• 열처리공학회지
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• 제14권2호
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• pp.81-88
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• 2001

The effects of post-oxidation and sulfnitriding treatments on the phase transformation in the nitrided case of tool steels have been studied. Dense and compact $Fe_3O_4$ layer was formed at the outer surface of nitride compound layer by post-oxidation treatment and multi layer of iron sulfide(FeS) was formed in the compound layer by sulfnitriding treatment. The surface hardness decreased because of formation of the soft oxide or sulfide at the nitride surface. Diffusion layer of nitride case was not affected by post-oxidation treatment or sulfnitriding treatment of nitrided alloy tool steels.

• Progress in Superconductivity
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• 제5권1호
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• pp.9-12
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• 2003

We observed the splitting of the fluxon-flow branches in the current-voltage characteristics of serially stacked intrinsic Josephson junctions (IJJs) formed in $Bi_2$$Sr_2$$CaCu_2$$O_{ 8＋x}$ single crystals in the long-junction limit. Stacks of IJJs were sandwiched between two Au electrodes deposited on the top and the bottom of the stack using the ‘double-side cleaving technique’. In all the samples studied, the branch splitting started occurring for a dense fluxon configuration around 2 T and became more distinct in a higher magnetic field range. This observation can be explained in terms of switching between different Josephson fluxon modes in resonance with the collective plasma oscillations induced by both inductive and capacitive coupling between stacked IJJs. This is the first detailed and quantitative identification of the coherent flux-flow modes in stacked..

• 한국세라믹학회지
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• 제31권7호
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• pp.731-738
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• 1994

TiN films were deposited on high speed steels by plasma assisted chemical vapor deposition (PACVD), cathode arc ion plating (CAIP) and reactive magnetron sputtering (RMS). The properties of the films deposited by the three different methods were compared. The preferred oriented plane of PACVD-TiN is (200) and those of CAIP-TiN and RMS-TiN are (111). PACVD-TiN shows a dome surface and a microstructure having small grains. CAIP-TiN shows the highest microhardness and the best adhesion strength of the three because it has a dense microstructure and an ill-defined interface. But is shows the greatest surface roughness due to the Ti droplet created by the arc. RMS-TiN shows a microstructure having large voids so that its properties in microhardness and adhesion are the worst of the three.

• 한국세라믹학회지
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• 제54권1호
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• pp.38-42
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• 2017

Vanadium nitride (VN) coatings were deposited using inductively coupled plasma (ICP) assisted sputtering at different ICP powers. Microstructural, crystallographic and mechanical characterizations were performed by FE-SEM, AFM, XRD and nanoindentation. The results show that ICP has significant effects on coating's microstructure, structural and mechanical properties of VN coatings. With an increase in ICP power, coating microstructure evolved from a porous columnar structure to a highly dense one. Single- phase cubic (FCC) VN coatings with different preferential orientations and residual stresses were obtained as a function of ICP power. Average crystal grain sizes of single phase cubic (FCC) VN coatings were decreased from 10.1 nm to 4.0 nm with an increase in ICP power. The maximum hardness of 28.2 GPa was obtained for the coatings deposited at ICP power of 200 W. The smoothest surface morphology with Ra roughness of 1.7 nm was obtained in the VN coating sputtered at ICP power of 200 W.

• 한국정보디스플레이학회:학술대회논문집
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• 한국정보디스플레이학회 2006년도 6th International Meeting on Information Display
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• pp.925-928
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• 2006

With the high sustain frequency at 250 kHz, a three-dimensional diagnostics of excited xenon atoms was investigated by the emission and absorption microscopic spectroscopy for plasma display panels, spatiotemporally. As a typical feature of the emissions, a broad discharge peak was observed on the temporal cathode and a sharp one was monitored on the anode, at the high frequency. However, the discharge starts from the cathode edge, actually, that is a discharge space on the floated address (or data) electrode. Spatially, the dense emission and absorption peak were observed in the discharge space between the sustain electrodes gap. Overall, the microdischarge at high sustain frequency showed priming dominant characteristics.

• 한국표면공학회:학술대회논문집
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• 한국표면공학회 2017년도 춘계학술대회 논문집
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• pp.103.2-103.2
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• 2017

Nanocrystalline HfN coatings were prepared by reactively sputtering Hf metal target with N2 gas using a magnetron sputtering system operated in DC and ABPP (asymmetric bipolar pulsed plasma) condition with various duties and frequencies. The effects of duty and frequency, ranging from 75 to 100 % and 5 to 50 kHz, on the coating microstructure, crystallographic and mechanical properties were systematically investigated with FE-SEM, AFM, XRD and nanoindentation. The results show that pulsed plasma has a significant influence on coating microstructure and mechanical properties of HfN coatings. Coating microstructure evolves from the columnar structure to a highly dense one as duty decreases. Average grain size and nano hardness of HfN coatings were also investigated with various pulsed conditions.

• 한국표면공학회:학술대회논문집
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• 한국표면공학회 2017년도 춘계학술대회 논문집
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• pp.103.1-103.1
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• 2017

Nanocrystalline HfN coatings were prepared by reactively sputtering Hf metal target with N2 gas using a magnetron sputtering system operated in DC and ICP (inductively coupled plasma) condition with various powers. The effects of ICP power, ranging from 0 to 200 W, on the coating microstructure, corrosion and mechanical properties were systematically investigated with FE-SEM, AFM, potentiostat and nanoindentation. The results show that ICP power has a significant influence on coating microstructure and mechanical properties of HfN coatings. With the increasing of ICP power, coating microstructure evolves from the columnar structure of DC process to a highly dense one. Average grain size and nano hardness of HfN coatings were also investigated with increasing ICP powers.

• 플랜트 저널
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• 제6권4호
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• pp.63-71
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• 2010

The best way to prevent the corrosion of piston rod is a selection of quality of the material and method of construction which minimize the porosity. The high velocity oxy fuel(HVOF) method, which generates lower porosity than existing plasma spray, was applied to ceramic laminated bond layer. Porosity percentage fell to bellow 2%, lower than that of plasma spray at 7%. Coating material of ceramic-coated main layer was selected as the $Cr_2O_3$ affiliation material, which is more dense than $Al_2O_3$ affiliation. To fill up the pores formed after the coating process, we sealed the bond layer and main layer. Sealing process was performed twice, once after the coating and once after the grinding. Upon the anti-corrosion test on the sealed sample and on the non-sealed sample, it is confirmed that the sealed sample was not corroded for 1,000 hours while the non-sealed sample was corroded within 48 hours.

• Korean Chemical Engineering Research
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• 제54권4호
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• pp.527-532
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• 2016

감압상태(1torr)의 순환유동층 플라즈마 반응기(내경 10 mm, 높이 800 mm)에서 기상 유속과 고체순환속도가 축방향 고체체류량 분포에 미치는 영향을 연구하였다. 폴리스타이렌 고분자 입자와 질소가스를 고체 및 기상 물질로 각각 사용하였다. 감압상태 순환유동층의 고체 순환량 변화는 상승관의 많은 기체 유량(40~80 sccm)에 의한 변화만큼 고체재순환부의 작은 유량 변화(6.6~9.9 sccm)에 의해서도 가능하였다. 감압상태 순환유동층의 고체 순환속도는 재순환부 기체 유속에 따라 증가하였다. 상승관내의 축방향 고체 체류량 분포는 하부의 농후상 영역에서 상부의 희박상 영역까지 높이에 따라 감소하는 형태를 나타내었다. 상승관 내 각 높이에서 고체순환속도의 증가에 따라 직선적으로 고체 체류량이 증가하였다. 이로써 플라즈마 형성과 유지 그리고 플라즈마 반응을 위해 적절한 플라즈마 로드 위치를 결정할 수 있다.

• Nuclear Engineering and Technology
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• 제12권3호
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• pp.163-170
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• 1980

4KJ의 에너지 뱅크(16.5KV, 35nH)를 사용하여 Mather형의 플라즈마총을 1 torr이하의 낮은 기체압력에서 동작시키면서 플라즈마의 효율적인 집속조건을 구하였다. 중수소기체의 충전압력이 0.18torr, 저장에너지가 3.8KJ일때 방전전류의 최고치는 180KA이었고 플라즈마의 축방향 평균속도는 약 $7cm/\mu\textrm{s}$이었다. 이것은 snowplow모델에 의해 계산된 속도보다 작은 값인데 이는 절연재 표면을 통한 전류의 손실에 기인하는 것으로 생각된다. H. Bruzzone의 플라즈마 집속장치(1KJ, 16KV, $4.2\mu\textrm{s}$)에 비해 본 실험에서는 기체압력이 낮은 역역에서 플라즈마 접속이 일어났다. 이는 이 실험에서 사용한 플라즈마총의 크기가 저장에너지에 비해 크고 또 잔여기체의 함량이 비교적 높기 때문이다. 집속된 플라즈마로 부터 방출되는 중성자는 Long counter를 사용해서 계측했다.