The effects of protease and/or lipase on the removal of protein soil and oily soil were investigated in this study. Cotton, rayon, nylon, and PET fabrics were soiled by padding of fresh bovine blood and spotting of mixed artificial sebum evenly. The soiled fabrics were aged at $130^{\circ}C$ for 30 minutes. The fabrics were washed by using Terg-O-Tometer at various conditions. Protease and/or lipase were added in the alcohol ethoxylate (AE) detergent solution. The removal efficiency was evaluated by analysis of protein and/or oil on the fabrics before and after washing, respectively. The detergency of protein and/or oil on the fabrics was discussed with enzyme concentration, washing time, washing temperature, pH of washing solution and fiber characteristics. The hydrolysis of protease improved effectively the removal of oil as well as protein by increasing removal of protein-oil mixed soil at the same time. The effect of lipase added detergent solution was slightly shown on the removal of oil and/or protein. The removal of mixed soils from cotton fabrics was very low because of large amount of residual soils caused by the physical characteristics of cotton fiber.
Journal of the Korean Society of Clothing and Textiles
/
v.23
no.7
/
pp.1064-1072
/
1999
Nylon fabric was grafted for the purpose of the development of detergency against the hemoglobin as a protein soil. By free-radical producing chemical initiator systems the graft using acrylic acid(AA) as a hydrophilic vinyl monomer was performed to change surface energies in the presence of ammonium persulfate(APS) as an initiator and then acrylic acid grafted Nylon was treated with NaOH solution. The surface morphology for Nylon-g-NaAA with changing graft rate were studied by scanning electron microscopy (SEM) The properties of the Nylon such as diameter tenacity elongation contact angle and the hemoglobin removal were also investigated. The diameter of grafted Nylon fiber increased as the graft ratio increased. The tenacity of grafted Nylon also increased with increasing graft ratio up to 15% The elongation however decreased gradually according to graft, The contact angle decreased after graft and alkaline treatment. The amount of hemoglobin on the grafted Nylon increased in proportion to the graft ratio. Hemoglobin was easily removed from grafted Nylon while it was difficult to be removed from ungrafted Nylon. The detergency of hemoglobin for grafted Nylon decreased when the graft ratio exceeded 15% The removal of hemoglobin increased markedly with increasing hemoglobin content and revolution speed. Therefore the removal of hemoglobin was improved due to graft and alkaline treatment.
Alkyl polyglucosides (APG), so called natural nonionic surfactants, are prepared with glucose from corn starch and fatty alcohol from palm and/or coconut oil. When we studied on interfacial properties of APG, surface and interfacial tension, cmc, foaming and effectiveness, according to degree of polymerization of glucose unit (D.P.=1.2~1.8) and alkyl chain length, the former hardly affects but the latter greatly affects on them. The order of detergency for fatty acid soils decreased as followings ; APG 0814> APG 1214> APG 10> APG 0810> APG 08, and the samples with lowest interfacial tension and maximum adsorption had a better detergency.
Interfacial tension between liquid soil and aqueous solution of surfactant can be obtained from theoretical and/or experimental data. A correlation factor(r) between work(Wac) from theotical interfacial tension and detergency was 0.93 at lower concentration(0.04%) and 0.37 at higher concentration(0.1%) but a correlation factor(r) from experimental data(Wae) was 0.95 and 0.84, respectively. There were, therefore, good correlation between adhesional work and detergency at lower concentration but large deviation between them from theoretical and experimental one at higher concentration.
Journal of the Korean Society of Clothing and Textiles
/
v.25
no.5
/
pp.991-1001
/
2001
This study has examined effects of protease on the removal of hemoglobin and triolein mixed soil with changes of soil content and soil composition from cotton and PET filament fabrics. The results obtained were as follows: The results obtained were as follows: 1) The detergency of PET fabrics was higher than that of cotton fabrics. The removal of hemoglobin was much higher than that of triolein from cotton fabrics, while the removal of hemoglobin was similar to that of triolein from PET fabrics. 2) The removal efficiency of hemoglobin and triolein was improved by protease from cotton and PET fabrics. Especially the removal efficiency of those was remarkably improved from cotton fabrics which the removal of soil was lower than PET fabrics. And the removal of hemoglobin and triolein by adding protease was increased with increase of hemoglobin content of mixed soil from cotton fabrics. 3) With the increase of hemoglobin content of mixed soil, the removal of hemoglobin was drastically increased but the removal of triolein was slightly decreased from cotton and PET fabrics. With the increase of triolein content of mixed soil, the removal of hemoglobin and triolein was decreased from cotton fabrics, but those were generally increased from PET fabrics.
Journal of the Korean Society of Clothing and Textiles
/
v.41
no.3
/
pp.527-536
/
2017
This study investigated the detergency and functionality of laminating finished fabrics for outdoor wear based on repeated washing. Laminating finished fabrics were selected as the main fabrics for outdoor wear and used as test fabrics. The effects of outdoor exclusive detergent and normal neutral detergent were examined according to washing time, temperature, rpm and detergent concentration based on the use of a Terg-O-Tometer. Re-soiling of the test fabrics was measured by Florio-Mersereau. Permeability, water repellency, water resistance and absorbency were estimated to measure improvements and effects in regards to outdoor exclusive detergent in optimal washing conditions. The detergent effect of outdoor exclusive detergent was superior compared to normal neutral detergent. Re-soiling was lower with exclusive outdoor detergent than with normal neutral detergent. The measurement of functionality for laminating finished fabrics before and after washing indicated that functionality was decreased with repeated washing.
This study has examined the removal of mixed soil of protein and fat by protease. Cotton and PET fabrics were soiled by spotting of hemoglobin and triolein, respectively. The soiling order and soil concentration were changed in this procedure. The soiled fabrics were aged at 130℃ for 20 minutes. Protease was added in the alcohol ethoxylate(AE) detergent solution. The removal effciency was evaluated by analysis of protein and/or fat on the fabrics before and after washing, respectively. The detergency of PET fabrics was higher than that of cotton fabrics. The removal efficiency of hemoglobin was improved by protease from cotton and PET fabrics. Especially the removal efficiency of hemoglobin was remarkably improved from cotton fabrics. With the increase of hemoglobin and triolein (1:1) mixed soil, the removal of mixed soil was increased in proportion to mixed soil content up to a certain point. but it began to decrease above the point from cotton fabrics, while it was generally increased from PET fabrics. The detergency of total mixed soil from cotton fabrics was higher in case of soiling order with triolein after hemoglobin than in case of soiling order with triolein before hemoglobin. But the soiling order was not greatly effected in the detergency of total mixed soil from PET fabrics.
This study has examined the removal of mixed soil of protein and fat by protease. Cotton and PET fabrics were soiled by spotting of hemoglobin and triolein, respectively. The soiling order and soil concentration were changed in this procedure. The soiled fabrics were aged at $130^\circ{C}$ for 20 minutes. Protease was added in the alcohol ethoxylate(AE) detergent solution. The removal effciency was evaluated by analysis of protein and/or fat on the fabrics before and after washing, respectively. The detergency of PET fabrics was higher than that of cotton fabrics. The removal efficiency of hemoglobin was improved by protease from cotton and PET fabrics. Especially the removal efficiency of hemoglobin was remarkably improved from cotton fabrics. With the increase of hemoglobin and triolein (1:1) mixed soil, the removal of mixed soil was increased in proportion to mixed soil content up to a certain point. but it began to decrease above the point from cotton fabrics, while it was generally increased from PET fabrics. The detergency of total mixed soil from cotton fabrics was higher in case of soiling order with triolein after hemoglobin than in case of soiling order with triolein before hemoglobin. But the soiling order was not greatly effected in the detergency of total mixed soil from PET fabrics.
Journal of the Korean Society of Clothing and Textiles
/
v.47
no.2
/
pp.353-370
/
2023
In this study, the performance of ultrasonic cleaners for ultrasonic washing, which is one of the wet cleaning methods, was evaluated. The washing performances of ultrasonic cleaners were compared with commercial washing machines under normal and wool courses based on different parameters such as detergency, wrinkle formation, fabric damage, dimensional stability, and germ removal ability. Cotton, silk and wool were used in this experiment. Results revealed that the ultrasonic washing detergency of cotton fabrics was lower than that of commercial washing machines under the normal course and similar to that of commercial washing machines under the wool course. Detergency of silk fabrics was similar under both normal and wool courses. In terms of wrinkle formation and dimensional stability, ultrasonic cleaners showed lesser wrinkles and lower shrinkage than commercial washing machines. Considering damage evaluation, ultrasonic cleaners more effectively removed soil without damaging fabrics compared with commercial washing machines. The bacteria removal rate of both cotton and silk was more effective than the wool course of a commercial washing machine. Thus, this study compares the performance of ultrasonic cleaners and commercial washing machines and provides meaningful results related to ultrasonic washing performance.
Journal of the Korean Society of Clothing and Textiles
/
v.18
no.1
/
pp.23-30
/
1994
The objective of this study was to analyze the effect of the dissolution of detergent on washing and rinsing efficiency, and the possibility of saving detergent in washing. Washing and rinsing efficiency were reviewed in three different ways : A method was to input dissolved detergent by the use of rapid detergent dissolution instrument, B method was to input dissolved detergent beforehand, and C method was to input undissolved detergent. The results were as follows 1. A method > B method > C method was shown in detergency with washing time and three method's gaps were reduced because detergent dissolution effect was reduced by mechanical action in proportion of washing time. Especially, according to detergency of A method of 0.07% and C method of 0.1% was appeared approximately, saving detergent was expected by rapid dissolution of detergent. 2. A method > B method > C method was shown in detergency with washing temperature. As the washing temperature rose, the detergent reached chemically more activated state and become easily soluble. It resulted for the detergent to penetrate and adhere to laundry easily. 3. A method > B method > C method was shown in detergency with detergent concentration and C method was more sensitive than A, B method against change of detergent cocentration. Rapid detergent dissolution made it possible not only to enhance the washing efficiency but also to save the detergent because detergency of A method in low concentration is higher than that of C method. 4. A method $\geq$ B method > C method was shown in rinsing ratio with detergent input method. It indicated input dissolved detergent was advantageous in rinsing. 5. The result of anion surfactant concentration test of each process with detergent input method was shown like that A method In B method > C method in washing and reverse result was shown in rinsing. The anion surfactant concentration of C method was low during washing but high during rinsing. This was identical with previous results which shown the washing and rinsing efficiency improved with dissolved detergent usasge. 6. C method > B method > A method was shown in the degree of remaining detergent after rinsing. There was no remaining detergent after second rinsing in A and B method, but in C method four rinsings were required for the same result. Consequently, in A and B methods, less water and electricity were used, and less abrasion of cloth.
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