• Title/Summary/Keyword: Dye Test

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A STUDY ON THE MICROLEAKAGE OF RETROFILLED TEETH WITH VARIOUS MATERIALS AND INSTRUMENTS FOR CAVITY PREPARATION (역행충전시 와동형성 기구 및 수복재에 따른 변연누출에 관한 연구)

  • Lee, Jae-Yong;Cho, In-Ho;Hong, Chan-Ui;Shin, Dong-Hoon
    • Restorative Dentistry and Endodontics
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    • v.18 no.1
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    • pp.187-196
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    • 1993
  • The purpose of this study was to evaluate the microleakage of retrofilled teeth with various materials [non-zinc Amalgam, IRM, Ketac-silver, CGP(cold-burnished, ultrafil)[and instruments for cavity preparation. Root apex were resected 2mm from apex horizontally and class I cavities were prepared in 2mm denpth, 1.5mm width and were filled with above mentioned materials. Root apex were resected 2mm from apex horizontally and class I cavities were prepared in 2mm depth, 1. 5mm width and were filled with above mentioned materials. 2% methylene blue dye solution was used for 4 days immersion and the linear leakage was measured with calipers and the volumetric leakage was determined with a spectrophotometer. The results were as follows : 1. Amalgam group showed the greatest amount of leakage and Ketac-silver group showed the least value. 2. By linear leakage test, the group retrofilled with Ketac-silver, or CGP showed better seal than the group of Amalgam or IRM. This was shown in both retrograde tip and Conventional method. 3. By volumetric leakage test, the group retrofilled with Ketac-silver showed significantly better seal than the group with IRM in retrograde tip method. 4. By volumetric leakage test, the group retrofilled with Ketac-silver showed significantly better seal than the group with Amalgam in the Conventional method.

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Comparison of Mechanical Properties between Bulk-fill and Conventional Composite Resin (Bulk-fill과 Conventional 복합레진의 물성비교)

  • Seok, Ujeong;Kim, Jongbin;Kim, Kiseob;Kim, Jongsoo
    • Journal of the korean academy of Pediatric Dentistry
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    • v.43 no.4
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    • pp.427-434
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    • 2016
  • The aim of this study was to compare the mechanical properties of high viscosity bulk-fill resin composites, $Filtek^{TM}$ Bulk Fill Posterior Restorative (FBF) and $Tetric^{(R)}$ N-Ceram Bulk Fill (TBF), with conventional composite ($Filtek^{TM}$ Z-350 XT, Z-350). The Vickers hardness test which indicates the degree of conversion was performed and the dye penetration test was performed to measure the microleakage which indicates polymerization shrinkage amount. To minimize experimental error, the standardized 3D-printed molds and the bovine teeth were used. Obtained data were analyzed by the Kruskal-Wallis test and Mann-Whitney test with the confidence interval of 95%. In the microhardness test within 1 hour of polymerization, lower surface of FBF and TBF showed significantly lower value than that of Z-350 (p < 0.05). But after 24 hours, the microhardness of FBF had increased and showed no significant difference with Z-350 (p > 0.05). In top and 2 mm depth surface, mean microhardness values were in the following order: Z-350 > FBF > TBF (p < 0.05). The mean microleakage value of TBF was significantly lower than others (p < 0.05). For clinical application of bulk-fill resin composites, caution for applying masticatory forces during 24 hours after polymerization is advised and further studies to decrease microleakage should be conducted.

Hematuria among Benzidine Dye Industry Workers (벤지딘 염료공장 노동자들의 혈뇨)

  • Son, Mi-A.;Paek, Do-Myung;Choi, Jung-Kun;Park, Su-Kyeong;Park, Jung-Soon;Oh, Se-Min;Park, Jung-Sun;Park, Dong-Ook
    • Journal of Preventive Medicine and Public Health
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    • v.28 no.1 s.49
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    • pp.225-243
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    • 1995
  • Benzidine Industry in Korea has started after Japan has banned its production in early 1970's, and it has been in operation in Korea for over 20 years. However, it is not known yet whether any bladder cancer has developed from benzidine exposure. This study was done to screen benzidine-exposed workers for bladder cancer, and to examine the feasibility of employing screening test at the workplace. All the workplaces that manufacture or use benzidine for more than 20 years in Korea have been covered in this study, and they include 2 benzidine manufacturing factories, 5 benzidine using factories, as well as 2 benzidine free factories as an outside control. In total, 516 workers were screened with urine stick test and urine cytology test for the evidence of hematuria and abnormal urothelial cells. Each worker was also asked about risk factors and symptoms of bladder cancer including past medical history, smoking, medication and occupational history Benzidine in the air was measured by personal and area sampling. Out of 516 screened workers, 84(16.3%) workers showed positive hematuria in urine stick test, and 7(1.4%) workers showed degenerative cells in urine cytology tests. Those workers with abnormal urine test results who have been exposed to benzidine fo more than 10 years were further screened, and, in total, 23 workers were examined with intra-venous pyelography and cystoscopy. None of those screened had any evidence of bladder cancer When workers with only past hematuria history were included in the positive hematuria group, 96(18.5%) had positive hematuria. On the multiple logistic regression analysis, positive hematuria was significantly associated with benzidine exposure, history of other occupations with elevated bladder cancer risk, pyuria and glycosuria. The association got stronger as direct benzidine exposure was accounted through individual task analysis, and as exposure duration was accounted with tenure analysis. For those with benzidine exposure with more than 10 years of tenure, the odds of having positive hematuria was elevated 2.14(95%C.I is 1.08 to 4.25) times more than for those without exposure. Even though bladder cancer was not detected for several limitations including short observation period, majority of studied workers with short latency, healthy worker effect, and low sensitivity of single screening test in a cross-sectional study, the study results suggest that hematuria screening is a feasible and very useful test for bladder cancer screening among benzidine exposed workers.

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IN VITRO COMPARISON OF VARIOUS DIAGNOSTIC METHODS OF OCCLUSAL CAR10US LESIONS (교합면 우식병소의 다양한 진단법에 관한 비교연구)

  • Kim, Jae-Gon;Kim, Young-Jin;Kim, Young-Sin;Baik, Byeong-Ju
    • Journal of the korean academy of Pediatric Dentistry
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    • v.28 no.4
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    • pp.613-619
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    • 2001
  • The aims of this study were to compare the accuracy, sensitivity and specificity of cnventional visual examination, radiography and a new laser fluorescence method, KaVo Diagnodent, for the detection of occlusal caries lesions. One hundred sound human premolars and molars which had no restorations or interproximal cavities were tested by three methods. Tooth lesions depth was assessed at histologic examination using Caries detector dye The following results were obtained. 1. Diagnodent show 7.8 in sound tooth, 25.4 in initial caries, 30.5 in enamel caries, and 53.8 in dentin caries with average score 2. Spearman and Pearson relation coefficient was high between tooth-specimen test with dye and Diagnodent(0.736, 0.619), visual examination(0.664, 0.666), and was low between tooth-specimen test with dye and radiographic examination(P<0.01, total) 3. Accuracy of occlusal caries was highest on Diagnodent(65%) and lowest on radiographic examination(35%) 4. In initial caries, the sensitivity and specificity of Diagnodent method was the highest. In enamel caries, the sensitivity of visual examination was the highest and specificity of Diagnodent method was the highest. In dentinal caries, the sensitivity and specificity of Diagnodent method was the highest and sensitivity of visual examination was the lowest.

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Studies on the surface charge and coagulation characteristics of suspended particles in the aqueous phase (수용액상에서 부유 미립자의 표면전위와 응집특성에 관한 연구)

  • 박상원;김성국;홍대일
    • Journal of Environmental Science International
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    • v.8 no.3
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    • pp.363-369
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    • 1999
  • This study aimed to elucidate the relationship between theoretical parameters affecting the coagulation process and the real coagulation phenomenon applied to the dye wastewater. Emphasis was placed on the effective removal of the suspend particulates. Parameters studied in this study are pH, coagulant concentration and surface potential. Optimal dosages of coagulants by the measurement of the zeta potential at lower then $25^{\circ}C$ are 5\times$10^P-3}$ M of $FeCl_3 and 1.4\times10^{-6}M of Fe_2(SO_4)_3$. The results were well agreeded with the separate Jar-test results. Emphasis was also placed on the relationship between water quality and the content of SS. It was found that the COD and DOC were reduced to 65% and 85%, respectively. The turbidity at the above condition was reduced from 300 NTU to 0~1 NTU. Efforts were made to clarify the behavior of the suspend solid as affecting the water quality. 12,000~13,000 particles/10mL in $1~50\mu$m size range particulates in the raw wastewater were reduced to 300 particle/10mL in the same range after treatment. This research has proposed the methodology to find out the optimal condition of coagulation for small scale wastewater treatment plant or chemical coagulation process.

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Dyeing Characteristics of Heat-generating Acrylate/Dyeable Polypropylene Blended Knit (흡습발열 Acrylate/Dyeable Polypropylene 섬유 방적사 편물의 염색 특성)

  • Lee, Eui-jae;Park, Chae-eun;Kim, Keun-hyeong;Lee, Chang-seok;Choi, Jae-hong
    • Textile Coloration and Finishing
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    • v.29 no.1
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    • pp.1-10
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    • 2017
  • Blended knit with two or more fiber has various dyeing characteristics depending on dyeing method because of different material properties of them. In this paper, newly developed blended knit was used. It was composed by Acrylate fiber and Dyeable polypropylene(DPP) fiber. As result of build-up dyeing test, acid dyes and disperse dyes respectively had good dyeabilities on 1% o.w.f. with Acrylate fiber and DPP fiber. Compatibility of trichromatic of disperse dyes was generally good for most dyes investigated and their critical absorption range were between $120^{\circ}C$ and $130^{\circ}C$. As depending on dyeing methods, there were many differences in dyeability. It was confirmed that 1-bath-1-step dyeing was most suitable when considering dye exhaustion yield and levelling property. Wash, rubbing and light fastness of knits were generally good in most dyes.

A New Analytical Method to Determine the Purity of Synthetic Fluorophores using Single Molecule Detection Technique

  • Song, Nam-Yoong;Kim, Hyong-Ha;Park, Tae-Sook;Yoon, Min-Joong
    • Journal of Photoscience
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    • v.12 no.2
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    • pp.87-93
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    • 2005
  • A new assay technique to distinguish between pure compounds and the isomeric mixtures has been suggested using single molecule (SM) fluorescence detection technique. Since the number of emission spots in a fluorophorespread film prepared from a genuine dye solution was determined by experimental condition, the deviation of spot numbers from the expected values could be considered to be an indication of lower purity of the sample solution. The lower limit of sample concentration for this assay was determined to be $5{\times}10^{-10}$ M to show uniform number of expected spots within 10% uncertainties in our experimental condition. An individual fluorescence intensity distribution for a mixture of isomers having doubly different emissivities was simulated by adding distributions obtained from Cy3 and nile red (NR) independently. The result indicated that the mixture could be identified from the pure compounds through the difference in the number of Gaussian functions to fit the distribution. This new assay technique can be applied to the purity test for synthetic biofluorophores which are usually prepared in small quantities not enough for classical ensemble assays.

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THE EFFECT OF ND : YAG LASER ON DENTINAL TUBULE SEAL AFTER ROOT END RESECTION (치근단절제시 노출된 상아세관의 밀폐효과에 대한 Nd : YAG 레이저의 효과)

  • Shin, Kwang-Chul;Hong, Chan-Ui
    • Restorative Dentistry and Endodontics
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    • v.21 no.1
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    • pp.311-320
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    • 1996
  • If root and resection is done during surgical endodontic treatment, newly exposed dentinal tubules form pathways between the canal and the peripheral tissue. Nd : YAG laser was used to block this phenomenon, and its effect was studied with dye penetration and SEM techniques. 40 intact single rooted teeth were divided into 4 groups(10 each) : control group and test groups, in which retrograde cavity surface, cutting surface, retrograde cavity surface & cutting surface were treated with laser(1 watt 15pps) and finally retrograde filling with IRM was conducted. After that, they were stained with 2 % methylene blue, sectioned and evaluated by the maximum infiltration depth. And to observe surface change, they were prepared for SEM. The results were as follows ; 1. All experimental groups showed microleakage with variation in amount. 2. The 2nd group which treated both the retrograde cavity and cutting surface showed significantly less microleakage than the other groups(p<0.05). There was no significant difference between groups treated on one side only. 3. As a result of SEM observation of dentin surface, obstruction of dentinal tubules with marble shaped granules, which were different from normal dentin could be seen. Cracks could be seen also. 4. In summary of this experiment, it is thought that effort to obstruct the exposed dentinal tubules as well as retrograde cavity after root end resection is needed.

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A study of DSC using Ultrasonic and Thermal treatment on nano-crystalline $TiO_{2}$ surface (염료감응형 태양전지 $TiO_{2}$ 광전극 표면의 초음파 열처리에 관한 연구)

  • Hong, Ji-Tae;Choi, Jin-Young;Seo, Hyun-Woong;Kim, Jong-Lak;Kim, Hee-Je
    • 한국신재생에너지학회:학술대회논문집
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    • 2007.06a
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    • pp.317-319
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    • 2007
  • Recently, there were many researches for efficiency improvement of DSC. Among of these works, research of surface treatment is still a prerequisite for electron diffusion, light-harvesting and surface state of $DSC^{4)}$. Using of the surface treatment, it can be raise up porosity of $TiO_{2}$ nano-crystalline structure on $photo-electrode^{5)}$. There are chemical, physical, electrical and optical methods which raise up its porosity. In this paper, we have designed and manufactured MOPA-type ultrasonic circuit (100W, frequency and duty variable). Manufactured ultrasonic circuit to use to force cavity density and power into $TiO_{2}$ paste. Then, we have optimized forcing time, frequency and duty of ultrasonic irradiation for surface treatment of photo-electrode of DSC. In I-V characteristic test of DSC, ultrasonic and thermal treated DSC shows 19% improved its efficiency against established DSC.

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Flow Visualization Study on Vortices over a Stealth UCAV Configuration (스텔스 무인전투기 형상의 와류 거동에 대한 흐름가시화 연구)

  • Kang, Seung-Hee;Lee, Do-Kwan;Hyun, Jae-Soo
    • Journal of the Korean Society for Aeronautical & Space Sciences
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    • v.35 no.6
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    • pp.467-473
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    • 2007
  • Flow visualization study to qualitatively define the flow field over a stealth UCAV(Uninhabited Combat Air Vehicle) configuration in a water tunnel has been conducted to clarify the basic aerodynamic performance. The test was performed at freestream velocity of 12.7 cm/sec which was corresponding to a Reynolds number of $1.4{\times}10^4$ based on mean aerodynamic chord. The development and breakdown of vortices illuminated by using dye were compared to the previous force and moment data. It was shown that the effect of the vortices generated by the main-body and junction are dominant in the low angle-of-attack region. However, in the high angle-of-attack region, the vortex generated by the fore-body mainly influenced the aerodynamic performance of the model.