• Journal of Powder Materials
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• v.28 no.4
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• pp.331-335
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• 2021

The effects of drying temperature on the microstructure of porous W fabricated by the freeze-casting process of tert-butyl alcohol slurry with WO₃ powder was investigated. Green bodies were hydrogen-reduced at 800℃ for 1 h and sintered at 1000℃ for 6 h. X-ray diffraction analysis revealed that WO₃ powders were completely converted to W without any reaction phases by hydrogen reduction. The sintered body showed pores aligned in the direction of tert-butyl alcohol growth, and the porosity and pore size decreased as the amount of WO₃ increased from 5 to 10vol%. As the drying temperature of the frozen body increased from -25℃ to -10℃, the pore size and thickness of the struts increased. The change in microstructural characteristics based on the amount of powder added and the drying temperature was explained by the growth behavior of the freezing agent and the degree of rearrangement of the solid powder during the solidification of the slurry.

• Polymer(Korea)
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• v.28 no.1
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• pp.18-23
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• 2004

Superabsorbent poly(potassium acrylate-co-acrylamide)s were synthesized in particle form using inverse suspension polymerization technique. Mean diameter of the prepared polymer particles decreased from 300 to 50 $\mu\textrm{m}$ with increasing surfactant concentration. The dynamic and equilibrium swelling behaviors during water absorption and drying process were investigated by weight measurement. The swelling ratio of polymer particles in water changed according to not only polymer crosslinking density, but particle size, saline concentration of aqueous medium, and copolymer compositions. Water sorption amount was increased with decreasing particle size, crosslinking agent concentration, and ion concentration in bulk solution. Being different from the water sorption process, the drying process was not significantly affected by particle size, polymer composition, or crosslinking amount.

• The Journal of Engineering Research
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• v.8 no.1
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• pp.31-50
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• 2006

Shrinkage may cause cracking in concrete. In practice such cracking must be considered in most concrete applications because, under normal conditions, drying of the concrete is unavoidable, and when drying takes place shrinkage occurs. Cracked concrete is an inferior concrete because it is weaker, more permeable, and more susceptible to chemical attack. The development of the strength of LAC with aging depends on a few factors such as type of the cement, W/C ratio, curing conditions and periods. The higher the strength of LAC, the lower the possibility of shrinkage cracking. Hence, the strength of LAC in the hypocaust system depends to a large extent on the effect of cracking decrease of the antifoaming rate to drying shrinkage in cement.

• Proceedings of the Korean Radioactive Waste Society Conference
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• 2003.11a
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• pp.220-225
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• 2003

Generally, liquid radioactive wastes generated in nuclear power plant exist in powder form which do not contain moisture through the evaporating process of the Liquid Waste Management System and drying process of the Concentrated Waste Drying System. This powder form wastes are blended homogeneously with paraffin solidification agent and packed in metal drum to ensure its stability during handling and disposal. However, it was experienced that the powder form wastes were not blended homogeneously and separated into two layers in metal drum, on the other hand, a Portion of powder was adhered and solidified to the Inside parts of facility during the blending process. And the flaw of blending process above would come in case the mole ratio of Boron to Sodium in liquid radioactive wastes exceeds 0.2.

• Conservation Science in Museum
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• v.11
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• pp.49-52
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• 2010

A wooden Comb excavated at Shinchang-dong wetland site was treated with cetylalcohol as a reinforcing agent. The conservation process was done by freeze drying the wooden artifact after substituting it with no.3 butyl alcohol and impregnating with 40wt% cetylalcohol solution. Consequently there was no noticeable surface damage. Also it showed 54% of remaining weight and a shrinkage of length 3.3%, width 2.1% and thickness 3.1%. Therefore using cetylalcohol for conservation of waterlogged archeological wood was effective dimensional stability and remaining weight.

• YAKHAK HOEJI
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• v.39 no.5
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• pp.487-494
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• 1995

Solid lipid microspheres (SLMs) were prepared using various lipids and solidifying agents, in order to enhance the gastrointestinal absorption of Cyclosporine A (Cs A) which is a practically water-insoluble drug with low systemic bioavailability. Egg lecithin and HCO-60 (polyoxyethylated 60 mol, hydrogenated castor oil) were used as lipids. Stearic acid and stearyl alcohol were used as solidifying agents. Emulsion concentrates containing Cs A were prepared by mixing the melted lipid and solidifying agent with water, employing bile salts as a cosurfactant. SLMs were obtained by dispersing the warm emulsion concentrate in cold distilled water under mechanical stirring, followed by freeze drying. Physical characteristics of each SLM were investigated by particle size analysis, optical microscopy and scanning electron microscopy. Mean particle size of SLMs was in the range of 30 to 40.mu.m. The SLMs were in good appearance with spherical shape before freeze drying, but were deformed partially after freeze drying. Drug loading efficiencies of SLMs were observed as high as 80 to 90% in average. The systemic bioavailability of Cs A from different SLM formula was investigated in rats following oral administration. Cs A in whole blood was extracted and assayed by HPLC. SLMs revealed the higher bioavailabilities than the standard formula based on the marketed product. SLMs might have several advantages over standard formula for enhanced gastrointestinal absorption, controlled release properties, high loading capacity of the water-insoluble drug, and feasibility of solid dosage forms with better stability in storage.

• Proceedings of the Korea Concrete Institute Conference
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• 1995.10a
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• pp.108-112
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• 1995

In this study, the fundamental properties of nonshrinkage high strength concrete using calcium sulphoaluminate cement (CSA cement) which was develiped at the Ssangyong Cement Ind, CO., Ltd. Were considered by some experiments. The concrete using CSA cement show a good workability and higher strength development in early age. And, the resultant compressive strength was also higher than OPC. The drying shrinkage of CSA concrete was much less than that of concrete made with OPC and expansive agent.In addition, the value of drying shrinkage was not dependent on the agitating time and the curing condition. Compared to that of OPC.

• Journal of the Korean Applied Science and Technology
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• v.12 no.1
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• pp.19-27
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• 1995

The 2-packaged polyurethane coatings were synthesized, blending pheylmodified polyesters(of which synthetic methods were reported in the previous paper), Desmodur L-75(polyisocyanate wide1y used for coatings), wetting-dispersing agent, white pigment. etc. A variety of coating properties were tested for the coating treatment polyurethane coationgs. Compared with conventional 2-packaged polyure-thane coating, abrasion resistance and lightness index difference of the ones synthesized in the present work were somewhat decreased, but the coating properties such as hardness, gloss specular, cross hatch adhesion. etc. were improved. Especially, resistance against chemical reagents and salt were strikingly improved. In addition. the coationgs had short drying time and long pot-life. This shows that the coationgs are appropriate for rapid drying coatings.

• Proceedings of the Korean Institute of Building Construction Conference
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• 2022.04a
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• pp.194-195
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• 2022

The jointing of unsupported concrete on the parking lot floor is a process for cracking and stress relief due to concrete drying shrinkage and restraint, but curling occurs due to long-term drying shrinkage after the initial age. will be lowered Therefore, by using an expansion material and a shrinkage reducing agent, the dry shrinkage of concrete is realized to 200 με or less.

• Proceedings of the Korean Institute of Building Construction Conference
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• 2009.11a
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• pp.73-76
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• 2009

In ultra-high-strength concrete, chemical shrinkage is larger than drying shrinkage due to using a large amount of cement and admixtures, and this is a factor deteriorating the quality of structures. Thus, we need a new technology for minimizing the shrinkage strain of ultra-high-strength concrete. So, this study have prepared super-high-strength concrete with specified mixing design strength of over 100MPa and have evaluated a method of reducing chemical shrinkage by using expander and shrinkage-reducing agent. According to the results of this study, with regard to the change in length by chemical shrinkage, an expansion effect was observed until the age of seven days. The expansion effect was higher than previous research that used only expander or shrinkage reducing agent. In addition, ultra-high-strength concrete showed a shrinkage rate that slowed down with time, and the effect of the addition of expander material on compressive strength was insignificant. That is shown that required more database to be accumulated through experimental research for the shrinkage strain of members.