• 제목/요약/키워드: Electrophoretic Deposition

검색결과 126건 처리시간 0.066초

Effect of silver oxide additions on YBCO thick film properties

  • Soh, Dea-Wha;Li, Ying-Mei;Cho, Yong-Joon;Korobova, N.
    • 한국전기전자재료학회:학술대회논문집
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    • 한국전기전자재료학회 2001년도 추계학술대회 논문집 Vol.14 No.1
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    • pp.81-84
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    • 2001
  • The effect of silver oxide (14 wt.%) addition to YBCO compounds and electrophoretic deposition of composite particles prepared by solid phase reaction have been investigated. The results were compared with those for as-processed samples with YBCO films on Ag wire substrate. Our experiments show that the adhesion, microstructure changes, superconducting properties of these films is sensitive to the silver content and sintering conditions. Adding a small amount of PEG tends to remove cracks in the YBCO and (YBCO + Ag) films, which develop during the heating process. An attempt has been made to explain the experimental observations regarding variation of critical current density with the YBCO and (YBCO + Ag) films.

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전기영동법에의해 제작된 Pl 박막의 표면처리 조건이 감습 특성에 미치는 영향 (The effect of surface treatment of Pl Thin Film Prepared by Electrodporetic method on the characteristics of Humidity Sensing)

  • 정승용;김종석;박강식;한상옥;이덕출
    • 대한전기학회:학술대회논문집
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    • 대한전기학회 1997년도 하계학술대회 논문집 C
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    • pp.1531-1533
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    • 1997
  • We prepared polyimide film by electrophoretic deposition onto glass film as a sensing materials of humidity, and treated with plasma discharging as a function of discharging power to improve performance of the sensor. Then evaluated the characteristics of polyimide on humidity.

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${B_2}{O_3}$가 전기영동법으로 제조된 형광막의 접착력에 미치는 영향 (Effect of ${B_2}{O_3}$on the Adhesion Properties of Electrophoretically Deposited Phosphor Films)

  • 오승목;이현덕;강태식;김강진;변재동
    • 한국세라믹학회지
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    • 제37권9호
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    • pp.927-932
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    • 2000
  • Mg(NO$_3$)$_2$가 용해된 IPA 용액에서 형광 분말의 전기영동법에 의한 증착 과정을 증착 시간, Mg(NO$_3$)$_2$의 농도 및 열처리 조건에 따라 분석하였다. 전기영동법으로 가장 두께가 균일한 형광막을 얻기 위한 Mg(NO$_3$)$_2$의 최적 농도는 $10^{-3}$~$10^{-4}$ M였다. 형광체의 접착력을 향상시키기 위해 새로운 방법을 고안하였다. 즉 전기영동법으로 증착된 형광막에 B$_2$O$_3$가 용해된 IPA 용액을 분사한 후 열처리를 하였다. 그 결과 기존의 PL 특성을 그대로 유지하면서 접착력을 향상시킬 수 있었다. 그러나 CL 휘도는 약간 감소하였다.

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Non-cracking YBCO Films on Silver Wire

  • Soh, Dea-Wha;Korobova, N.;Li, Young-Mae
    • 동굴
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    • 제76호
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    • pp.1-13
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    • 2006
  • Electrophoretic deposition (EPD) of alcohol YBCO suspensions on the Ag wire electrode is studied. Poly(ethylene glycol) was coordinated to a structure formed by the EPD process with YBCO particles. The suspension is characterized in terms of zeta potential and conductivity. The d.c electric fields of 200-300 V/cm are applied for 1-10 min. The optimal condition for the EPD allows modifying the properties and microstructure of the deposited films. Superconducting coatings with nanometer-sized pores and a preferred orientation along the c-axis were prepared from the result with chemically modified precursor solution. In contrast, YBCO coatings of submicrometer-sized pores and randomly orientated grains were prepared from the solution without PEG.

폴리이미드 박막을 이용한 습도 센서의 개발에 관한 연구 (A Study on The Development of Humidity Sensor Using Polyimide Film)

  • 정광희;조동헌;이병성;정병기;한상옥;김용락;박강식;김종석
    • 대한전기학회:학술대회논문집
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    • 대한전기학회 1994년도 하계학술대회 논문집 C
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    • pp.1233-1235
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    • 1994
  • In this work, polyimide thin films fabricated by the electrophoretic deposition are investigated as a humidity sensing material. Capacitance and impedance are measured with increasing relative humidity to find the nature of the film. From the results, the polyimide humidity sensor is not classified impedance change type but capacitance change type and appear more sensitive in the region of higher humidity than that of lower humidity.

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Effect of silver oxide additions on YBCO thick film properties

  • Soh, Dea-Wha;Li, Ying-Mei;Cho,Yong-Joon;N., Korobova
    • 한국전기전자재료학회:학술대회논문집
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    • 한국전기전자재료학회 2001년도 추계학술대회 논문집
    • /
    • pp.81-84
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    • 2001
  • The effect of silver oxide (14 wt.%) addition to YBCO compounds and electrophoretic deposition of composite particles prepared by solid phase reaction have been investigated. The results were compared with those for as-processed samples with YBCO films on Ag wire substrate. Our experiments show that the adhesion, microstructure changes, superconducting properties of these films is sensitive to the silver content and sintering conditions. Adding a small amount of PEG tends to remove cracks in the YBCO and (YBCO + Ag) films, which develop during the heating process. An attempt has been made to explain the experimental observations regarding variation of critical current density with the YBCO and (YBCO + Ag) films.

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PEG 첨가에 의한 YBCO 후막 표면 변화 (Influence of PEG addition on the surface properties of YBCO Thick Films)

  • 소대화;전용우;조용준;코로보바 나탈리아
    • 한국전기전자재료학회:학술대회논문집
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    • 한국전기전자재료학회 2003년도 춘계학술대회 논문집 센서 박막재료 반도체 세라믹
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    • pp.53-56
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    • 2003
  • The properties of YBCO thick film coated on Ag wire with YBCO powder is deeply affected by cracking on its surface which was deposited in organic solution by electrophoretic method. YBCO superconducting thick films were prepared on Ag wire$({\Psi}0.8mm)$ by electrophoresis in acetone with added PEG (Poly-Ethylene Glycol, 3% in Acetone), 1ml for being crack-free. The surface properties of YBCO superconducting wire was evidently improved with adding PEG. Added PEG which molecular weight is 600, 1000, 3400 was affected with variation of deposition voltages to the surface properties of samples. As a result, with adding PEG (its molecular weight is 3400), YBCO superconducting wire was better on its surface properties.

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Preparation of Crack-free HTS YBCO Films by EPD Method

  • Soh, Dea-Wha;Li Yingmei;Nataly Korobova
    • Transactions on Electrical and Electronic Materials
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    • 제4권5호
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    • pp.6-9
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    • 2003
  • Electrophoretic deposition (EPD) of alcohol YBCO suspensions on the Ag wire electrode is studied. Polyethyleneglycol was coordinated to a structure formed by the EPD process with YBCO particles. The d.c electric fields of 200-300 V/cm are applied for 1-10 min. The optimal condition for the EPD allows modifying the properties and microstructure of the deposited films. Superconducting coatings with nanometer-sized pores and a preferred orientation along the caxis were prepared from the result with chemically modified precursor solution. In contrast, YBCO coatings of submicrometer-sized pores and randomly orientated grains were prepared from the solution without PEG.

음극 전기영동법에 의해 제조된 구리/탄소 나노입자 하이브리드 복합재료의 전기적/기계적 특성 평가 (Electrical and Mechanical Properties of Cu/Carbon Nano-Particle Hybrids Composites by Cathodic Electrophoresis)

  • 이원오;이상복;최오영;이진우;변준형
    • 대한금속재료학회지
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    • 제48권12호
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    • pp.1130-1135
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    • 2010
  • Cu/carbon nano-particle hybrids were fabricated through the cathodic electrophoretic deposition (EPD) process. CNT and CNF nano-particles were modified to give positive charges by polyethyleneimine (PEI) treatment before depositing them on the substrate. Since a Cu plate was used as an anode in the EPD process, Cu particles were also deposited along with the carbon nano-particles. Experimental observation showed the nano-hybrids constructed a novel formicary-like nano-structure which is strong and highly conductive. Utilizing the hybrids, carbon fiber composites were manufactured, and their electrical conductivity and interlaminar shear strength were measured. In addition, the deposition morphology and failure surface were examined by SEM observations. Results demonstrated that the electrical conductivities in the through-the-thickness direction and the interlaminar shear strength significantly increased by 350~2100% and 14%, respectively.

전기영동법으로 알루미늄에 침적된 영가 철 나노입자에 의한 질산성 질소의 환원 (Reduction of Nitrate-Nitrogen by Zero-valent Iron Nanoparticles Deposited on Aluminum yin Electrophoretic Method)

  • 류원선
    • 청정기술
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    • 제15권3호
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    • pp.194-201
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    • 2009
  • 최근 주요 수질오염 물질로 대두되고 있는 질산성 질소의 제거를 목적으로 영가 철 나노입자에 의한 질산성 질소의 환원반응성을 평가하였다. 영가 철 나노입자의 제조방법에 따른 반응성 차이를 규명하기 위해 유기용매 상에 계면활성제를 첨가하여 나노미터 크기 수준의 수용액 분산상에서 입자를 합성하는 마이크로에멀젼 방법과, 수용액 상의 철 이온을 환원시켜 입자를 합성하는 두 가지 방법으로 영가 철 나노입자를 합성하였다. 또한 전기영동법으로 알루미늄에 침적시킨 영가 철 나노입자에 의한 질산성 질소 제거속도를 측정하고, 고정화되지 않은 나노 철 입자에 의한 반응속도와 비교하였다. 환원반응을 질산성 질소에 대한 1차 반응으로 가정하여 수용액 방법 및 마이크로에멀전 방법으로 제조된 영가 철 나노입자의 반응성을 평가한 결과, 반응속도상수는 각각 $1.40{\times}10^{-2}min^{-1}$$3.49{\times}10^{-2}min^{-1}$ 로서 비표면적에 비례하여 증가하였다. 알루미늄에 침적된 나노입자는 현탁된 나노입자의 반응과 비교하여 약 30% 감소된 반응속도를 보였으나, 과량의 질산성 질소가 존재하는 경우 나노 철의 단위 질량당 질산성 질소의 제거효율 면에서 더 우수한 특성을 보였다. 나노철 입자의 현탁액은 반응시간 30분 이내에 반응속도가 감소하는 경향을 보였으나, 알루미늄에 침적된 나노철 입자는 3시간 이상 활성을 유지하였으며, 최종 생성물로 기체 질소를 발생시키는 것을 확인하였다.