• Title/Summary/Keyword: EDS분석

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Fault Diagnosis of M.tr using Acoustic Sensor Technique (초음파 기술을 이용한 변압기 이상상태 진단)

  • Jeong, Jae-Ki;Yoon, Si-Young;Kang, Chang-Ik;Jin, Young-Eun
    • Proceedings of the KIEE Conference
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    • 2007.07a
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    • pp.744-745
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    • 2007
  • 변압기를 진단하는 분석 요소 중 흔히 사용하는 방법으로 유중가스분석을 이용하는 방식을 많이 사용하고 있다. 유중가스 분석은 변압기 내 Oil이 열과 Arc등에 의해 화학적으로 변화된 것을 측정하여 열화 정도를 추정하는 방식이지만 신속한 검출 및 위치추정이 불가능하다는 단점이 있다. 신속한 검출이 되지 않으면 신속한 보고가 이루어 질 수 없으므로 변압기 교체시점을 맞추지 못하여 사고로 인한 막대한 피해보상이 발생한다. 이런 단점을 보완하기 위해 변압기내 부분방전 및 Arc에 의해 발생하는 부분방전신호를 초음파 대역에서 검출하여 열화 및 위치를 추정할 수 있는 초음파 분석이 필요하게 되었고 실험을 통해 변압기에 대한 분석, 진단을 시행하였다.

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PEG Distribution in the Cell Walls of PEG-treated Woods using SEM-EDS (SEM-EDS를 이용한 PEG처리재 세포벽내의 PEG분포 분석)

  • Kwon, Gu-Joong;Kim, Nam-Hun
    • Journal of the Korean Wood Science and Technology
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    • v.34 no.4
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    • pp.9-14
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    • 2006
  • This study was carried out to investigate the distribution and penetration of PEG molecules into the cell wall of wood by SEM-EDS method. SEM observation indicated that the cell walls of PEG-treated specimen were swollen, and didn't show any change in their shapes, while the cells of untreated specimen were more or less collapsed. The results of X-ray analyses of potassium stained samples revealed the distribution of the impregnated chemicals within the cell walls, when considering the distribution of potassium ions in the cell walls. Consequently, this study supported the possibility of PEG molecules penetrated into the wood cell wall play an important role in enhancing the dimensional stability of wood.

Model Development of Event Detection System Software in Water Distribution Networks (상수관망 수리이상감지시스템 SW(K-EDS) 모델 개발)

  • Noh, Joon Woo;Shin, Eun Her;Yoo, Do Guen
    • Proceedings of the Korea Water Resources Association Conference
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    • 2017.05a
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    • pp.270-270
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    • 2017
  • 스마트워터그리드와 같은 첨단 정보통신기술을 활용한 물 관리 기술의 도입으로 수도운영사업에서도 누수와 같은 이상사건인지 목적의 효율적 빅 데이터 분석기법의 중요성이 증대되고 있다. 국내외적으로 누수인지를 위한 다양한 연구기법, 범위, 계측항목, 샘플링 주기 등이 제시된 바 있으나, 이상감지시스템(Event Detection System, EDS)은 대상지역 특정적 특성을 가지고 있어 범용적인 모델을 구축하는 데는 어려움이 있다. 본 연구에서는 소블럭 단위의 유량자료 분석을 통한 이상감지시스템의 적용가능여부를 판별하고 적합 모델구축자료 방안을 제시하는 K-EDS 모델을 개발하였다. 모델분석의 절차는 자료획득, 자료 전처리, 탐색적 자료해석, 그리고 각 기법 평가로 진행된다. 개발된 모델을 다양한 특성을 가지는 실제 지방상수도시스템에 적용하여 분석하였으며, 최종적으로 모델적용 가능성과 영향인자 등을 도출하였다. 개발된 모델은 소블럭별 현장계측자료 기반의 이상감지모델 적용 적합도 판별에 활용될 수 있으며, 향후 누수 인지 및 누수지속시간 감소를 위한 SW로 개발이 가능하다.

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Spectroscopic Evaluation on the Chemical Damage of Hair by Hydrogen Peroxide (과산화수소에 의한 모발의 화학적 손상에 관한 분광학적 평가)

  • Ha, Byung-Jo
    • Applied Chemistry for Engineering
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    • v.22 no.5
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    • pp.579-581
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    • 2011
  • Spectroscopic evaluation of hair chemical damage was performed by SEM/EDS, CLSM, and FT-IR spectroscopy. In SEM/EDS, hydrogen peroxide treated hair showed the loose packing of surface scales, lower ratio of sulfur element and higher ratio of oxygen atom. In the optical single section by using CLSM, high fluorescent intensity appeared in untreated hair. However, in case of treated hair, low fluorescent intensity appeared. This results the aromatic amino acids which can be autofluorescent were more abundant than bleached hair. FT-IR spectra showed that cysteic acid band intensity was increased by performing the bleaching treatments. These results indicate that the oxidative damage cleaves the S-S bond and results in the lower working force of hair fiber.

Determination of Thin Film Thickness by EDS Analysis and its Modeling (EDS 분석과 모델링에 의한 박막두께 측정 방법에 관한 연구)

  • Yun, Jae-Jin;Lee, Won-Jong
    • Journal of the Korean Institute of Electrical and Electronic Material Engineers
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    • v.24 no.8
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    • pp.647-653
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    • 2011
  • In this study, a method to measure the thickness of thin film by EDS (energy dispersive spectroscopy) is suggested. We have developed a model which calculates the thickness of thin film from the characteristic x-ray intensity ratio of the elements in thin film and substrate by considering incident electron beam energy, x-ray generation curve, backscattering and absorption of x-ray, take-off angle of x-ray and tilt angle of the sample. We obtained the relation curve between the film thickness measured experimentally and the x-ray intensity ratio of elements. The film thicknesses calculated from the model agrees quite well with those measured experimentally. Therefore, the thin film thickness can be measured rapidly and accurately by using the model developed in this study and the x-ray intensity ratio obtained in EDS analysis.

The interfacial reaction between Sn-based lead-free solders and Pt (Sn-base 무연솔더와 Pt층의 계면반응에 대한 연구)

  • 김태현;김영호
    • Proceedings of the International Microelectronics And Packaging Society Conference
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    • 2003.11a
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    • pp.76-79
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    • 2003
  • 본 실험에서는 $S0.7wt\%Cu,\;Sn3.8wt\%Ag0.7wt\%Cu$ solder와 금속층으로서의 좋은 특성을 가지고 있지만 아직 연구 보고 된 적 없는 Pt층과의 리플로 반응에 의해 형성되는 계면금속간화합물의 상 분석을 시도 하였다 또한 솔더내 Cu함량에 따른 계면금속간화합물의 변화에 대하여 연구하기 위해 $Sn1.7wt\%Cu$솔더와 Pt층의 계면반응 현상에 대한 연구도 수행하였다. $Sn0.7(1.7)wt\%Cu$솔더는 순수한 Sn과 Cu를 이용하여 중량비로 제조하였고, $Sn3.8wt\%Ag0.7wt\%Cu$솔더는 솔더페이스트를 사용하였다. 분석은 SEM, EDS, XRD를 이용하였다. 분석 결과 세 가지 무연솔더 모두에서 $PtSn_4$가 계면 금속간화합물로 존재함을 발견하였으며 $1.7wt\%Cu$를 포함한 솔더와 Pt와의 반응에서는 고용도 이상으로 첨가된 Cu에 의해 솔더 내부에 조대한 형상의 $Cu_6Sn_5$가 존재함을 SEM 및 EDS분석을 통하여 발견 하였다.

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Defect analysis of fabricated glass by passive pot furnace (수동 도가니로에서 제조된 유리제품내 결함 분석)

  • 윤태민;윤영진;이용수;강원호
    • Proceedings of the KAIS Fall Conference
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    • 2002.05a
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    • pp.70-73
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    • 2002
  • 도가니로를 사용하여 유리제품을 생산하고있는 중소 유리제조업체인 D.H사의 제품내 발생한 결함을 분석하였다. 제품내 결함으로는 기포, 코드(cord), 석물(stone)이 발생하고 있었으며, 광학현미경, EDS 등의 분석장비를 통해 제품내 결함을 분석한 결과 코드는 석물에 의해 발생하고 있음을 확인하였다. 석물의 EDS 분석결과 주요성분은 Si로 나타났으며, 이는 도가니의 장기간 사용시 도가니 내벽과 유리물의 반응에 의한 도가니의 용융침식에 의해 발생한 한가지 결점원에 의한 한가지 결정상으로 SiO₂의 고온결정상인 cristobalite임을 확인할 수 있었다.

Analysis of Path Model Based on Objectification Theory for College Women's Eating Disorder Symptomatology (대상화이론에 근거한 여대생의 섭식장애증상 경로모형 분석)

  • Lee, Eun-Joo
    • Women's Health Nursing
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    • v.16 no.1
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    • pp.78-86
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    • 2010
  • Purpose: This study was to examine the fitness of a path model based on the objectification theory and to expand it by including the new variables to explain eating disorder symptomatology (EDS). Methods: The subjects consisted of 444 college women. Data was collected through self-report questionnaires that measured self-objectification (SO), social physique anxiety (SPA) and EDS as the original variables in the objectification theory, and influence of mass media (IMM) and sex-role attitude (SRA) as the new variables. Data was analyzed by SPSS/WIN 12.0 and Amos 5.0 programs. Results: IMM and SRA showed direct effect on SO. IMM had direct and indirect effect on SPA and EDS. SRA had direct and indirect effect on EDS, but only indirect effect on SPA. SO and SPA influenced EDS directly, and SO influenced indirectly EDS. Conclusion: Path analyses indicated support for the original theory and the expanded theory. It is necessary for repeated studies including various age groups of women to clarify the applicability of the objectification theory to Korean women's eating disorders. And it were recommended that we should promote womens' criticism of the image and message about the perfect female body presented in the mass media, and to highlight the relationship of gender equality to women's eating disorders in health education.

Application of Spectrochemical Analysis in the Study of Archaeological Textiles (복식유물의 연구에 있어서 분광화학분석의 활용)

  • 안춘순
    • Journal of the Korean Society of Costume
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    • v.49
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    • pp.49-63
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    • 1999
  • This research utilized the Energy Dispersive X-ray Spectroscopy(EDS) and the Inductively Coupled Plasma Mass Spectrometry in the analysis of chemical elements present among the textiles exhumed from Kupori Hwasung-kun Kyunggi-do. The two research objectives were: first to examine the elements present and their percent presence in Kupori samples: second to investigate whether the elements are part of mordant substances which could have been used when dyeing the KUpori textiles in the past. To meet such research purposes standard silk fabric was dyed with Sophorajaponica using alum and iron mordants. For alum mordant unpurified general alum and potassium aluminum sulfate(AlK(SO4)2). iron sulfate(FeSO4·7H2O) were used, From the results of EDS and ICP-Mass analysis the following conclusions were drawn. 1 According to the EDS analysis 9 elements Ca, S, Al, Si, K, Fe, P, Mg and Na were detected. 2. ICP-Mass result of the mordant chemicas showed high amount of A, Al and k present in alum mordants and S and Fe present in iron mordants. 3. Comparison of the ICP-Mass results of the mordant chemicals and those of the standard dyed samples suggested that the amount presence of Al and Fe is a strong indication of the usage of alum and iron mordants respecticely in an unknown dyed textile. 4, In the washed Kupori textiles Fe showed a relatively higher rate of presence in the samples Therefore it can be conjectured that those Kupori textiles were dyed with iron mordant based on the result of the above number 3. 5. It is probable that the other elements detected from the Kupori samples were incorporated into the textiles as part of the soil debris produced from the degradation of the dead within the coffin or the earth debris. They can also be part of the inorganic compounds inherent in the silk textiles themselves before dyed. 6. Among the elements it is likely that Ca which showed a high degree of presence among the unwashed samples was part of the inorganic compound inferent in the silk textiles.

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