• Title/Summary/Keyword: Distribution of grain shape

Search Result 81, Processing Time 0.025 seconds

Characteristics of Catalytic Combustible Gas Sensor Based on Planar Technology (평탄형 접촉 연소식 가스 센서의 특성)

  • Kim, Yeong-Bok;Noh, Hyo-Sub;Park, Jin-Seong
    • Journal of the Korean Institute of Electrical and Electronic Material Engineers
    • /
    • v.21 no.9
    • /
    • pp.812-817
    • /
    • 2008
  • A catalytic combustible sensor for LPG/LNG detection was fabricated on $Al_2O_3$ substrate using planar technology. The catalysts of Pd and Pt were added to ${\alpha}$- and ${\gamma}-Al_2O_3$ powders. The mixture of Pt, Pd and $Al_2O_3$ were homogenized by using a three roll mixer. TCR characteristics of Pt heater were optimized with the heat treatment temperature. Sensing properties were investigated as a function of the microstructure of $Al_2O_3$, the gas concentration and the variation of input voltage. ${\alpha}-Al_2O_3$ sintered at 500 $^{\circ}C$ is more suitable as LPG/LNG sensor due to good grain shape and size distribution of about 300 nm than that of ${\gamma}-Al_2O_3$ which is in irregular shape and with a particle size of 5-30 ${\mu}m$. The sensor has shown maximum output voltage of 14 mV for 1000 ppm $C_4H_{10}$ and 3.8 mV for 1000 ppm $CH_4$ at 5.0 V input voltage.

MICROSTRUCTURAL CHARACTERISTICS OF HOT FORGED AL 6061 ALLOY

  • Kwon Y.-N.;Lee Y.-S.;Lee J.-H.
    • Proceedings of the Korean Society for Technology of Plasticity Conference
    • /
    • 2003.10b
    • /
    • pp.55-58
    • /
    • 2003
  • Many researches have been already done on the issues of high temperature deformation and the microstructural evolution. The information has been very useful for the plasticity industry, especially successful for the extrusion. However, the parts made with forging usually have a complex shape. It is difficult to control the distribution of the variables like strain, strain rate and temperature rise due to the working heat during a hot-forging process. Consequently, the microstructural variation could be occurred depending on the plastic deformation history that the forged part would get during a hot forging. In the present study, the microstructural characteristic of a hot-forged 6061 aluminum alloy has been discussed on the aspect of grain size evolution. A forging of 6061 aluminum alloy has been carried out for a complex shape with a dimensional variation. Also, finite element analysis has been done to understand how the deformation variables such as strain, strain rate give an influence on the microstructure of a hot forged aluminum product.

  • PDF

Texture Evolution of Extruded AZ80 Mg Alloy under Various Compressive Forming Conditions (AZ80 마그네슘 합금 압출재의 압축 성형조건에 따른 방위특성 분석)

  • Yoon, J.H.;Lee, S.I.;Lee, J.H.;Park, S.H.;Cho, J.H.
    • Transactions of Materials Processing
    • /
    • v.21 no.4
    • /
    • pp.240-245
    • /
    • 2012
  • With the increasing demand for light-weight materials to reduce fuel consumption, the automobile industry has extensively studied magnesium alloys which are light weight metals. The intrinsic poor formability and poor ductility at ambient temperature due to the hexagonal close-packed (HCP) crystal structure and the associated insufficient number of independent slip systems restricts the practical usage of these alloys. Hot working of magnesium alloys using a forging or extrusion enables net-shape manufacturing with enhanced formability and ductility since there are several operative non-basal slip systems in addition to basal slip plane, which increases the workability. In this research, the thermomechanical properties of AZ80 Mg alloy were obtained by compression testing at the various temperatures and strain rates. Optical microscopy and EBSD were used to study the microstructural behavior such as misorientation distribution and dynamic recrystallization. The results were correlated to the hardening and the softening of the alloy. The experimental data in conjunction with a physical explanation provide the optimal conditions for net-shape forging under hot or warm temperatures through control of the grain refinement and the working conditions.

Study on the Soil Compaction (Part 4) -The Influence of Soil Compadtion on Unconfined Compressive Strength and Coefficient of Permeability- (흙의 다짐에 관한 연구(제4보) -흙의 다짐이 -축골조강동 및 투수계수에 미치는 영향-)

  • 강예묵
    • Magazine of the Korean Society of Agricultural Engineers
    • /
    • v.12 no.3
    • /
    • pp.2003-2012
    • /
    • 1970
  • In order to the influence of grain size distribution on compressive strength and coefficient of permeability, unconfined compression test and permeability test were performed for seventy samples that have various grain-size distributions. Its results are as follows: 1. Maximum unconfined compressive strength appears at the dry side of optimum moisture content. 2. Unconfined compressive strength is proportional to the increase of percent passing of No. 200 sieve. 3. Precent of deformation in failure increases in proportion to the increase of percent passing of No. 200 sieve, and modulus of No. 200 sieve, and modulus of deformation also increases in proportion to percent passing of No. 200 sieve. 4. Unconfined compressive strength increases in proportion to uniformity coefficient, liquid limit and plastic index, but it decreases gradually according to the increase of coefficient of grading and classification area. 5. Maximum dry density decreases according to the increase of void ratio. 6. Coefficient of permeability decreases according to the increase of percent passing of No. 200 sieve, and when percent of No. 200 sieve, and when percent passing of No. 200 enlarged more than 40%, it becomes less than $10^{-6}cm/sec$ which is the limit of coefficient of permeability of core material for earth dam proposed by Lee. 7. Coefficient of permeability increases according to the increase of coefficient of grading, classification area and index of Talbot formula r, but it was rather decrease by the increase of uniformity coefficient. 8. Coefficient of permeability seems to depend on the size and the shape of the flow path which is a series of void to be concerned by the size and the proprton of soil grain, even though void ratios are same.

  • PDF

Surface Roughness Impact on Francis Turbine Performances and Prediction of Efficiency Step Up

  • Maruzewski, Pierre;Hasmatuchi, Vlad;Mombelli, Henri-Pascal;Burggraeve, Danny;Iosfin, Jacob;Finnegan, Peter;Avellan, Francois
    • International Journal of Fluid Machinery and Systems
    • /
    • v.2 no.4
    • /
    • pp.353-362
    • /
    • 2009
  • In the process of turbine modernizations, the investigation of the influences of water passage roughness on radial flow machine performance is crucial and validates the efficiency step up between reduced scale model and prototype. This study presents the specific losses per component of a Francis turbine, which are estimated by CFD simulation. Simulations are performed for different water passage surface roughness heights, which represents the equivalent sand grain roughness height. As a result, the boundary layer logarithmic velocity profile still exists for rough walls, but moves closer to the wall. Consequently, the wall friction depends not only on roughness height but also on its shape and distribution. The specific losses are determined by CFD numerical simulations for each component of the prototype, taking into account its own specific sand grain roughness height. The model efficiency step up between reduced scale model and prototype value is finally computed by the assessment of specific losses on prototype and by evaluating specific losses for a reduced scale model with smooth walls. Furthermore, surveys of rough walls of each component were performed during the geometry recovery on the prototype and comparisons are made with experimental data from the EPFL Laboratory for Hydraulic Machines reduced scale model measurements. This study underlines that if rough walls are considered, the CFD approach estimates well the local friction loss coefficient. It is clear that by considering sand grain roughness heights in CFD simulations, its forms a significant part of the global performance estimation. The availability of the efficiency field measurements provides an unique opportunity to assess the CFD method in view of a systematic approach for turbine modernization step up evaluation. Moreover, this paper states that CFD is a very promising tool for future evaluation of turbine performance transposition from the scale model to the prototype.

Microstructure and Fracture Path of Cr-Mn-N Steel upon Aging Treatment

  • Lee, Se-Jong;Sung, Jang-Hyun;Ralls, K.M.
    • Journal of the Korean Society for Heat Treatment
    • /
    • v.4 no.3
    • /
    • pp.21-30
    • /
    • 1991
  • Microstructural analysis was conducted to observe the effect of aging treatments in a Cr-Mn austenitic stainless steel containing nitrogen, and the amount, size, shape and distribution of precipitates were investigated. It was found that on water quenching from $1000^{\circ}C$ after holding 3 h at that temperature, the steel contained no precipitates observable by optical microscopy. Precipitation of phases begins at places most favorable for the formation of nuclei-in the boundaries of grains and twins. Precipitates were studied in detail by means of scanning electron microscopy (SEM) and transmission electron microscopy (TEM). Chemical compositions of precipitates were examined by the use of scanning transmission electron microscopy (STEM) together with an energy dispersive X-ray (EDX) microanalysis. Also chromium depletion adjacent to grain boundary precipitates was investigated by the use of Auger electron spectroscopy (AES) for a direct examination of the fracture surface chemistry.

  • PDF

Effect of Powder Size of Mg-Zn-Y Alloy on the Consolidation

  • Kim, Taek-Soo;Chae, H.J.;Lee, J.K.;Jung, H.G.;Kim, Y.D.;Bae, J.C.
    • Proceedings of the Korean Powder Metallurgy Institute Conference
    • /
    • 2006.09b
    • /
    • pp.1266-1267
    • /
    • 2006
  • [ $MgZn_{4.3}Y_{0.7}$ ] alloy powders were prepared using an industrial scale gas atomizer, followed by warm extrusion. The powders were almost spherical in shape. The microstructure of powders as atomized and bars as extruded was examined as a function of initial powder size distribution using Scanning Electron Microscope (SEM), Energy Dispersive X-ray Spectroscope (EDS) and X-ray Diffractometer (XRD). The grain sizes were decreased with extruding as well as decreasing the initial powder sizes. Both the ultimate strength and elongation were enhanced as the initial powder sizes were decreased.

  • PDF

Dynamic Precipitation and Substructure Stablility of Cu Alloy during High Temperature Deformation

  • Han, Chang-Suk;Choi, Dong-Nyeok;Jin, Sung-Yooun
    • Korean Journal of Materials Research
    • /
    • v.29 no.6
    • /
    • pp.343-348
    • /
    • 2019
  • Structural and mechanical effects of the dynamical precipitation in two copper-base alloys have been investigated over a wide range of deformation temperatures. Basing upon the information gained during the experiment, also some general conclusion may be formulated. A one concerns the nature of dynamic precipitation(DP). Under this term it is commonly understood decomposition of a supersaturated solid solution during plastic straining. The process may, however, proceed in two different ways. It may be a homogeneous one from the point of view of distribution and morphological aspect of particles or it may lead to substantial difference in shape, size and particles distribution. The effect is controlled by the mode of deformation. Hence it seems to be reasonable to distinguish DP during homogeneous deformation from that which takes place in heterogeneously deformed alloy. In the first case the process can be analyzed solely in terms of particle-dislocation-particle interrelation. Much more complex problem we are facing in heterogeneously deforming alloy. Deformation bands and specific arrangement of dislocations in form of pile-ups at grain boundaries generate additional driving force and additional nucleation sites for precipitation. Along with heterogeneous precipitation, there is a homogeneous precipitation in areas between bands of coarse slip which also deform but at much smaller rate. This form of decomposition is responsible for a specially high hardening rate during high temperature straining and for thermally stable product of the decomposition of alloy.

A study on Weibull Probability Statistics Characteristics for Vickers Hardness of Degraded Stainless Steel (열화된 스테인리스강의 비커스 경도에 대한 와이블 확률 통계 특성에 관한 연구)

  • Nam, Ki-Woo;Cho, Sung-Duck;Kim, Seon-Jin;Ahn, Seok-Hwan
    • Journal of Power System Engineering
    • /
    • v.21 no.5
    • /
    • pp.79-85
    • /
    • 2017
  • Vickers hardness is an important material in the design and reliability is required. Therefore, these values are very important as the basic data for design, manufacture and development, and the identification of quantitative probability distribution characteristics such as mean and dispersion is a very important parameter in design. In this study, Vickers hardness was measured after artificially heat-treated in the temperature range 753K, where chrome depletion near the grain boundary occurred for three kinds of stainless steels, and the Vickers hardness were evaluated. From the results, Vickers hardness increased with increasing heat treatment temperature. In Weibull distribution for Vickers hardness, the dispersion of STS310S at 813K and 873K was small, and the dispersion of STS316L at 753K, 933K and 993K was small. Also, STS347H exhibited the lowest dispersion at 753K in three kinds of stainless steels. The scale parameter increased with increasing heat treatment temperature in three kinds of stainless steels.

Research of reducing thermal stress generated in MGC turbine nozzles

  • Fujimoto, Syuu
    • Proceedings of the Korean Society of Propulsion Engineers Conference
    • /
    • 2004.03a
    • /
    • pp.385-390
    • /
    • 2004
  • An unique ceramic material produced through unidirectional solidification with eutectic composition of two-phase oxides was introduced recently. This composite material has the microstructure of coupled networks of two single crystals interpenetrate each other without grain boundaries. Depending on this microstructure this material, called Melt Growth Composite (MGC), can sustain its room temperature strength up to 1$700^{\circ}C$ (near its melting point) and offer strong oxidization-resistant ability, making its characteristics quite ideal for the gas turbine application. The research project on MGC started in 2001 with the objective of establishing component technologies for MGC application to the high temperature components of the gas turbine engine. MGC turbine nozzles are expected to improve efficiency of gas turbine. However, reduction of the thermal stress is required since high thermal stress is easily generated in MGC turbine nozzles due to temperature distribution. Firstly, the hollow nozzle shape was optimized to reduce thermal stress using numerical analysis. From the results of the first hot gas flow tests, the thermal stress due to span-wise temperature distribution was required to be reduced, and separated nozzle to three pieces was designed. This was tested in hot gas flow at 140$0^{\circ}C$ level, and temperature distributions on the nozzle surface were obtained and stress field was evaluated.

  • PDF