered as the key design variable. Therefore, understanding of the overall transient characteristics of the system is essential to the preliminary design as well as steady-state characteristics. The objective of this study is to develop a computer simulation model and estimate theoretical1y the transient performance of an automotive air-conditioning system. To accomplish this, a mathematical modelling of each component, such as compressor, condenser, expansion valve, and evaporator, is presented first of all. For a detailed calculation, condenser and evaporator are divided into many subsections. Each sub-section is an elemental volume for modelling. In models of expansion valve and compressor, dynamic behaviors are not considered in an attempt to simplify the ana1ysis, but the quasi-static ones are just considered, such as the relation between mass flow rate and pressure drop in expansion device, polytropic process in compressor, etc. The developed simulation model is validated with a comparison to laboratory test data of an automotive air-conditioning system. The overall time-tracing properties of each component agreed fairly well wish those of test data in this case.

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Development of Near-Critical Water Reaction System for Utilization of Lignin as Chemical Resources

  • 엄희준;홍윤기;박영무;정상호;이관영
    • 한국신재생에너지학회:학술대회논문집
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    • 한국신재생에너지학회 2010년도 춘계학술대회 초록집
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    • pp.251.2-251.2
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    • 2010
  • Plant biomass has been proposed to be an alternative source for petroleum-based chemical compounds. Especially, phenolic chemical compounds can be obtained from lignin by chemical depolymerization processes because lignin consists of complex aromatic polymer such as trans-p-coumaryl, coniferyl and sinapyl alcohols, etc. Phenolic chemical compounds from lignin were usually produced in super critical water. However, we applied Near-critical water (NCW) system because NCW is known as a good solvent for lignin depolymerization. Organic matter like lignin can be solved in NCW system and the system has a unique acid-base property without conventional non-eco-friendly chemicals such as sulfuric acid and sodium hydroxide. In this work, we tried to optimize the NCW depolymerization system by adjusting the processing variables such as reaction time, temperature and pressure. Moreover, the amount of additional phenol was optimized by changing the molar ratio between water and phenol. Phenol was used as capping agent to prevent re-polymerization of active fragment such as formaldehyde. Alkali-lignin was used as a starting material and characterized by a Solid State 13C-NMR, FT-IR and EA (Elemental Analysis). GC-MS analysis confirmed that o-cresol, p-cresol, anisole and 4-hydroxyphathalic acid were the main product and they were quantitatively analyzed by HPLC.

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