• 한국결정성장학회지
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• 제7권4호
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• pp.560-566
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• 1997

Seeded vapor transport법에 의해 성장된 ZnSe 결정내에서 전위거동을 살펴보았다. (111)과 (100) ZnSe wafer의 etch pit 형상을 관찰하였고 성장된 결정이 높은 전위밀도를 가지면 전위들이 lineage와 cellular 두 가지 형태로 배열됨을 알았다. Seed로부터 측방성장된 부위에서 전위밀도의 변화는 없었으나 수직 성장방향으로는 전위밀도가 감소하였고, 같은 wafer내에서 전위밀도는 wafer center 지역의 전위밀도가 edge부위의 전위밀도 보다 낮았다. 성장된 결정의 평균 전위밀도는 $4{\times}10^4 /\textrm{cm}^2$이었다.

• Interaction and multiscale mechanics
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• 제1권4호
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• pp.437-448
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• 2008

This paper examined the stability of high-dense dislocation substructures (HDDSs) associated with martensite laths in High Cr steels supposed to be used for FBR, based on a series of dislocation dynamics (DD) simulations. The DD simulations considered interactions of dislocations with impurity atoms and precipitates which substantially stabilize the structure. For simulating the dissociation processes, a point defect model is developed and implemented into a discrete DD code. Wall structure composed of high dense dislocations with and without small precipitates were artificially constructed in a simulation cell, and the stability/instability conditions of the walls were systematically investigated in the light of experimentally observed coarsening behavior of the precipitates, i.e., stress dependency of the coarsening rate and the effect of external stress. The effect of stress-dependent coarsening of the precipitates together with application of external stress on the subsequent behavior of initially stabilized dislocation structures was examined.

• Nuclear Engineering and Technology
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• 제45권3호
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• pp.385-392
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• 2013

Zirconium and zirconium alloys are widely used as nuclear reactor core materials such as fuel cladding and guide tubes because they have excellent corrosion- and radiation-resistant properties. In the reactor core, zirconium alloys are subjected to high-energy neutron fluence, causing radiation-induced dislocation and growth. To discern a possible correlation between radiation-induced dislocation and growth, characteristics of dislocation and growth in zirconium and its alloys are examined. The radiation-induced dislocation including and dislocation loops is reviewed in various temperature and fluence ranges, and their growth behavior is examined in the same way. To further a fundamental understanding, radiation-induced growth prediction models are briefly reviewed. This research will assist in the design of zirconium based components as well as the safety analysis of various reactor conditions, in both research and commercial reactors.

• Nuclear Engineering and Technology
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• 제53권7호
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• pp.2304-2311
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• 2021

The dislocation density in strain-hardened Alloy 690 was analyzed using scanning transmission electron microscopy (STEM) to study the relationship between the local plastic strain and susceptibility to primary water stress corrosion cracking (PWSCC) in nuclear power plants. The test material was cold-rolled at various thickness reduction ratios from 10% to 40% to simulate the strain-hardening condition of plant components. The dislocation densities were measured at grain boundaries (GB) and in grain interiors of strain-hardened specimens from STEM images. The dislocation density in the grain interior monotonically increased as the strain-hardening proceeded, while the dislocation density at the GB increased with strain-hardening up to 20% but slightly decreases upon further deformation to 40%. The decreased dislocation density at the GB was attributed to the formation of deformation twins. After the PWSCC growth test of strain-hardened Alloy 690, the fraction of intergranular (IG) fracture was obtained from fractography. In contrast to the change in the dislocation density with strain-hardening, the fraction of IG fracture increased remarkably when strain-hardened over 20%. From the results, it was suggested that the PWSCC growth behavior of strain-hardened Alloy 690 not only depends on the dislocation density, but also on the microstructural defects at the GB.

• 한국정밀공학회:학술대회논문집
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• 한국정밀공학회 2005년도 춘계학술대회 논문집
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• pp.1390-1393
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• 2005

The hardening model based on the dislocation mechanics is employed to study the experimentally observed high tensile elongations of NiAl along the [110] orientation at intermediate temperatures. In the hardening model proposed, a mobility of dislocation is assumed to be restricted to glide through the slip plane by forest dislocation and thermally activated cross-slip event. Overall deformation behavior of NiAl was greatly influenced by temperature-dependent dislocation mobility that both experimental and simulated yield stresses decreased as temperature increased. The results of simulation showed anomalous hardening behaviors analogous to those of experiment at certain circumstances. This behavior occurred due to the hardening contributions generated by cross-slip events that disable the dislocation motion in the primary slip systems. By comparing simulation results with experiments, it is confirmed that the proposed hardening model can represent anomalous tensile elongations due to the hardening by forest dislocations and cross-slip events.

• 소성∙가공
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• 제13권2호
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• pp.160-167
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• 2004

In order to theoretically analyze the creep behavior of high Cr steel at $600^{\circ}C$, a unified elasto-viscoplastic constitutive model based on the consideration of dislocation density is proposed. A combination of a kinetic equation describing the mechanical response of a material at a given microstructure in terms of dislocation glide and evolution equations for internal variables characterizing the microstructure provides the constitutive equations of the model. Microstructural features of the material such as the grain size and spacing between second phase particles are directly implemented in the constitutive equations. The internal variables are associated with the total dislocation density in a simple model. The model has a modular structure and can be adjusted to describe a creep behavior using the material parameters obtained from uniaxial tensile tests.

• 한국재료학회지
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• 제20권1호
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• pp.7-11
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• 2010

Yttria stabilized zirconia (Y-CSZ) single crystals show plastic deformation at high temperatures by activating dislocations. The effect of strain rate on the plastic behavior of this crystal was studied. As increasing strain rate from $\varepsilon=1.04\times10^{-5} sec^{-1}$ to $2.08\times10^{-5} sec^{-1}$ the yield drop was suppressed and resulted in higher Young's modulus and yield stress. Dislocation structures of the strained crystals were analyzed using a transmission electron microscope to elucidate the plastic behavior of these crystals. In the early stage of plastic deformation, dislocation dipoles and prismatic dislocation loops were formed in both samples. However, dislocation density was increased by increasing strain rate. Strong sessile dislocations were observed in the sample with higher strain rate, which may cause the higher work hardening.

• 소성∙가공
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• 제17권1호
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• pp.46-51
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• 2008

Polycrystalline materials such as steels(BCC) and aluminum alloys(FCC) show the strain hardening and the strain rate hardening during the plastic deformation. The strain hardening is induced by deformation resistance of dislocation glide on some crystallographic systems and increase of the dislocation density on grain boundaries or inner grain. However, the phenomenon of the strain rate hardening is not demonstrated distinctly in the rage of $10^{-2}$ to $10^2/sec$ strain rate. In this paper, tensile tests for various strain rates are performed in the rage of $10^{-2}$ to $10^2/sec$ then, specimens are extracted on the same strain position to investigate the microscopic behavior of deformed materials. The extracted specimens are investigated by using the electron backscattered diffraction(EBSD) and transmission electron microscopy(TEM) results which show the effect of texture orientation, grain size and dislocation behavior on the strain rate hardening.

• 소성∙가공
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• 제30권5호
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• pp.226-235
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• 2021

The strain aging behavior of a low carbon dual phase steel was examined in two conditions: representing room temperature strain aging (100 ℃ × 1 hr after 7.5 % prestrain) and bake hardening process (170 ℃ × 20 min after 2 % prestrain), basing on carbon effective diffusion and dislocation distribution. The first principle calculations revealed that (Mn or Cr)-vacancy-C complexes exhibit the strongest attractive interaction compared to other complexes, therefore, act as strong trapping sites for carbon. For room temperature strain aging condition, the carbon effective diffusion distance is smaller than the dislocation distance in the high dislocation density region near ferrite/martensite interfaces as well as ferrite interior considering the carbon trapping effect of the (Mn or Cr)-vacancy-C complexes, implying ineffective Cottrell atmosphere formation. Under bake hardening condition, the carbon effective diffusion distance is larger compared to the dislocation distance in both regions. Therefore, formation of the Cottrell atmosphere is relatively easy resulting in to a relatively large increase in yield strength under bake hardening condition.

• 한국소성가공학회:학술대회논문집
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• 한국소성가공학회 2003년도 춘계학술대회논문집
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• pp.111-115
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• 2003

Nanoindentation is simply an indentation test in which the length scale of the penetration is measured in nanometres rather than microns or millimetres, the latter being common in conventional hardness tests. Three-dimensional molecular dynamics simulations have been conducted to evaluate the nanoindentation test. Molecular dynamics simulations were carried out on single crystal copper by varying crystal orientations to investigate nano-behavior of material beneath an indenter in nanoindentation. Morse potential function was used as an interatomic force between indenter and thin film. The result of the simulation shows that crystal orientation significantly influenced the slip system, dislocation nucleation and dislocation behavior.