• 한국결정성장학회지
• /
• 제14권1호
• /
• pp.12-16
• /
• 2004

본 실험은 대형의 고품질 DAST 결정을 위한 결정안정성과 재현성의 향상에 관하여 연구하였다. DAST 결정은 냉각법에 의한 메탄을 포화용액에서 성장시켰으며, 4-methyl-n-methyl pyridinum tosylate의 축합상태로 합성하였다. DAST 분말은 piperidine이 존재한 상태에서 r-picoline. methyl p-tolune sulfonate 그리고 P-dimethylaminobenzaldehyde로부터 제조하였다. 이때 DAST $H_2O$의 생성을 피하기 위하여 dry Argon분위기에서 합성하였다. 이것은 DAST분자가 습한 분위기에서 결정화될 경우 결정구조는 중심 대칭이 되고 그러한 경우에 DAST 미세결정이 습기를 함유하면 2차 비선형 광학특성은 사라지기 때문이다. 우리는 성장방향을 (001)면으로 고정시켰다. 성장조건은 $H_2O$/day로 서냉시켰으며 기간은 4일 동안이었다. seed 결정의 크기는 $2.5\times 3.6\times0.4\textrm{mm}^3$이며 $10\times 10.5\times3.0\textrm{mm}^3$의 DAST 결정을 제조했다. 육성된 DAST는 빨간색이며 메탈릭그린처림 보이는 표면특성을 나타내였다.

• 한국의류학회지
• /
• 제48권4호
• /
• pp.707-728
• /
• 2024

This study aimed to assess the colorizing properties of bacterial cellulose (BC) using plant-based dyes, namely spinach, beet, and banana peel, and determine the dyeing conditions of each dye based on color strength (K/S) values. Tannic acid and walnut shell powder were utilized as bio-mordants, and their effects on the dyeability of BC were compared to metallic mordants. Additionally, the type of mordant and the mordanting method were assessed according to their rubbing fastness and dry-cleaning fastness. The K/S values of the colorized and mordanted BCs were also compared to examine their mordanting conditions. Finally, the mordanting conditions for spinach, beet, and banana peel dyeing were selected as post-mordanting with tannic acid, meta-mordanting with tannic acid, and post-mordanting with walnut shell powder, respectively. Based on the results, the selected mordanting conditions improved both rubbing fastness and dry-cleaning fastness of BCs to grade 5, and the light fastness achieved grade 4-5. The tensile strength and flexibility of the dyed BCs were also enhanced and comparable to that of untreated cowhide leather.

• 한국식품조리과학회지
• /
• 제21권4호
• /
• pp.545-555
• /
• 2005

The physicochemical and microbial characteristics of Oiji prepared with dry salting method, which has been used industrially for industry, were investigated. Low salting and low storage temperature were employed:extremely low salting extremely low temperature; ESET $(5\%,\;0^{\circ}C)$, very low salting extremely low temperature;VSET $(10\%,\;0^{\circ}C)$, extremely low salting very low temperature; ESVT$(5\%,\;5^{\circ}C)$, low salting very low temperature; VSVT$(10\%,\;5^{\circ}C)$ and high salting low temperature;HSLT$(30\%,\;10^{\circ}C)$ for control. Acidity was lower, and pH was higher in VSET, in of which the fermentation pattern was similar with that of HSLT The time required to reach the optimum acidity ($0.3\%$ lactic acid) was longer delayed for VSET (168 days), than for compared to ESVT (51 days). During storage of Oiji, greenness (-a) as measured with of the Hunter color system wasshowed the highest in VSET, and the lowest while in ESVT, the lowest. Total microbial and lactic acid bacteria counts number were the lowest in HSLT and VSET and were the lowest than in other groups, while the highest in ESVT. Yeast was not detected in HSLT, but was the highest while in VSVT. E coli coliform and listeria were detected in the $5\%$ salting groups, although Salmonella was not detected in any of the all groups. Texture profile analysis demonstrated exhibited that fracturability and hardness were highest in HSLT and VSET, compared to the other groups. Scores of over-all preference for ESVT and HSLT were higher atwith 6.3 and 6.2, respectively, compared to the other products. Based on these results, lower saltiness less than $10\%$ and lower storage temperature (less than $5^{\circ}C$) condition was optimum for maximizing the better for good quality of industrial Oiji preparation in industry.

• 혜화의학회지
• /
• 제13권2호
• /
• pp.187-196
• /
• 2004

Now many sustitution and false articles is used in korea instead of shanyao. To use shanyao correctly, we will make a quilitative certificational plan of shanyao to investigate all of lieraturea, records and documents. And we could reach conclusions as folloews. 1) Source About a source of shanyao, though korea and china has a each other source, we think there is no problem in use of both. 2) Process In our country producing shanyao as medical use is a 'duanma', we can divide into peeling and non-peeling, drying at bulks and at briquets, steaming shanyao and fresh shanyao. Regardless of existence for peeling and steaming, a distributing shanyao is received a proper judgment. Like this result was expressed by insufficiency of standards about medical components or indicating components. We detected a reminding S02 more than 10 ppm. And this expresses that there ia a problum at a drying method. To suggest proper processing methods, a standard of quility will have to be made which the existence of peeling, difference of quility between 'changma' and 'duanma', drying method and exudation test with cutted thickness are adaptable. Besides, 'maoshanyao' and 'guangshanyao' of china is processed by various methods which decrease a medical effect such as too much soaking shanyao in water, steaming with a sulfur, too much peeling, So we must process shanyao like the next methods. (1) When harvesting, dig deeply not to cut off roots. (2) Not to peel, wash shanyao in a washing machine. (3) Dry to 50-60% degree at sunny place or drying machine. (4) To be easy for drying and exudation, cut off a thick piece with 5 mm (5) Dry perfectly at ding machine. 3) Quality3) Quality (1) Functional standards It is not Proper that 'guangshanyao' is used in china because it has a problem with quility on process of working, If they did not soak shanyao in water or heat with steam, it is the real situation that they cannot cutt off shanyao evenly. In conclusion, shanyao must be heavy, powdery with a perfectly non-peeling surface, section surface is yellow-white color, unequal and has no holes. (2) Physicochemical standards It is the real situation that we can not distinguish into quility of shanyao with established test because various workings which decrease medical effects is used. Therefore we suggest a testing standard of S02 which is used in bleaching. And testing standards relatived with decrease of medical effects must be established at once. It must that Dry on loss is less than 14.0%, content of ash is less than 6.0%. Content of acid-nonsoluble ash is less than 0.5%. Contens of heavy metal has to detect less than 30 ppm and there is no reminding agricultural medince.

• 기술사
• /
• 제17권4호
• /
• pp.28-39
• /
• 1984

Experiments were carried out for the development of a processing method of soybean into full-fat or defatted flour, using two varieties of soybean (kwangkyo produced in Korea and Bragg produced in India) Samples were subjected to dry dehulling, size reduction and wet heat treatment processes to make soybean flours. The quality of soybean flours were evaluated, and the results obtained were summarized as follows. 1. Crude fiber content of dehulled soybean was under 3.0% which indicated satisfactory dehulling, and there was no significant difference in crude fibre content between two varieties. 2. When dehulled soybean was cracked into soy grits by a hammer mill, 98.71∼98.86％ of the soy grit was in the range of 10∼18 mesh which was the optimum size of particle for quick and uniform penetration of heat into the intra-particle air spaces. 3. Moisture content of soy flour after steam treatment at 15 psig for 5 to 30 min was only 0.29∼1.68% which did not hinder the next milling operation. 4. From the color analysis of soy flours, it was observed that the dominant wavelength for all the samples are in a very narrow range from 575 to 581 nm and the color variation was from yellow to yellowish orange. Twenty to twenty five ％ higher reflectance was observed in the defatted flours than full fat flours. The ％ chroma of the defatted flour slightly increased as the duration of steaming of soy grits increased, whereas that of the full-fat flour did not. 5. The protein extractability in the defatted flour at pH 7.6 showed progressive decrease in solubility from 48.40％ (Bragg), 75.20％ (kwangkyo) for untreated flours to 9.75％ (Bragg), 26.27％ (kwangkyo) for 30 min steaming. But Kwangkyo variety showed twice higher protein extractability than Bragg variety.

• 한국염색가공학회지
• /
• 제21권4호
• /
• pp.23-32
• /
• 2009

The objective of this study is to investigate the efficacy of leaf powder colorants as substitutes for traditional indigo dyeing. Leaf powder colorants were prepared by hot air($50^{\circ}C$) and room temperanrre($25^{\circ}C$) drying methods from fresh leaves. The presence of indigo in the leaf powder colorants was confirmed by UV/Visible absorption spectra. All the powder colorants showed broad absorption at 602 nm as same as synthetic indigo. Dyeing was done by reduction method with sodium hydrosulfite and sodium hydroxide. Leaf powder colorants produced blue color on silk fabrics, showing similar color to the one dyed traditionally with fresh juice extract. The powder colorants prepared at room temperature drying were more stable for long term storage than that prepared by hot air drying. Thus, the powder colorants prepared by room temperature drying was reduced and dyed in one-step process without sodium hydroxide in the dyebath for further investigate dyeing properties. K/S value of the fabric dyed without sodium hydroxide was much higher than one dyed with sodium hydroxide. Regardless of the addition of sodium hydroxide, rubbing fastness was fairly good showing above 4 rating. Fastness to dry cleaning and light of the fabrics dyed without sodium hydroxide were mote higher than that dyed in alkaline condition.

• 한국환경농학회:학술대회논문집
• /
• 한국환경농학회 2011년도 30주년 정기총회 및 국제심포지엄
• /
• pp.177-187
• /
• 2011

This study was conducted to determine some physical and chemical properties of the soil and their relationship to spectroscopic-based (visible range) analytical methods while evaluating soil organic matter fractions and soil quality in degraded and non-degraded soils in a wide range of environments. Soil samples were collected from the different landscape positions of cultivated and noncultivated soils, and the latter from the same landscape positions but with different vegetation, at Songco, Lantapan, Bukidnon. The physical and chemical properties of the soils were determined at the SPAL, CMU, Musuan, Bukidnon while the metagenomic properties were determined at the Laboratory of the University of Missourri, Missourri, USA. Bulk density and air dry soil strength values of the soils from the cultivated areas were generally higher than those of the uncultivated areas. Also, soils at the summit generally had lower bulk density and soil strength values than the other landscape positions. Moreover, soils planted to camote (Ipomoea batatas) had higher bulk density and soil strength values compared to soils grown to pepper under the trees. Exchangeable calcium (Ca), magnesium (Mg), and potassium (K) and cation exchange capacity (CEC) of the soils were generally higher in uncultivated areas than those of the cultivated areas. A similar trend was observed for the potassium permanganate ($KMnO_4$)-oxidizable organic C contents determined by spectroscopic method and the total C contents determined by the Walkley-Black method. The $KMnO_4$-oxidizable organic C contents determined by spectroscopic method and the total C contents determined by the Walkley-Black method were closely related ($r=0.631^{**}$). Hence, the former method shows promise in assessing soil quality as it is a rapid test, relatively low cost and can be distributed as a field kit either with a portable spectrometer or with a color chart.

• 아시안잔디학회지
• /
• 제22권1호
• /
• pp.49-56
• /
• 2008

본 연구는 효모균과 유산균의 발효액을 함유한 비료가 크리핑벤트그래스 잔디의 생육에 미치는 영향을 시험하고자 2007년 8월부터 11월까지 SKY72 골프클럽 증식포장에서 수행하였다. 시험처리는 무처리구, 대조구, 처리구1, 처리구2, 처리구3로 3반복 난괴법으로 수행하였다. 시험기간 동안에는 토양화학성, 엽색지수, 엽록소함량 및 예초물량, 잔디분석 등을 조사하였으며, 그 결과는 아래와 같다. 토양화학성은 공시비료의 시비가 토양에는 별다른 영향이 미치지 않음을 알 수 있었다. 엽색지수는 무처리구보다 비료처리구(대조구, 처리구)에서 7.6% 증가하였으나 대조구와 처리구간차이는 나타나지 않았으며, 처리구 2에서 가장 높은 엽색지수 값을 나타내었다. 엽록소 함량은 무처리구보다 비료처리구(대조구, 처리구)에서 48.3% 증가하였고, 대조구와 처리구간 차이는 처리구 2과 처리구 3에서 각각 4.4%와 2.7% 높게 나타났으며, 시험기간 중 가장 좋은 잔디생육을 나타내는 처리구는 처리구 2로 조사되었다. 예초건물중은 무처리구 보다 비료처리구(대조구, 처리구)에서 83.6% 증가하였고, 대조구와 처리구간 차이는 처리구 2와 처리구 3에서 각각 13.8%와 13.9% 증가한 것으로 조사되었다. 시험 종료 후 채취한 잎의 무기성분은 시비구(CF, T-1, T-2, T-3)가 무처리구보다 질소는 82%, 인은 19%, 칼리는 42% 정도 증가하였고, 대조구(CF)와 처리구(T-1, T-2, T-3)사이에서는 비슷하였다.

• 보존과학회지
• /
• 제30권1호
• /
• pp.27-32
• /
• 2014

본 논문에서 보존처리 한 책은 1935년 일본사에서 발행된 "위인최후(偉人最後)の언엽집(言葉集)"이다. 1900년대 초반의 책들은 대부분이 산성지로 되어있어 책의 산도가 높고 스테이플로 인한 갈변현상이 심하다. 본 시료도 갈변현상이 관찰되었으며, 책의 pH가 3.2로 매우 낮았다. 스테이플에 의한 갈변 이외에 종이 전체의 색이 많이 변하였으며, 종이 자체의 산성도로 인하여 종이가 바스러지는 현상이 보였다. 스테이플 철심을 제거한 후 건식, 습식클리닝을 행하여 오염물을 제거하였다. 가볍게 프레스하여 종이를 건조시킨 후, 미농지($4g/m^2$)를 사용하여 속지와 겉 표지를 배접하여 보강처리를 하였다. 본 논문에서는 스테이플 심을 대신하여 실이나 종이로 다시 묶는 기존의 보존처리 방법과 다르게 기존의 스테이플과 유사한 철심을 만들어 원래의 자리에 복원하는 작업을 하였다. 복원 하기 위해 스테이플의 두께와 비슷한 철사를 사용하였고, 착색액 ($H_2O$, $C_2H_5OH$, $CuSO_4{\cdot}5H_2O$, $FeCl_3{\cdot}6H_2O$)에 넣어 부식된 스테이플 심과 유사한 색으로 착색하였다. 마지막으로 20%의 paraloid B-72로 방식처리를 하여 차후의 부식을 예방하였다.

• Applied Biological Chemistry
• /
• 제29권2호
• /
• pp.190-197
• /
• 1986

탈지분유(脫脂粉乳)에서 마이야르 반응(反應)(Maillard reaction)의 속도(速度)를 간단히, 그리고 효과적으로 측정(測定)하기 위(爲)한 지표(指標)로서 포장상위공간내(包裝上位空間內)의 $CO_2$함량(含量)을 이용(利用)하였고,$CO_2$량(量 )과 갈변색소형성(褐變色素形成) 사이의 상관관계(相關關係)를 조사(調査)하였다. 갈변색소(褐變色素)와 $CO_2$함량(含量)사이에는 높은 상관관계(相關關係)를 나타냈으며, 시료(試料)의 상위공간내(上位空間內)의 $CO_2$량(量)을 측정(測定)함으로 마이야르 반응(反應)을 예측(豫測)할 수 있는 빠르고 간단한 방법(方法)이 될 수 있었다. 휘발성분(揮發成分)은 저장기간(貯藏期間)이 증가(增加)할수록 증가(增加)하였고, 산소함량(酸素含量)과는 반비례(反比例)하였다. 리신(lysine)은 반응(反應)의 촉매(觸媒)로 글루코스보다 더 효과적이었으며, 시료(試料)를 $55^{\circ}C$와 $65^{\circ}C$에 넣어 저장(貯藏)할 때 반응(反應)을 촉진(促進)시켜 시험기간(試驗期間)을 단축(短縮)시켰으며 $75^{\circ}C$에서는 빨리 변질(變質)되었다.