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Magnetron Sputter Coating of Inner Surface of 1-inch Diameter Tube

  • Han, Seung-Hee;An, Se-Hoon;Song, In-Seol;Lee, Keun-Hyuk;Jang, Seong-Woo
    • 한국진공학회:학술대회논문집
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    • 한국진공학회 2015년도 제49회 하계 정기학술대회 초록집
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    • pp.135-135
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    • 2015
  • Tubes are of extreme importance in industries as for fluid channels or wave guides. Furthermore, some weapon systems such as cannons use the tubes as gun barrels. To increase the service life of such tubes, a protective coating must be applied to the tubes' inner surface. However, the coating methods applicable to the inner surface of the tubes are very limited due to the geometrical restriction. A small-diameter cylindrical magnetron sputtering gun can be used to deposit coating layers on the inner surface of the large-bore tubes. However, for small-bore tubes with the inner diameter of one inch (~25 mm), the magnetron sputtering method can hardly be accommodated due to the space limitation for permanent magnet assembly. In this study, a new approach to coat the inner surface of small-bore tubes with the inside diameter of one inch was developed. Instead of using permanent magnets for magnetron operation, an external electro-magnet assembly was adopted around the tube to confine the plasma and to sustain the discharge. The electro-magnet was operated in pulse mode to provide the strong axial magnetic field for the magnetron operation, which was synchronized with the negative high-voltage pulse applied to the water-cooled coaxial sputtering target installed inside the tube. By moving the electro-magnet assembly along the tube's axial direction, the inner surface of the tube could be uniformly coated. The inner-surface coating system in this study used the tube itself as the vacuum chamber. The SS-304 tube's inner diameter was 22 mm and the length was ~1 m. A water-cooled Cu tube (sputtering target) of the outer diameter of 12 mm was installed inside of the SS tube (substrate) at the axial position. The 50 mm-long electro-magnet assembly was fed by a current pulse of 250 A at the frequency and pulse width of 100 Hz and 100 usec, respectively. The calculated axial magnetic field strength at the center was ~0.6 Tesla. The central Cu tube was synchronously driven by a HiPIMS power supply at the same frequency of 100 Hz as the electro-magnet and the applied pulse voltage was -1200 V with a pulse width of 500 usec. At 150 mTorr of Ar pressure, the Cu deposition rate of ~10 nm/min could be obtained. In this talk, a new method to sputter coat the inner surface of small-bore tubes would be presented and discussed, which might have broad industrial and military application areas.

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대룡산 토석류 특성 분석 및 위험지역 예측에 관한 연구 (Characteristic Analysis and Prediction of Debris Flow-Prone Area at Daeryongsan)

  • 최영남;이형호;유남재
    • 한국지리정보학회지
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    • 제21권3호
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    • pp.48-62
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    • 2018
  • 본 연구에서는 2013년 7월 강원도 춘천시와 홍천군에 위치한 대룡산에서 발생한 토석류 산사태 현장 51개소를 조사하고 강우와 현장조사 자료를 바탕으로 토석류의 거동특성을 분석하였다. 사면형과 계곡형 토석류에 따라 발생부와 퇴적부의 위치 및 경사 그리고 침식 폭 및 두께를 토석류 전 구간에 대해 조사하였다. 또한, 1:5,000의 수치지형도를 통해 대룡산의 DEM(Digital Elevation Model)을 구축하고 SINMAP(Stability INdex MAPping)을 이용하여 산사태 위험도를 평가하고 실제발생 위치와 비교 분석하였다. 분석결과 사면형 토석류는 위험지역과 실제발생 위치가 유사한 것으로 나타났으며, 계곡형의 경우 SINMAP(Stability INdex MAPping)계산상 계산되는 지형학적 습윤지수를 통해 발생위치를 추정하였다. 또한, 미국 NRCS에서 제안한 매개변수 투수량계수/지하수함양률(T/R)에 대한 4가지 조건별 해석 결과 현장조사 결과와 다소 차이를 보였으며, 투수량계수/지하수함양률(T/R)의 값이 작을수록 위험도가 높게 나타나는 경향을 보였다.

금융기관 정리절차와 관련된 법률적 고찰과 시사점: 영국 FSMA와 국내 관계법률을 중심으로 (The study of U.K.'s FSMA on the insolvency of financial institutions and implications in South Korea)

  • 장병훈;김신욱
    • 디지털융복합연구
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    • 제11권1호
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    • pp.13-25
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    • 2013
  • FSMA 24 규정을 고찰한 결과, 금융기관의 도산과 관련된 규정은 임의정리, 관리명령, 재산관리인, 임의청산, 법정청산, 파산, 채무부인의 금지 규정, 보험업자에 관한 보칙 등으로 구성되며, 각 절차에 따른 FSA의 권한과 책임이 명시되어 있다. 절차마다 약간의 차이는 있으나 전체적으로 FSA는 채권자와 동일한 지위에서 각 도산절차에 관한 법원 청구권, 각종 집회참석권, 청취권 등을 행사할 수 있다. 영국과 우리나라의 금융기관 도산과 관련된 규정의 차이점 및 시사점을 요약하면, 첫째, 영국은 FSA의 금융기관 도산 절차와 관련된 권한의 행사 주체가 FSA(Financial Services Authority)로 통일되어 있으나, 우리나라의 경우, 각 특별법에 따라 금융기관 정리 방법이 여러 기관으로 분산되어 있어서 관련절차의 행사 주체가 금융위원회, 금융감독원, 예금보험공사 등으로 혼재되어 나타난다. 이는 외환위기 이후 금융개혁의 조속한 시행을 위해 금융기관 정리와 관련된 입법활동을 서둘러 시행하면서 나타난 특징으로 볼 수 있다. 둘째, FSA는 금융기관 도산과 관련된 보험업종의 특성을 고려하여 계약유지에 관한 특별규정이 포함되었으나 우리나라는 규정상 업종별 차이 또는 금융 계약의 특징 등을 고려하지 않고 있어 향후 이에 대한 보완이 필요할 것으로 판단된다.

오제스키병의 생체 조기진단을 위한 면역세포화학, In situ hybridization 및 전자현미경적 연구 (Immunocytochemistry, In situ hybridization and electron microscopy for early diagnosis of Aujeszky's in living pigs)

  • 문운경;김순복;서정향;송근석;노환국
    • 대한수의학회지
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    • 제36권4호
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    • pp.845-858
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    • 1996
  • The purpose of this study was to establish early diagnostic methods for the detection of Aujeszky's disease viral antigens and nucleic acid in nasal cells, and buffy coats from experimentally infected living pigs by a combination of immunocytochemistry, in situ hybridization with digoxigenin(DIG)-labled probe and electron microscopy. Forty days old piglets were inoculated intranasally with $10^{7.0}TCID_{50}$ of Aujeszky's disease virus (ADV, NYJ-1-87 strain). The viral antigens and nucleic acid of ADV were detected in nasal cells, and buffy coat for 20 days after inoculation by immunocytochemistry, in situ hybridization with DIG-labeled probe and electron microscopical method. The results were compared with conventional methods such as a porcine Aujeszky's disease serodiagnostic(PAD) kit, neutralization test(NT) and virus isolation. 1. The viral antigens, nucleic acids and capsids of ADV were detected in nasal cells, buffy coats from 3 days to 20 days after inoculation by immunocytochemistry, in situ hybridization with DIG-labeled probe and electron microscopy, respectively. 2. When viral antigens were detected by the immunocytochemical technique, a diffuse brown deposit was observed in the nucleus and cytoplasm of nasal cells, buffy coats and PK-15 cells under a microscope. 3. DIG-labeled DNA probe was prepared by amplification of conserved sequence of recombinant ADV-gp50 clone with polymerase chain reacction. When ADV-DNA was detected by ISH with DIG-labeled probe, purplish blue pigmentation were observed in the nuclei and cytoplasms of ADV-infected cells under a microscope. Positive signals were observed in nasal cells and in the buffy coat and PK-15 cells at the first day after inoculation. 4. Where ADV-capsids were detected by transmission electron microscopical method, aggregation of capsids was observed in the nuclei and cytoplasms of nasal cells, buffy coats and PK-15 cells. The results suggested that these methods were considered as the highly sensitive and reliable tools for rapid and confirmative diagnosis of Aujeszky's disease in living pigs.

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