• 열처리공학회지
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• 제8권4호
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• pp.302-317
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• 1995

After initial structure of AISI 9260 steel is changed into pearlite and martensite, one is isothermally annealed at $700^{\circ}C$ below of $A_1$ transformation point and the other is isothermally annealed at the same condition after 3 cycles of heating and cooling between $680^{\circ}C$ and $780^{\circ}C$ of $A_1$ transformation point. Analyzing the changes of microstructure, mechanical properties and fractography of tension test, we obtained result as follows. The fastest spheroidization rate by changes of initial structure and heat treatment cycles is appeared at the heat treatment cycle which is isothermally annealed after 3 cycles of heating and cooling at below and above $A_1$ transformation point for martensite. At the above condition, the perfect spheroidization structure is appeared after 60hrs and after then, globular carbide is being coarsened. The mean diameter of globular carbide is $2.4{\times}10^{-3}mm$ after 90hrs. The changes of tension strength during spheroidization heat treatment follows Orwan function, ${\sigma}_o={\sigma}_i+Gb/l$, where l is interspacing of carbide particles and at the above condition, ${\sigma}_o=70.48+2.5{\times}10^{-3}/l(kg/mm^2)$. Fractography of fracture of spheroidization structure in tension test is appeared as dimple which is ductile rupture type by nucleation and growth of void, size of dimple is larger and deeper with increasing of heat treatment time.

• 구강회복응용과학지
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• 제38권3호
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• pp.138-149
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• 2022

치과용 세라믹의 파절실험 후 파절이 발생한 원인을 분석하면 세라믹의 임상적용 가능성을 높일 수 있다. 파절원인을 파악하기 위한 파단면분석은 주사전자현미경 등 영상기술의 발달로 점차 널리 적용되고 있는데 이를 정확히 해석하기 위해서는 실험조건 설정이 중요하다. 파절시편이 오염되지 않도록 보관하고 세척하며, 관찰을 위해 금속 전처리가 필요하다. 파절은 양상에 따라 주로 금속에서 관찰되는 보조개모양 파절, 열개, 분리파손 및 세라믹에서 관찰되는 피로파절과 조가비 모양 파절이 있다. 세라믹의 주된 파절원인인 피로파절을 실험실에서 재현하기 위해 느린 균열성장을 관찰할 수 있는 동적 하중이 필수적이며 하중조건과 하중횟수 등을 적절히 설정해야 한다. 세라믹의 파단면에서 나타나는 대표적인 특징은 해클이며 다양한 해클의 형태를 잘 관찰하여 세라믹 파절의 원인과 과정을 분석할 수 있도록 하는 것이 필요하다. 파단면분석은 치과용 세라믹의 파절을 심층적으로 파악할 수 있는 유용한 방법이므로 정확한 실험과정을 따르고 결과해석에 유의해야 한다.

• Journal of Welding and Joining
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• 제32권1호
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• pp.93-101
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• 2014

This study aims to investigate the effect of heat input of outside SAW weld on low temperature toughness($-20^{\circ}C$) of inside SAW weld for API 5L X70 with sour gas resistance. As increasing heat input of the outside weld, low temperature toughness of the inside weld was decreased. Especially, in spite of the same heat input, the value of low temperature toughness was fluctuated. On the basis of fracture and microstructure analysis, the low temperature toughness is correlated with the fracture area ratio of shear lips and four kinds of fracture sections. These sections were divided with size and shape of dimple correlated with grain boundary ferrite and cleavage correlated acicular and polygonal ferrite in grain. Therefore, it was seen that these sections were two of final solidification area in the inside weld and the outside weld, no reheated zone and reheated zone in the inside weld. In conclusion, it is thought that the difference of low temperature toughness at the same heat input is due to the fact that each of impact test specimens could have the different microstructure, even though the notch was machined under the error tolerance of 1mm. It is because the final solidification area of the inside weld is very narrow.

• Journal of Welding and Joining
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• 제15권1호
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• pp.92-100
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• 1997

손상된 ASTM A-470 class 8 고압 증기 터어빈 로터강의 수명 연장을 위해 보수 용접이 행하여졌다. SAW 용접부의 미세경도 측정결과 모재의 경도는 VHN 253이었으나 모재에 근접한 열영향부의 경도는 VHN 227로 떨어졌다. 이와 같이 경도가 떨어진 영역을 "연화층"이라 정의하였으며 약 0.5-0.6mm의 크기를 나타내었다. 한편 크립 파단 시험시 파괴는 연화층 부근에서 일어났으며 593.deg. C와 19Ksi(132 Mpa)에서 파단시간은 772.4hr이었다. 연화층의 크기를 줄이기 위해서 MIG 및 TIG 용접이 행하여졌는데 연화층 크기는 MIG의 경우 0.3-0.4mm이고, TIG의 경우에는 입열량의 크기에 따라 0부터 0.4mm의 크기를 나타내었다. 그러나 크립 파단시간은 연화층 크기가 작아질수록 감소하였다. 특히 TIG 용접부의 경우 크립 파단시간은 입열량과 밀접한 관계를 나타내었는데 입열량이 클수록 파단시간은 길어졌다. 대부분의 파괴는 ICHAZ에서 발생되었으나 입열량이 감소함에 따라 파단부는 CGHAZ으로 이동하였다. 파단면은 tearing과 dimple을 갖는 입내파괴를 나타내었다.파괴를 나타내었다.

• Journal of Welding and Joining
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• 제27권3호
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• pp.73-79
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• 2009

This present paper investigated the mechanical properties and the microstructures of each penetration shapes classifying the conduction shape area and the keyhole shape area about electron beam welded 120(T)mm thick plated aluminum 5052 112H. As a result the penetration depth is increased linearly according to the output power, but the aspect ratio is decreased after the regular output power. In the conduction shape area, the Heat affected zone is observed relatively wider than the keyhole shape area. In the material front surface of the welded specimen, the width is decreased but the width in the material rear surface is increased. After the measuring the Micro Vikers Hardness, it showed almost similar hardness range in all parts, and after testing the tensile strength, the ultimate tensile strength is similar to the ultimate tensile strength of the base material in all the specimens, also the fracture point was generated in the base materials of all the samples. In the result of the impact test, impact absorbed energy of the Keyhole shape area is turned up very high, and also shown up the effect about four times of fracture toughness comparing the base material. In the last result of observing the fractographs, typical ductile fraction is shown in each weld metal, and in the basic material, the dimple fraction is shown. The weld metals are shown that there are no other developments of any new chemical compound during the fastness melting and solidification.

• 한국재료학회지
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• 제30권1호
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• pp.8-13
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• 2020

Effect of heat treatment on microstructure and mechanical properties of an Fe-6.5Mn-0.08C medium-manganese steel is investigated in this study. Three kinds of medium-manganese steel specimens are fabricated by varying heat treatments of intermediate quenching (IQ), step quenching (SQ), and intercritical annealing (IA). Hardness and tensile tests are performed to examine the correlation of microstructure and mechanical properties for the Fe-6.5Mn-0.08C medium-manganese steel specimens. The IQ and SQ specimens have microstructures of martensite matrix with ferrite, whereas IA specimen exhibits microstructure of acicular ferrite matrix with martensite. The tensile test results show that the SQ specimen with martensite matrix has the highest yield strength and the lowest elongation. On the other hand, the SQ specimen has the highest hardness due to the relatively lower reduction of carbon content in martensite during intercritical annealing. According to the fractography of tensile tested specimens, the SQ specimen exhibits a dimple and quasi-cleavage fracture appearance while the IQ and IA specimens have fully ductile fracture appearance with fine-sized dimples caused by microvoid coalescence at ferrite and martensite interface.

• Restorative Dentistry and Endodontics
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• 제32권2호
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• pp.130-137
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• 2007

본 연구의 목적은 니켈티타늄 전동파일의 피로파절에 있어서 표면 결함의 역할을 규명하고자 fatigue tester에서 반복적 인 fatigue force를 부여한 후 파절된 단면을 주사전자현미 경으로 관찰하여 파절 역학을 규명하는 것이다. 총 45개의 #30/.04 taper와 21 mm의 HEROShaper 니켈-티타늄 전동파일을 15개씩 3개의 군으로 분류하였다. 제 1군은 결함이 없는 새 HEROShaper파일, 제 2군은 제조과정에서 metal rollover나 machining marks와 같은 표면결함을 갖는 HEROShaper파일, 제 3군은 임상에서 4- 6개의 구치부 근관의 확대에 사용한 HEROShaper 파일을 사용하였다. 모든 파일들은 회전속도(300 rpm)와 pecking distance (3 mm)가 일정하게 맞춘 fatigue tester에서 파절될 때까지 시간을 측정한 후 통계분석을 통해 각 군간의 유의성을 분석하였고, 파절 단면의 farctographic analysis를 통해 파절역학을 규명하고자 하였다 실험결과 평균 파절시간에 있어서 group 1과 2, group 1과 3사이에는 통계학적으로 유의할 만한 차이가 있었으나 (p<0.05), group 2와 3사이에는 통계학적인 차이가 없었다. Fractographic analysis 결과 대부분의 파절면에서 microvoid와 dimple 소견을 갖는 ductile fracture양상이 관찰되었다. 또한 brittle fracture가 일어난 파절면에서는 파절선 전방에 수 많은 striation들이 관찰되었고 transgranular 및 intergranular cleavage 소견도 보였다. 표면결함이 있는 제 2, 3 군의 파절단면에서는 모든 시편에서 표면결함이 관찰되었다. 이와 같은 결과로 미루어 보아 표면결함이 반복 피로파절에서 미세균열의 기시점으로 중요한 역할을 하며 fractography분석법은 Ni-Ti 파일의 파절역학을 규명하는데 유용함을 알 수 있었다.

• 열처리공학회지
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• 제14권5호
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• pp.267-274
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• 2001

Microalloyed steels, which substituted by conventional quenched and tempered steels, have been used in a wide variety of structural and engineering application. The main driving force for preference of MA steels is a cost reduction which can be achieved by an omission of heat treatment. In this study, low carbon martensitic MA steels in 0.18C-0.30(0.60)Si-2.00(1.80)Mn-0.05S-1.5Cr-0.05(0.10)V-0.015Ti(wt%) were investigated to know the effects of cooling method on the mechanical properties and microstructures of Si, Mn, V added microalloyed steel at different reheating temperature. Microstructure of oil quenched steels which were comprised lath martensite, auto-tempered martensite and retained austenite, had more various structure than that of air cooled steel made of mainly bainite. Therefore, oil quenched steels, which had more various microstructure, had better strength-toughness balance compare to air cooled steels. In the impact test, fracture mode of oil quenched steels, which showed good mechanical properties, were dimple, but that of air cooled steels were cleavage.

• Journal of Welding and Joining
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• 제19권1호
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• pp.65-74
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• 2001

A study on the corrosion behavior in case of As-welded and PWHT temperature 55$0^{\circ}C$ of welding part of RE36 steel for marine structure was investigated with parameters such as micro-Vickers hardness, corrosion potential measurement of weld metal(WM), base metal(BM) and heat affected zone(HAZ), both Al anode generating current and Al anode weight loss quantity under sacrificial anode cathodic protection conditions. And also we carried out slow strain rate test(SSRT) in order to research both limiting cathodic polarization potential for hydrogen embrittlement and optimum cathodic protection potential as well as mechanical properties by post-weld heat treatment(PWHT) effect. Hardness of HAZ was the highest among three parts(WM, BM and HAZ) and the highest galvanic corrosion susceptibility was HAZ. And the optimum cathodic polarization potential showing the best mechanical properties by SSRT method was from -770mV to -875mV(SCE). In analysis of SEM fractography, applied cathodic potential from -770mV to -875mV(SCE) it appeared dimple pattern with ductile fracture while it showed transgranular pattern (Q. C : quasicleavage) under -900mV(SCE). However it is suggested that limiting cathodic polarization potential indicating hydrogen embrittlement was under -900mV(SCE).

• 열처리공학회지
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• 제14권4호
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• pp.212-219
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• 2001

The fatigue test was carried out to evaluate the fatigue characteristics of fire resistance steel for frame structure and heat affected zone (HAZ) by the one side Gas Metal Arc Welding (GMAW). In this paper, the fatigue crack growth behavior was investigated with the compact tension specimen of base metal and the HAZ according to chemical composition and rolling end temperature, respectively. And the acoustic emission signals obtained from the fatigue test were analyzed by the time-frequency analysis method as a nondestructive evaluation. Main results obtained are summarized as follows; The hardness was appeared softening phenomenon that weld metal and HAZ are lower than that of base metal. Fatigue life of welded specimen was longer than that of base metal. m was 3~4.5 in base metal and 3.8~5.8 in HAZ. The main frequency range of acoustic emission signal analyzed from time-frequency method is different with the range by noise and crack. Also, it could be classified that it was also generated by fracture mechanics of dimple, inclusion etc.