• Title/Summary/Keyword: Dehydrate

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Studies on Preparation of Transparent Iron Oxide (투명산화철의 製造에 관한 硏究)

  • Baek, Moo-Hyun;Lim, Jong-Ho;Kim, Tae-Kyung;Lee, Seoung-Won
    • Resources Recycling
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    • v.13 no.6
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    • pp.9-15
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    • 2004
  • The optimum conditions were studied for the preparation of transparent iron oxide with the air oxidation of FeOOH. The FeOOH obtained by mixing NaOH and FeSO$_4$ solution in various conditions such as R(=2NaOH/FeSO$_4$), FeSO$_4$ concentration. reaction temperature and air flow rate. When the FeSO$_4$ increased gradually, the concentration of iron ion in the solution became high. So, particle size increased precipitating Fe$_3O_4$. Goethite dehydrate at about 200$^{\circ}C$ and ended the reaction at about 320$^{\circ}C$ forming hematite. The lower the reaction temperature was, the shorter the particle length of goethite and particle size decreased. When the flow rate of air as an oxidant increased, the amount of dissolved oxygen in the solution increased, which made oxidation rate increased. And then particle size of goethite decreased.

Production of Environment-friendly Artificial Media for Agriculture Using Urban Sludge (도시발생 슬러지를 이용한 환경친화적 인공배지 생산)

  • 김선주;윤춘경;양용석
    • Magazine of the Korean Society of Agricultural Engineers
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    • v.40 no.2
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    • pp.102-111
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    • 1998
  • Large amount of sludge have been generating in the process of water and wastewater treatment in urban area, and it has been making many environmental problems. Currently almost of sludge is landfilled, and since sludge is difficult to handle and dehydrate, the permeated water from the filled-in ground contaminate the surrounding soil and groundwater which may cause serious environmental and sociological problems. The organic component in sludge can be almost removed through the heat treatment process, and the final product is called artificial soil or artificial media according to the temperature control. To produce artificial media using sludge, chabazite and lime were used as an additive, and the mixture of sludge & additives was thermally treated in the firing kiln at about 800~1, 100。C for about fifteen minutes. The physical and chemical characteristics of the produced artificial media were analyzed, and it showed that it can be used as an artificial media for plant production or soil conditioner for farmland. The concentrations of the toxic heavy metals in the artificial media were lower than the soil quality standard for farmland. The characteristics of produced artificial media, using the mixture of sludge and additives through the heat treatment, is similar to the natural chabazite and soil. The analyzed result of the mineral composition of artificial media showed that it has a characteristics similar to natural stable soil, so the produced artificial media may be applied to farmland or water culture without causing adverse effect. Therefore this study showed that the above process can be a feasible alternative for sludge treatment.

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Rapid Weight Loss and Physical and Psychological Difficulties in National Combat Sports Athletes (국가대표 투기종목 선수들의 급속 체중 감량과 신체적, 심리적 고충)

  • Kim, Hyun-Chul;Park, Ki-Jun
    • Journal of the Korean Society of Physical Medicine
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    • v.15 no.3
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    • pp.61-68
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    • 2020
  • PURPOSE: The purpose of this study was to investigate the current state of rapid weight loss and physical and mental complaints among elite combat athletes who were selected and trained as national representatives. METHODS: A total of 127 combat athletes who had trained at the national training center in 2019 were enrolled. The questionnaire used as the survey tool was interpreted as words that Korean athletes could easily understand based on the Portuguese version of the 'Rapid Weight Loss Questionnaire' (RWLQ). χ2 tests was performed to determine the differences in physical and mental changes according to sports and weight loss method. RESULTS: Combat athletes in Korea regularly undergo rapidly weight loss within a short period of time prior to competition. There were statistically similar results in terms of weight loss method, physical and mental changes and information about weight loss according to the sport. Weight loss methods often limit food and water intake and dehydrate. The physical complaints associated with them are symptoms such as "no energy", "dizziness", and "muscle spasms". The mental complaints include "irritability", "concentration loss" and "anxiety". These symptoms can be caused by side effects such as food intake limitation, water restriction and dehydration. Information sources for weight loss were in the order of "senior or colleagues", "supervisor or coach", and "Internet". No information was obtained from a doctor or dietitian. CONCLUSION: These results provide a baseline for predicting proper weight loss in athletes and provide useful information for developing performance enhancement as well as weight loss.

Cryo-SEM Methodology of Arabidopsis thaliana Stem Using High-Pressure Freezing (고압동결고정을 이용한 애기장대 줄기의 cryo-SEM 분석법)

  • Choi, Yun-Joung;Lee, Kyung-Hwan;Je, A-Reum;Chae, Hee-Su;Jang, Ji-Hoon;Lee, Eun-Ji;Kweon, Hee-Seok
    • Applied Microscopy
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    • v.42 no.2
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    • pp.111-114
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    • 2012
  • The scanning electron microscopy is an ideal technique for examining plant surface at high resolution. Most hydrate samples, however, must be fix and dehydrate for observation in the scanning electron microscope. Because the microscopes operate under high vacuum, most specimens, especially biological samples, cannot withstand water removal by the vacuum system without morphological distortion. Cryo-techniques can observe in their original morphology and structure without various artifacts from conventional sample preparation. Rapid cooling is the method of choice for preparing plant samples for scanning electron microscopy in a defined physiological state. As one of cryo-technique, high-pressure freezing allows for fixation of native non-pretreated samples up to $200{\mu}M$ thick and 2 mm wide with minimal or no ice crystal damage for the freezing procedure. In this study, we could design to optimize structural preservation and imaging by comparing cryo-SEM and convention SEM preparation, and observe a fine, well preserved Arabidopsis stem's inner ultrastructure using HPF and cryo-SEM. These results would suggest a useful method of cryo-preparation and cryo-SEM for plant tissues, especially intratubule and vacuole rich structure.

Cryopreservation of winter vegetation buds of Betula platyphylla var. japonica in liquid nitrogen (자작나무 동아의 액체질소 내 초저온 보존)

  • 안영희
    • Korean Journal of Plant Resources
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    • v.15 no.2
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    • pp.89-95
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    • 2002
  • In woody plant germplasms, using prefrozen dormant buds for materials is one way to achieve successful cryopreservation. The protocol of cryopreservation for White birch (Betula platyphylla var. japonica) winter vegetative buds is the following. First, the branches of White birch were collected in January 20, when the vegetative buds were still in a state of quiescence. The winter buds with about 5㎜ of xylem tissue were removed from the branches. They were dehydrated to moisture contents about 44% by air dry treatment. The buds were prefrozen, with the temperature being decreased by 5∼-20$\^{C}$ and then transfered to the LN(liquid nitrogen) maintained below -l96$\^{C}$. After cryopreservation, the vegetative buds were rapidly thawed in a water bath at 40$\pm$5$\^{C}$. In this case, the cell survival rate of samples was about 86%. After sterilization, buds were then cultured on MS medium. These results demonstrate the feasibility for cryopreservation of winter vegetation buds of Betula platyphylla var. japonica.

Dehydration of Soybean Residue by Hot-air in Conjunction with Filter Pressing (압착여과와 열풍에 의한 비지의 건조)

  • Chung, Sung-Soo;Chang, Ho-Nam;Park, Moo-Young
    • Korean Journal of Food Science and Technology
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    • v.10 no.1
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    • pp.1-7
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    • 1978
  • The wet soybean residue, a byproduct of soymilk industry having potential food value has been tried to dehydrate for the purpose of storage. The total solid of the byproduct was composed of 28.9% protein, 13.6% fat, 4.4% ash and 53.0% carbohydrates. The original water content of 593%(dry-weight basis) was reduced to 378% by pressing mechanically. The sufficient pressure and time for the pressing were found to be 0.5M/T and 5minutes, respectively. The partially dehydrated soybean residue was formed into pellets of 3mm in diameter and 10mm in length. By applying hot air on the thin layer of pellets the moisture could be further reduced to the level of 10% which is equivalent to that of the commercial wheat flour. No significant color deterioration in the product was observed if the hot air dehydration procedure was within the limit of 95 minutes at $120^{\circ}C$ under the air flow velocity of 160 feet per minute.

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Drying Characteristics of Agricultural Products under Different Drying Methods: A Review

  • Lee, Seung Hyun;Park, Jeong Gil;Lee, Dong Young;Kandpal, Lalit Mohan;Cho, Byoung-Kwan;Hong, Soon-jung;Jun, Soojin
    • Journal of Biosystems Engineering
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    • v.41 no.4
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    • pp.389-395
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    • 2016
  • Purpose: Drying is one of the most widely used methods for preserving agricultural products or food. The main purpose of drying agricultural products is to reduce their water content for minimizing microbial spoilage and deterioration reaction during storage. Methods: Although numerous drying methods are successfully applied to dehydrate various agricultural products with little drying time, the final quality of dried samples in terms of appearance and shape cannot be guaranteed. Therefore, based on published literature, this review was conducted to study the drying characteristics of various agricultural products when different drying methods were applied. Results: An increase in the drying power of sources-for example, increase in hot air temperature or velocity, infrared or microwave power-and the combination of drying power levels can reduce the drying time of various agricultural products. In addition, energy efficiency in drying significantly relies on the compositions of the dried samples and drying conditions. Conclusions: The drying power source is the key factor to control entire drying process of different samples and final product quality. In addition, an appropriate drying method should be selected depending on the compositions of the agricultural products.

Si 기판위에 형성된 ZnO 나노입자의 열처리 온도변화에 따른 구조적 성질과 전자적 성질에 관한 연구

  • Park, Geun-Gap;No, Yeong-Su;Park, Gyeong-Hun;Son, Dong-Ik;Kim, Tae-Hwan
    • Proceedings of the Korean Vacuum Society Conference
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    • 2010.02a
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    • pp.107-107
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    • 2010
  • ZnO는 상온에서 에너지 밴드갭이 3.37 eV 이고 엑시톤 속박에너지가 60 meV 인 넓은 에너지 띠를 가진 반도체이다. ZnO 반도체는 고에너지 영역에서 광투과율 및 에너지 수집율이 큰 특성을 가지고 있기 때문에 단파장 영역에서 작동하는 발광 다이오드나 반도체레이저 소자 응용에 사용되고 있다. 이와 더불어 액정디스플레이, 유기발광소자 및 태양전지에서 투명 산화물 전극으로 많은 응용이 되고 있다. 본 연구에서는 p-type Si 기판 위에 ZnO 나노입자 형성과 구조적 성질과 전자적 성질에 대하여 조사하였다. ZnO 나노입자를 형성하기 위해 ethanol에 zinc acetate dehydrate (5 wt%)을 적절히 분산시킨 $Zn(CH_3COO)_2H_2O\;+\;CH_3OH$ 용액을 스핀 코팅하여 산소 분위기에서 각각 $300^{\circ}C$, $500^{\circ}C$, $700^{\circ}C$$900^{\circ}C$로 각각 2시간 동안 열처리 하였다. X-ray 회절 실험 결과는 열처리 온도에 관계없이 ZnO (0001)의 피크가 관측되었다. 원자힘 현미경 이미지상으로 열처리 온도에 따른 ZnO 나노입자의 표면상태의 변화와 나노입자의 크기의 변화를 확인하였다. X-ray 광전자 분광 스펙트럼 결과는 Zn $2p_{3/2}$와 O 1s의 전자상태 스펙트럼을 분석하여 ZnO 나노입자가 형성됨을 보여주었다. 본 연구를 통하여 용액방법을 사용하여 제작된 ZnO 나노입자의 열처리 온도변화에 따른 구조적 성질과 전자적 성질을 이해하는데 도움을 줄 것이다.

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Evaluation and application of pretreatment methods for pharmaceuticals and personal care products in the solid phase of sewage samples (하수처리시설 고상시료 중 잔류의약물질 분석을 위한 전처리법 평가 및 적용)

  • Park, Junwon;Kim, Changsoo;Ju, Byoungkyu;Lee, Wonseok;Chung, Hyenmi;Jeong, Dong-Hwan
    • Journal of Korean Society of Water and Wastewater
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    • v.32 no.6
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    • pp.559-572
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    • 2018
  • The aim of this study was to evaluate pretreatment methods for 27 pharmaceuticals and personal care products (PPCPs) in various sewage samples using a modified quick, easy, cheap, effective, rugged, and safe (QuEChERS) and online solid-phase extraction with LC-MS/MS. Extraction efficiencies of PPCPs in the solid phase under different experimental conditions were evaluated, showing that the highest recoveries were obtained with the addition of sodium sulfate and ethylenediaminetetraacetic acid disodium salt dehydrate in acidified conditions. The recoveries of target compounds ranged from 91 to 117.2% for liquid samples and from 61.3 to 137.2% for solid samples, with a good precision. The methods under development were applied to sewage samples collected in two sewage treatment plants (STPs) to determine PPCPs in liquid and solid phases. Out of 27 PPCPs, more than 19 compounds were detected in liquid samples (i.e., influent and effluent) of two STPs, with concentration ranges of LOQ-33,152 ng/L in influents and LOQ-4,523 ng/L in effluents, respectively. In addition, some PPCPs such as acetylsalicylic acid, ibuprofen, and ofloxacin were detected at high concentrations in activated sludge as well as in excess sludge. This methodology was successfully applied to sewage samples for the determination of the target compounds in STPs.

Recent Development Based on 2D Composite Membrane for Pervaporation (투과증발을 위한 2차원 복합막 기반의 최근 개발)

  • Seungwoo Ha;Rajkumar Patel
    • Membrane Journal
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    • v.33 no.4
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    • pp.158-167
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    • 2023
  • The increasing concerns for environmental pollution and depletion of natural resources have prompted the development of environmentally sustainable technologies. Pervaporation has garnered attention in recent decades due to its low energy consumption, environmental impact, and performance efficiency. This method has been used to separate chemical species and dehydrate organic solvents, as the membranes can be fine-tuned to fulfill the desired selectivity. Several separation processes, such as reverse osmosis and distillation, are being utilized in both experimental settings and industrial applications. However, pervaporation has several advantages, such as low operating pressure and temperature and a higher rejection rate. Nonetheless, the current state of membrane technology alone can't suffice the demands of practical applications. Composite membranes, on the other hand, can leverage the benefits of both organic and inorganic materials. Many studies have effectively incorporated inorganic nanomaterials such as graphene oxide (GO) and MXene (MX) in polymeric membranes to tackle the current limitations. This review investigates the recent development of 2D composite membranes in pervaporation and evaluates performance enhancement.