• Title/Summary/Keyword: EDS analysis

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Capsule Train Dynamic Model Development and Driving Characteristic Analysis Considering the Superconductor Electrodynamic Suspension (초전도 유도 반발식 부상특성을 고려한 캡슐트레인 동특성 해석 모델 구축 및 주행 특성 분석)

  • Lee, Jin-Ho;Lim, Jungyoul;You, Won-Hee;Lee, Kwansup
    • Journal of the Korea Academia-Industrial cooperation Society
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    • v.21 no.7
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    • pp.38-45
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    • 2020
  • A magnetically levitating capsule train, which runs inside the sub-vacuum tube, can reach ultra-fast speeds by dramatically reducing the aerodynamic drag and friction. The capsule train uses the superconductor electrodynamic suspension (SC-EDS) method for levitation. The SC-EDS method has advantages, such as a large levitation gap and free of gap control, which could reduce the infra-construction cost. On the other hand, disadvantages, such as the large variation of the levitation-guidance gap and small damping characteristics in levitation-guidance force, could degrade the running stability and ride comfort of the capsule train. In this study, a dynamic analytical model of a capsule train based on the SC-EDS was developed to analyze the running dynamic characteristics. First, as important factors in the capsule train dynamics, the levitation and guidance stiffness in the SC-EDS system were derived, which depend non-linearly on the velocity and gap variation. A 3D dynamic analysis model for capsule trains was developed based on the derived stiffness. Through the developed model, the effects of the different running speeds on the ride comfort were analyzed. The effects of a disturbance from infrastructure, such as the curve radius, tube sag, and connection joint difference, on the running stability of the capsule train, were also analyzed.

Intermetallic Formation between Sn-Ag based Solder Bump and Ni Pad in BGA Package (BGA 패키지에서 Sn-Ag계 솔더범프와 Ni pad 사이에 형성된 금속간화합물의 분석)

  • Yang, Seung-Taek;Chung, Yoon;Kim, Young-Ho
    • Journal of the Microelectronics and Packaging Society
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    • v.9 no.2
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    • pp.1-9
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    • 2002
  • The intermetallic formation between Sn-Ag-(Cu) solders and metal pads in a real BGA package was characterized using SEM, EDS, and XRD. The intermetallic phase formed in the interface between Sn-Ag-Cu and Au/Ni/Cu pad is likely to be ternary compound of $(Cu,Ni)_6Sn_5$ from EDS analysis High concentration of Cu was observed in the solder/Ni interface. XRD analysis confirmed that $\eta -Cu_6 Sn_5$ type was intermetallic phase formed in the interface between Cu containing solders and Ni substrates and $Ni_3$Sn_4$ intermetallic was formed in the Sn-Ag solder/Ni interface. The thickness of intermetallic phase increased with the reflow times and Cu concentration in solder.

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A Study of Penetration Depth into Ceiling Materials containing Asbestos according to Dilution Rate of Scattering Prevention Agent (석면 함유 천장재의 안정화제 희석에 따른 침투깊이 연구)

  • Shin, Hyungyoo;Choi, Youngkue;Jeon, Boram;Ha, Jooyeon
    • Journal of Korean Society of Occupational and Environmental Hygiene
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    • v.25 no.1
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    • pp.82-88
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    • 2015
  • Objectives: This study is designed to analyze the penetration performance into ceiling materials containing asbestos of scattering prevention agents and investigate the change in penetration depth and viscosity according to the dilution rate of anti-scattering agents diluted with distilled water. Methods: Five different types of scattering prevention agents were spread on plate-type asbestos ceiling materials. The penetration depth of each coated ceiling material was measured by energy dispersive spectroscopy (EDS) analysis, based on X-ray fluorescence (XRF) results of the non-coated ceiling materials. Test equipment installed the ceiling materials and 60 minutes were collected at a flow rate of $10{\ell}/min$ at a filter of 25 mm. Results: An EDS analysis of the cross-section of ceiling materials constructed with a scattering prevention agent revealed that potassium is detected in the process of penetrating hardener solidification and this element could be an indicator for infiltration. When anti-scattering agents with different viscosities were constructed and the penetration depth was analyzed by potassium detection assessment using EDS, the depth results with viscosities of 5.0, 2.5, and 1.9 cP were 98.5, 103, and $147{\mu}m$, respectively. Penetration performance improved with decrease in viscosity. Conclusions: For asbestos ceiling materials, it is concluded that a higher dilution rate of the scattering prevention agent leads to lower viscosity, and hence a deeper penetration depth from $156{\mu}m$ to 3 mm. The asbestos anti-scattering properties according to the penetration depth will be confirmed through further study.

Mineral content analysis of root canal dentin using laser-induced breakdown spectroscopy

  • Eren, Selen Kucukkaya;Uzunoglu, Emel;Sezer, Banu;Yilmaz, Zeliha;Boyaci, Ismail Hakki
    • Restorative Dentistry and Endodontics
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    • v.43 no.1
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    • pp.11.1-11.10
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    • 2018
  • Objectives: This study aimed to introduce the use of laser-induced breakdown spectroscopy (LIBS) for evaluation of the mineral content of root canal dentin, and to assess whether a correlation exists between LIBS and scanning electron microscopy/energy dispersive spectroscopy (SEM/EDS) methods by comparing the effects of irrigation solutions on the mineral content change of root canal dentin. Materials and Methods: Forty teeth with a single root canal were decoronated and longitudinally sectioned to expose the canals. The root halves were divided into 4 groups (n = 10) according to the solution applied: group NaOCl, 5.25% sodium hypochlorite (NaOCl) for 1 hour; group EDTA, 17% ethylenediaminetetraacetic acid (EDTA) for 2 minutes; group NaOCl+EDTA, 5.25% NaOCl for 1 hour and 17% EDTA for 2 minutes; a control group. Each root half belonging to the same root was evaluated for mineral content with either LIBS or SEM/EDS methods. The data were analyzed statistically. Results: In groups NaOCl and NaOCl+EDTA, the calcium (Ca)/phosphorus (P) ratio decreased while the sodium (Na) level increased compared with the other groups (p < 0.05). The magnesium (Mg) level changes were not significant among the groups. A significant positive correlation was found between the results of LIBS and SEM/EDS analyses (r = 0.84, p < 0.001). Conclusions: Treatment with NaOCl for 1 hour altered the mineral content of dentin, while EDTA application for 2 minutes had no effect on the elemental composition. The LIBS method proved to be reliable while providing data for the elemental composition of root canal dentin.

Fatigue Strength in Aged Turbine Rotor Steel (시효 열화시킨 터빈 로터강의 피로강도에 관한 연구)

  • 서창민;허정훈;이해무;서덕영
    • Journal of Ocean Engineering and Technology
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    • v.10 no.2
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    • pp.77-87
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    • 1996
  • The estimation of the remaining life for the aged components in power plant as well as chemical and peroleum plants has been recently coberned. The raw materials used in this syudy are the 1Cr-1Mo-0.25V rotor steel which intensified P and S compositions along with the nominal compositions of ASTM A470 standard. Five kinds of specimens with the different degradation levels were prepared by isothermal aging teat treatment at $630^{\circ}C$ The mechanical properties and fatigue strength of virgin and aged 1Cr-1Mo-0.25V rotor steel have been inbestigated through the hardness, tensile, fatigue test, SEM fractograph and EDS analysis at room temperature. Thus, the data of aged specimens were compared with those of virgin specimen to evaluate the aging effects. The main results obtained in this study are as follows; The decrease of the hardness due to degradation was distinguished until 50, 000hrs simulated service time. And is was confirmed that the considerable amount of P, Mn, Cr and S was precipitated at the grain boundary of aged material through the SEM and EDS analysis. The fatigue strength of 25, 000, 50, 000, 75, 000 and 100, 000hrs aged material was decreased 29.5%, 24.4%, 28.6%, 35.7% than that of virgin material at $10^7$ cycles of room temperature. The major cracks of virgin and aged materials initiated at the inclusions including Si, P and Mn compositions which were located at the outer periphery of the specimen.

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Confirmation of Long-term stability on THPP using thermodynamic and kinetic analysis (열역학적 및 속도론적 분석을 통한 THPP의 노화 안정성 확인)

  • Lee, Junwoo;Kim, Sangwon;Choi, Kyoungwon;Lee, Seung Bok;Ryu, Byungtae;Park, Taiho
    • Proceedings of the Korean Society of Propulsion Engineers Conference
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    • 2017.05a
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    • pp.513-516
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    • 2017
  • When stored for long periods in a powder-based device (PMD), the explosive power in the device is aged and the explosive power is changed. Thus, The gunpowder used in the PMD must be chemically and physically stable for both internal and external factors. Since $BKNO_3$ and THPP are used as representative gunpowder, thermodynamic and kinetic analyzes were performed based on these gunpowders. Differential scanning calorimeter (DSC) was used to analyze the calorific value and reaction rate. As a result, there was no significant change in caloric value and reaction rate in THPP. In addition, XPS and TEM-EDS analyzes were performed to confirm the formation of oxide films directly related to aging, and no oxide films were observed as a result of thermal analysis. In addition, XPS and TEM-EDS analyzes were performed to confirm the formation of oxide films directly related to aging. As a results, no oxide films were observed. It can be concluded that THPP is the most famous gunpowder in terms of long-term stability.

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Two Dimensional Gold Nanodot Arrays Prepared by Using Self-Organized Nanostructure

  • Jung Kyung-Han;Chang Jeong-Soo;Kwon Young-Soo
    • Journal of Electrical Engineering and Technology
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    • v.1 no.2
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    • pp.246-250
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    • 2006
  • Highly ordered gold nanodot arrays have been successfully obtained by vacuum evaporation using an anodic aluminum oxide (AAO) as a shadow mask. An AAO mask with the thickness of 300 um was prepared through an anodization process. The structure of the nanodot arrays was studied by a field- emission scanning electron microscope (FE-SEM) equipped with an energy dispersive spectrometer (EDS). A tapping mode atomic force microscope (AFM) was employed for studies of height and phase feature. The nanodot arrays were precisely reproduced corresponding to the hexagonal structure of the AAO mask in a large area. In the gold nanodot arrays, the average diameter of dots is approximately the same as the AAO pore size in the range from 70 um to 80 nm and 100 nm center-to-center spacing. EDS analysis indicated that the gold dots were almost entirely consisted of gold, a highly demanded material.

Asbestos Analysis of China Sepiolite by Transmission Electron Microscopy (중국산 해포석 내 석면 함유 유무 분석)

  • Song, Se Wook;Chung, Yong Hyun;Han, Jeong Hee
    • Journal of Korean Society of Occupational and Environmental Hygiene
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    • v.23 no.3
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    • pp.205-211
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    • 2013
  • Objectives: 21 sepiolite substances produced in China were investigated for the presence of asbestos in their materials. Materials and methods: In order to identify asbestos in sepiolite substances, test materials were analyzed using a transmission electron microscope equipped with energy dispersive X-ray spectrometer (TEM-EDS) for confirming their shape and components (atomic %). Results: Five of 21 sepiolte substances were asbestos-containing materials. Two chrysotile containing sepiolite proved to be asbestoscontaining materials, as did two chrysotile mixed with tremolite containing sepiolite. 16 sepiolite substances did not contain asbestos materials. Conclusions: When importing sepiolite substances, they must be analyzed to determine if there is asbestos in their materials.

황동볼트 손상원인 분석사례

  • Jeong, Nam-Geun
    • 열병합발전
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    • s.30
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    • pp.21-25
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    • 2002
  • According to recent Korea Electric Power Company report, yearly distribution line brass cramp bolts failure summed up to 4,400 cases emerging as one of main local break-down causes. Naturally, the need for the investigation was proposed To determine the root cause of the cramp bolt failures, mechanical and metallurgical investigation were performed for 90 samples which collected from various sites. For the understanding of the geometric characteristics, stress distribution was evaluated by CAE program and proof load of each bolts was tested. The SEM&EDS was used for metallurgical investigation. Through the investigation, the root causes of failures were confirmed. All damaged bolts showed intergrannular fracture mode and the all fractured bolt showed ß phase morphology contrast to the a&ß mixture morphology of the non-damaged samples. Additionally, EDS analysis confirmed the existence of lead rich layer on grain boundaries.

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Analysis of magnetic forces for dynamic characteristics of electrodynamic Maglcv Systcm (반발식 자기부상열차의 동특성해석을 위한 전자력계산)

  • 홍순흠;한송엽;차귀수
    • Journal of the Korean Magnetics Society
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    • v.4 no.2
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    • pp.106-113
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    • 1994
  • This paper deals with the magnetic forces of the combined levitation and guidance EDS(Electrodynamic Suspension) maglev system when the car bogie is tilted by the roll, pitch and yaw. The end effect on the magnetic forces are considered by calculating the air-gap flux without the assumptions for its pattern. Induced voltages and currents of the ground coils are given as results. The restoring torque due to roll, pitch and yaw of the bogie body are also examined. It has been shown that the end effect of the concentrically loaded vehicle are not negligible and the combined EDS is stable maglev system against disturbing forces.

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