The dry cleaning effect related to the type of soil and fiber was analyzed using silicone and alcohol-based solvents(ethyl alcohol, isopropyl alcohol, acetone) that are relatively safe for the human body and environment to improve the detergency of hydrophilic soils in dry cleaning system. Based on this analysis, an effective dry cleaning method to be carried out for improving the detergency according to the type of hydrophilic soils. After dry cleaning was performed using 20 types of artificial soiled fabrics consisting of 7 types of fibers and 4 types of hydrophilic soils, the detergency was measured and the results were compared and analyzed by solvents and fiber types. The results are presented as follows; first, the detergency of hydrophilic soils using silicone solvents showed a low rate of detergency. In particular, the tannin soil showed a lower level of detergency compared to the protein soil. Second, the detergency of hydrophilic soils using silicon solvents with dry soap differed in some detergency according to the soil and fiber types. Especially, the detergency of curry soil on cotton fabric showed significant improvement. Third, the protein soil was not removed from dry cleaning using alcohol-based solvents, but the effect of dry cleaning of curry soil on both cotton and polyester fabric was substantially improved. As a result, the elimination of blood soil is more effective in silicon solvents than in alcohol-based solvents. The removal of tannin soils may improve detergency by adding dry soap to silicon solvents or by using alcohol-based solvents as alternative solvents. The use of alternative solvents such as silicon and alcohol solvents can contribute to the environmental improvement of the dry cleaning industry, which uses petroleum-based solvents. It is also expected to provide consumers with the opportunity to choose eco-friendly and efficient dry cleaning methods.
The effects of surface free energy of substrates on the soiling and on the detergency of the oily soil were studied. The surface tension consisted of dispersion force and polar force components of substrate, oily soil and surfactant solutions were calculated by extended Fowkes' equation. From these values, work of adhesion($W_a$), work of detergency($W_D$), ana residual work of detergency($W_{D,R}$) were calculated. The correlations between these theoretical values of the works and detergency were discussed. MAA grafted PET film was used as substrate, triolein as oily soil and nonylphenol polyoxyethylene ether(NPE) having various mole numbers of oxyethylene adducts and dodecylbenzene sulfonate (DBS) as surfactants. Detergency was estimated by means of radioactive tracer method using $C^{14}-triolein$. The results showed that $W_a$ was decreased with the increase of surface free energy of substrate. In water, $W_D\;and\;W_{D,R}$ were decreased and detergency of tiolein was increased with the increase of surface free energy of substrate. In surfactant solutions, the lower the surface free energy of substrate and the lower oxyethylene adducts of NPE were the more effective on detergency. The detergency of DBS solution was the lowest in the case of ungrafted PET film, but even small increase in surface free energy by grafting showed much increase in detergency.
In order to investigate the detergency effects of various detergents to stained polyester & cotton fabric with solid soils such as carbon black, liquid paraffin and fat, the optimum washing conditions according to the types of washing agent, the assesment of detergency effect by the measurement of reflectance after and before washing were studied. The detergency effect of various detergents to stained polyester and cotton fabric increased by using the mixtures of bleaching and enzyme detergent. In order to obtain the excellent detergency effect, 2-step treatment, the pre-washing with bleaching agent and bleaching-enzyme mixture detergent treatment is preferred. In comparison of the detergency to polyester and cotton fabric, it is assumed that the detergency to polyester stained fabric was superior than that to cotton stained fabric because of the difference of adhesive force between soil material and fabric in preparing solid stained fabric.
In order to investigate the detergency effect of stained cotton and PET fabric, respectively, these fabrics stained with solid soils such as carbon black, liquid paraffin, and fat and examined the detergency effect in the optimum washing condition. The evaluation of washing efficiency of washed fabrics studied by using the surface reflectance measurement before and after washing treatment. The maximum detergency effect of stained cotton and PET fabric obtained in the mixed washing liquor-bleachig agen(ml)/concentrated washig agent(g/l). To obtain the excellent detergency effect, 2-step washing treatment, pre-washing by bleaching agent only and washing by concentrated detergent, is preferred. In comparing the detergency of polyester and cotton fabric, the detergency of stained polyester fabric superior than that of stained cotton fabric because of the difference of adhesive force between soil material and fabric in preparing soled stained fabric. In this study, we also studied the degree of fabric damage by the measurement of tensile strength change. From the results of the tensile strength measurement, the damage of washed fabric before and after washing treatment was nearly changed.
In order to evaluate the exact effect of detergency it is necessary both to measure the actual soil content by chemical analysis and to determine the degree of soil removal visually. Since it takes considerable time and effort to use both methods, usually one of the two methods is used. Many studies have been carried out through increasing the visibility of oily soil to evaluate detergency by measuring reflectance of fabrics. In this study Sudan Black B, an oil soluble dye was used as an indicator to increase the visibility of oily soil on cotton and polyester fabrics. The condition of artificially soiled fabrics and the method of evaluating detergency were investigated which represent the actual detergency of oily soil by measuring the reflectance only. Also the detergency of Sudan Black B and that of oily soil were compared with each other under various washing conditions, As a result, the K/S values converted from the reflectances showed a good correlation with the actual soil content. Linear relationship between K/S value and the actual soil content was obtained. The K/S values of washed fabrics were higher than those of unwashed fabrics which included same content of soil since the soil visibility changed during washing. But the difference was small when Sudan Black B was used. With the increase of soil content, detergency of cotton fabric decreased, but detergency of polyester fabric increased gradually. With regards to soiled fabrics, detergency of cotton fabric measured by K/S value was close to that of actual oily soil when Sudan black B was used as an indicator.
The effects of Temperature on the removal of triglyceride were studied with soaps having various chain lengths of alkyl group. Cellophane, polyester film and alkali-treated polyester film were soiled with tripalmitin, tagged with 0" and detergency was evaluated by analysing the tripalmitine on the fabric before and after washing by means of liquid scintillation counting. The results were as following: 1) Triglyceride was completely removed from cellophane in distilled water without surfactant at any temperature, because of the hydrophillic nature of cellulose. The detergency of triglyceride from polyester film fully depended on the state of tripalmitin. The detergency of alkali treated polyester film was better than that of untreated polyester film at lower temperature due to increased hydrophillcity, but worse at higher temperature due to the diffusion of molten tripalmitin into the grooves, formed by alkali treatment. 2) The detergency from polyester film was increased with elevating temperature and after reaching some optimum detergencies, the detergencies were rather decreased with increasing temperature. The temperatures of optimum detergency were shifted to higher with increasing chain length of alkyl group. 3) When the soiled film was baked at $60^{\circ}C$ and $70^{\circ}C$ for 20 min, the detergency vs. temperature was much the same as the case of without-baking. These results indicate that the detergency of triglyceride was largely correlated with the suspending power of surfactants at low temperature and with state of soil and hydrophilicity of substrates with elevating temperature.
This study investigates the effect of mixed characteristics of oily soil such as mixed ratio, polarity of oily soil on contact angle of fabric, removal of oily and particulate soil from PET fabric in oily/particulate soil mixed system. The contact angle of fabric in the surfactant solution with suspended oily soil was examined as a fundamental environment of detergency of soil from fabrics. Detergency was investigated as function of mixed ratios of oily/ particulate soil, type of oily soil, surfactants concentration, surfactant type and temperature of detergency in surfactant solution. The contact angle of fabric in surfactant solution sharply increased with mixing nonpolar oily soil; in addition, the contact angle slightly increased with increasing contents of oily soil and decreased with increasing surfactant concentration. The removal of oily and particulate soil from fabric was higher in the solution mixed with polar versus nonpolar oily soil. The detergency increased with increasing surfactant concentration and the increased temperature of surfactants solution that were relatively improved in NPE compared to DBS solutions, The results indicated that the detergency of oily and particulate soil showed a similar trend in oily/ particulate mixed soil systems. The general contact angle of fabric was well related with the detergency of oily and particulate soil in oily/particulate mixed soil system, therefore, the primary factor determining the detergency of soil in oily/particulate mixed soil system may be the contact angle of fabric caused by wettability.
In order to investigate the detergency of the mixture of compact detergent and bleaching agent to fabric stained with a coffee and a red wine, respectively, and a japanese wet stained fabrics, to evaluation of detergency was studied under various washing conditions. In order to study the effect of alkaline agent addition on the detergency, the soda ash was added in the compact detergent system. The results are as follows : In a low temperature washing condition, the alkalinity of washing liquor effected more the removal of the composite stained fabrics than that of oilic stained fabrics. For the colored stained fabric such as red wine stained sample, the influence of the repeated washing treatment on the detergency was not significant factor. On the other hand, the influence of the repeated washing treatment for the coffee stained and japanese wet stained fabric on the detergency was gradually increased.
The purpose of this research is to improve sustainable clothes care by comparing household washer's standard course and quick course. Detergency at each course was classified by laundry weight, detergent concentration, and soils. Also, fabric damage from each course was compared. Washing experiments were carried out using two types of washing machines and three types of detergents. Using the standard soiled fabrics of EMPA 108 set, detergency was compared by laundry weight, soil, and detergent concentration. Additionally, fabric damage was evaluated using the mechanical action of MA-40. The results of the research were as follows. First, a standard course, having more working time exhibited better detergency than a quick course. However, the detergency deviation under 6kg laundry weight was as low as 9.0%. Second, detergency by the type of soil was more effective in standard course than in a quick course, but hydrophilic protein soils had a small detergency deviation at 7.6%. Moreover, hydrophobic oil, complex, and particulate soils had a higher deviation at 19.7% Third, fabric damage was in proportion to operating time. Fourth, a quick course showed approximately 80% detergency regardless of the type of detergent. in the case of using 50% of the recommended allowance by the detergent manufacturer. In conclusion, reducing the operating washing time and detergent concentration is in accordance with increasing sustainability, in the case of washing with lightly soiled fabrics under 6kg of laundry weight.
This study was designed to investigate the influence of ratio of anionic/nonionic surfactant mixture on detergency of particulate soil under various solutions. The detergency of the particulate soil was determined by adhesion of particle to fabric and its removal from fabric separately. The PET fabric and ${\alpha}-Fe_2O_3$were used as materials of textile and model of particulate soil, respectively. The detergency was investigated as a function of surfactants concentration, ionic strength, kinds of electrolyte and mole numbers of oxyethylene ether of nonionic surfactant in different ratio of anionic/nonionic surfactant mixture. Although some deviations exist, the adhesion of particle to fabric generally increased with decreasing its removal from fabric. The detergency of particulate soil on PET fabric was relatively higher in anionic/nonionic surfactant mixed solution than in each single surfactant solution, but the influence of ratio of anionic/nonionic surfactant mixture on detergency of particulate soil was low. Generally the detergency of particulate soil on fabric was at its maximum at 0.1% surfactant concentration, $1{\times}10^{-3}$ ionic strength, $Na_5P_3O_{10}$ electrolytes and 10 mole numbers of oxyethylene ether of nonionic surfactant, regardless of ratio of anionic/nonionic surfactant mixture.
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