• Title/Summary/Keyword: Dispersion variation

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Detection of Defects in a Thin Steel Plate Using Ultrasonic Guided Wave (유도초음파를 이용한 박판에서의 결함의 검출에 관한 연구)

  • Jeong, Hee-Don;Shin, Hyeon-Jae;Rose, Joseph L.
    • Journal of the Korean Society for Nondestructive Testing
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    • v.18 no.6
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    • pp.445-454
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    • 1998
  • In order to establish a technical concept for the detection of defects in weldments in thin steel plate, an experimental and theoretical investigation was carried out for artificial defects in a steel plate having a thickness of 2.4mm by using the guided wave technique. In particular the goal was to find the most effective testing parameters paying attention to the relationship between the excitation frequency by a tone burst system and various incident angles. It was found that the test conditions that worked best was for a frequency of 840kHz and an incident angle of 30 or 85 degrees, most of the defects were detected with these conditions. Also, it was clear that a guided wave mode generated under an incident angle of 30 degrees was a symmetric mode, So, and that of 85 degrees corresponded to an antisymmetric mode, Ao. By using the two modes, most of all of the defects could be detected. Furthermore, it was shown that the antisymmetric mode was more sensitive to defects near the surface than the symmetric mode. Theoretical predictions confirmed this sensitivity improvement with Ao for surface defects because of wave structure variation and energy concentration near the surface.

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Studies on Particle Size Control and Stability of Lead Chromate Pigment Particles (크롬산납 무기안료 입자 제어 및 안정성에 관한 연구)

  • Park, Chan Kyu;Jung, Dae Yoon;Chang, Sang Mok;Lee, Sang Rok
    • Applied Chemistry for Engineering
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    • v.19 no.3
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    • pp.264-269
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    • 2008
  • For the synthesis of lead chromate pigments, we investigated the characteristics of particle growth with reacting conditions in the synthetic process, the effect of additives, and its micro-capsulation. The more tiny and uniform dispersion particles could be obtained at a lower pH and diluter intial concentration. The variation range of average pigment size was increased with the agitating speed. The pigment size could be controlled by adding aluminum sulfate as an additive, which maintained the optimum particle dispersion. It was found that the optimum micro-capsulation conditions were pH 9~10 and above $90^{\circ}C$ during the micro-capsulation of lead chromate pigment, and below 0.5% humidity after micro-capsulation.

Effect of Nanomesh Structure Variation on the Friction and Wear Characteristics of Carbon Nanotube Coatings (탄소나노튜브 코팅의 마찰/마모 특성에 대한 나노메쉬 구조의 영향)

  • Kim, Hae-Jin;Kim, Chang-Lae
    • Tribology and Lubricants
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    • v.36 no.6
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    • pp.315-319
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    • 2020
  • In various fields, several studies based on carbon nanotubes (CNTs) have been conducted. The results of previous studies, wherein CNT coatings have been incorporated as solid lubricants, demonstrate that the friction and wear characteristics of CNT coatings can be improved through the absorption/dispersion of the contact pressure by controlling the stiffness of the nanomesh structure comprising CNT strands. In this study, the friction and wear characteristics of the following are compared: CNT coating formed by spin coating of CNT solution, compressed CNT coating, and compressed/heated CNT coating (wherein CNT strands are squeezed through compression and/or heating). It is observed that the friction coefficient of the CNT coating having the largest number of voids between the CNT strands is significantly lower than those of the compressed CNT coating and the compressed/heated CNT coating. The wear tracks of the compressed CNT coating and the compressed/heated CNT coating indicate that some parts become torn or adhere into a lump. However, in the case of the CNT coating, a smooth wear surface is formed by rubbing. Furthermore, as the void space between the squeezed and adhered CNT strands decreases, the resistance to structural deformation increases, thereby resulting in an increased frictional force and a wear pattern that becomes torn or forms a lump. Hence, the results obtained from this study corroborate that the friction and wear characteristics of CNT coatings can be enhanced through the absorption/dispersion of the contact pressure by controlling the stiffness of the nanomesh structure of CNT coatings.

Ternary Phased Graphene/Silica/EVOH Nanocomposites Coating Films (삼성분계 그래핀/실리카/EVOH 나노 복합 코팅 필름)

  • Kim, Seong Woo
    • Journal of Adhesion and Interface
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    • v.23 no.3
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    • pp.94-99
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    • 2022
  • Ternary phased graphene/silica/EVOH nanocomposite coating materials were prepared via sol-gel process and solution blending process. From both SEM observations and XRD analysis, the exfoliated structure and dispersion state of graphene nanosheets and silica particles in the nanocomposites as well as the intercalated and exfoliated structure of the prepared graphene oxide were confirmed. The incorporation of GrO and silica at appropriate content resulted in remarkable improvement in oxygen barrier property of the ternary phased nanocompoiste-coated BOPP films, compared with that of binary(silica/EVOH) phased nanocomposite coating films, however, at excess amount of GrO and silica, very slight variation was observed due to incomplete exfoliation, dispersion of graphene tactoids, and formation of micro cracks in the silica clusters. In addition, the transparency of nanocomposite-coated film was investigated by measuring the light transmittance as a function of GrO contents, suggesting the possibility for the application of food packaging films.

Sperm chromatin structure assay versus sperm chromatin dispersion kits: Technical repeatability and choice of assisted reproductive technology procedure

  • Laxme B, Vidya;Stephen, Silviya;Devaraj, Ramyashree;Mithraprabhu, Sridurga;Bertolla, Ricardo P.;Mahendran, Tara
    • Clinical and Experimental Reproductive Medicine
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    • v.47 no.4
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    • pp.277-283
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    • 2020
  • Objective: The sperm DNA fragmentation index (DFI) guides the clinician's choice of an appropriate assisted reproductive technology (ART) procedure. The DFI can be determined using commercially available methodologies, including sperm chromatin dispersion (SCD) kits and sperm chromatin structure assay (SCSA). Currently, when DFI is evaluated using SCD kits, the result is analyzed in reference to the SCSA-derived threshold for the choice of an ART procedure. In this study, we compared DFI values obtained using SCSA with those obtained using SCD and determined whether the difference affects the choice of ART procedure. Methods: We compared SCSA to two SCD kits, CANfrag (n=36) and Halosperm (n=31), to assess the DFI values obtained, the correlations between tests, the technical repeatability, and the impact of DFI on the choice of ART. Results: We obtained higher median DFI values using SCD kits than when using SCSA, and this difference was significant for the CANfrag kit (p<0.001). The SCD kits had significantly higher coefficients of variation than SCSA (p<0.001). In vitro fertilization/intracytoplasmic sperm injection (IVF/ICSI) would be chosen for a significantly higher proportion of patients if a decision were made based on DFI derived from SCD rather than DFI determined using SCSA (p=0.003). Conclusion: Our results indicate that SCD kit-specific thresholds should be established in order to avoid the unnecessary use of IVF/ICSI based on sperm DNA damage for the management of infertility. Appropriate measures should be taken to mitigate the increased variability inherent to the methods used in these tests.

Physical Analysis of High Strength Concrete According to Mixing Methods of Binders for Application Analysis of Pre-Mix Cement (프리믹스 시멘트의 활용성 분석을 위한 결합재의 혼합방법에 따른 고장도 콘크리트의 물성 분석)

  • Han, Cheon-Goo;Lee, Hae-Ill
    • Journal of the Korea Institute of Building Construction
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    • v.9 no.5
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    • pp.127-133
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    • 2009
  • It is important to increase the strength of binders in order to enhance the strength of concrete. However, when the mineral admixture used for high strength concrete is incorporated individually, its dispersibility decreases due to the phenomenon of compaction, which reduces its fluidity and results in insufficient strength being created. To solve this problem, we can pre-mix each binder in advance to disperse a mineral admixture among binders, which will strengthen the fluidity and strength of concrete. Therefore, this study analyzed the properties of high strength concrete depending on the mix method used, to determine the effect of pre-mix cements ranging from W/B 15 to 35%. It was found that the fluidity of pre-mix increased to a level higher than that of individual mix due to its dispersion and ball bearing effect. The air content was slightly decreased from the result of individual mix due to the micro filler effect, which causes fine particles of silica-fume to fill the voids among cement particles, while the setting time of pre-mix was shorter than that of individual mix, because enhanced dispersion of pre-mix affects hydration heat time. The compressive strength of pre-mix increased due to the phenomenon of compaction of gap structure, and the variation of coefficient decreased by 1.69% on average in strength variation.

The Development of Dynamic Model for Long-Term Simulation in Water Distribution Systems (상수관망시스템에서의 장기간 모의를 위한 동역학적 모형의 개발)

  • Park, Jae-Hong
    • Journal of Korea Water Resources Association
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    • v.40 no.4
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    • pp.325-334
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    • 2007
  • In this study, a long-term unsteady simulation model has been developed using rigid water column theory which is more accurate than Extended-period model and more efficient comparing with water-hammer simulation model. The developed model is applied to 24-hours unsteady simulation considering daily water-demand and water-hammer analysis caused by closing a valve. For the case of 24-hours daily simulation, the pressure of each node decreases as the water demand increase, and when the water demand decrease, the pressure increases. During the simulation, the amplitudes of flow and pressure variation are different in each node and the pattern of flow variation as well as water demand is quite different than that of KYPIPE2. Such discrepancy necessitates the development of unsteady flow analysis model in water distribution network system. When the model is applied to water-hammer analysis, the pressure and flow variation occurred simultaneously through the entire network system by neglecting the compressibility of water. Although water-hammer model shows the lag of travel time due to fluid elasticity, in the aspect of pressure and flow fluctuation, the trend of overall variation and quantity of the result are similar to that of water-hammer model. This model is expected for the analysis of gradual long-term unsteady flow variations providing computational accuracy and efficiency as well as identifying pollutant dispersion, pressure control, leakage reduction corresponding to flow-demand pattern, and management of long-term pipeline net work systems related with flowrate and pressure variation in pipeline network systems

Tracer Experiment for the Investigation of Urban Scale Dispersion of Air Pollutants - An Improved Method for the Release and Determination of Perfluorocarbon Tracers in the Urban Atmosphere (추적자 확산 실험에 의한 서울 도심 확산 현상 연구 - 도시규모 대기확산 실험을 위한 PFCs 추적자 방출 및 분석 시스템의 개발 및 적용 연구)

  • Yoo, Eun-Jin;Lee, Chong-Bum;Ro, Chul-Un;Kim, Hye-Kyeong;Lee, Gang-Woong
    • Journal of Korean Society for Atmospheric Environment
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    • v.23 no.5
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    • pp.547-556
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    • 2007
  • The release, sampling and analytical methods have been developed and tested for perfluorocarbons (PFCs) atmospheric tracers in order to gain insight into the atmospheric transport and dispersion over the urban conditions of Seoul, Korea. Although PFCs tracer experiments provide unique opportunities to test local and urban scale of transport and dispersion, no previous experiment with PFCs has been conducted in Korea. PMCH and PDCH were chosen as targeted tracers in our study due to their extreme low ambient concentrations and great sensitivities among various PFCs. For PFCs release system, a set of micro-metering pump, electronic balance, vaporizing furnace and high speed blower was constructed for precise and accurate release of tracers. The precision of released rate by this system was estimated to be 1%. Samplings of PFCs were carried out by fabricated portable air samplers with micro pumps and rotameters into glass tubes packed with 150 mg of Carboxen-569. The uncertainty of these sampling system was maintained below 14%. PMCH and PDCH were quantified in GC/ECD with preconditioned injection system to eliminate the interference compounds using traps and subsequent catalytic conversion system prior to column separation. Three intensive field test were undertaken during the springtime of 2002 to 2004 in eastern part of Seoul. Daily background samples were collected to characterize the background levels of PMCH and PDCH prior to their release. The observed background concentrations of PMCH ranged from 3.5 to 10.1 fL/L and varied randomly in location and time in this study. Its mean and standard variation of background concentration ($6.8{\pm}1.9\;fL/L$) are higher than those ($3.2{\sim}5.8\;fL/L$) of other historic tracer studies. Identified uncertainty for background PMCH was $1.7{\sim}2.0\;fL/L$ using this analytical system. Combined relative uncertainty in determining the tracer's concentrations was estimated as 17%. However, its background concentrations and uncertainty in concentration determination were found to be low and stable enough for tracer study.

Self-Sensing and Interfacial Property of Carbon Nanofiber/Epoxy Composites with Different Aspect Ratios (형상비가 다른 탄소나노섬유/에폭시 복합재료의 자체 감지능 및 계면특성)

  • Jang, Jung-Hoon;Kim, Pyung-Gee;Kim, Sung-Ju;Wang, Zuo-Jia;Park, Joung-Man;Yoon, Dong-Jin
    • Journal of Adhesion and Interface
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    • v.9 no.1
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    • pp.3-8
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    • 2008
  • Self-sensing was evaluated for carbon nanofiber (CNF)/epoxy composites with two different aspect ratios via electro-micromechanical technique and wettability test. Volumetric electrical resistance was measured to evaluate the comparative dispersion degree indirectly and it decreased due to the increase of electric contacts with increasing CNF concentration. The dispersion degree was evaluated indirectly by calculating coefficient of variation (COV) of volumetric electrical resistance. The CNF type A with a high aspect ratio showed better self-sensing than the case of CNF type B with a short aspect ratio. The CNF type B/epoxy composite showed little self-sensing at a concentration higher than 2 vol% probably due to poor dispersion. The apparent modulus of CNF type B was higher than that of CNF type A due to the orientation effect and the high surface area. The thermodynamic work of adhesion was consistent with the result of apparent modulus.

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A Study on Statistical Properties of Vickers Hardness of Friction Welded Parts in Alloy718 Steel (Part 1. As-welded) (Alloy718 마찰용접재의 비커스 경도의 통계적 성질에 관한 연구 (As-welded 재의 경우를 중심으로))

  • Kwon, Hyeok-Yong;Choi, Sung-Yoong;Lee, Sang-Yeal;Kong, Yu-Sik;Kim, Seon-Jin
    • Journal of Ocean Engineering and Technology
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    • v.22 no.5
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    • pp.87-93
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    • 2008
  • The objective of this paper is the investigation of the statistical properties of Vickers hardness (HV) of friction welded parts in nickel based super resisting steel, alloy 718 steel. First, we examine the statistical properties on the case of as-welded parts. Several Virkers indentations were made under same nominal conditions. This was repeated for three different applied loads, 100, 200 and 300g with a duration time, 10 second. The arithmetic mean of Vickers hardness in base metal (BM) materials is larger than that of HAZ in all applied loads. The measure of dispersion, that is, the coefficient of variation (COV) for BM and HAZ is decreased by increasing with the applied load. The distribution of Vickers hardness was not found to be symmetric type. The probability distribution of Vickers hardness was well followed Weibull distribution. The shape parameter and the scale parameter (characteristic hardness) are increased by increasing with the applied load, as both BM and HAZ.