• 제목/요약/키워드: Degree of cure

검색결과 168건 처리시간 0.027초

폴리카보실란 전구체로부터 고온 산화성분위기서 기계적물성이 우수한 파이롯-규모의 탄화규소섬유 제조공정 개발 (Development of Pilot-Scale Manufacturing Process of SiC Fiber from Polycarbosilane Precursor with Excellent Mechanical Property at Highly Oxidation Condition and High Temperature)

  • 윤병일;최우철;김정일;김재성;강홍구;김명주
    • Composites Research
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    • 제30권2호
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    • pp.116-125
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    • 2017
  • 본 연구의 목적은 고온 산화성 분위기하에서 기계적물성이 우수한 탄화규소섬유(SiC Fiber)를 파일롯-규모로의 생산 제조공정을 개발하는 것이다. 프리세라믹 전구체로서 폴리카보실란(PCS)을 사용하여 탄화규소섬유를 제조하였다. 연속성의 PCS 섬유는 $300{\sim}350^{\circ}C$에서 PCS를 용융한 후에 용융방사로부터 얻었다. 열처리 전에 섬유의 불융화를 위하여 공기 분위기하에서 경화를하였다. 경화 전, 후에 측정한 FT-IR 스펙트라 피크로 부터 경화도를 계산하였다. 탄화규소섬유의 물성은 경화도에 따라 크게 영향을 받았다. 본 개발에서 열처리 중 섬유의 장력 조절로 우수한 물성을 갖는 탄화규소섬유를 얻었다. 탄화규소섬유의 화학조성과 기계적물성은 안정화섬유의 열처리시의 이송속도에 영향을 받았다. 탄화규소섬유를 공기분위기하 $1000^{\circ}C$에서 1분부터 50시간까지 노출한 후에 인장시험을 수행하였다. 그 결과 인장강도는 약 60%까지 감소함을 보여주었다. 장시간 노출시험시 낮은 인장 강도값을 나타내는 섬유는 화학성분 분석시 섬유의 표면에 많은 탄소량을 함유하고 있었다.

임상가를 위한 특집 2 - 심미수복용 레진 (Tooth-colored Restorative Resin Composites)

  • 권태엽
    • 대한치과의사협회지
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    • 제51권1호
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    • pp.12-17
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    • 2013
  • Curing methods for denial resin-based materials are limited because of the need to polymerize quickly in the oral cavity at an ambient temperature. At present, most dental restorative composites use a camphorquinone-amine complex initiation, visible light-cure, one-component systems. Clinically, it is important to try to optimize the degree of conversion of res in composites using proper manipulation and adequate light-curing techniques to ensure the best outcome.

UV 나노임프린트를 위한 UV 경화성 수지의 경화 모델 개발

  • 이진우;조동우;이응숙
    • 한국정밀공학회:학술대회논문집
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    • 한국정밀공학회 2004년도 춘계학술대회 논문요약집
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    • pp.13-13
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    • 2004
  • 나노테크놀러지 중의 한 가지인 나노임프린트 리소그래피 기술은 수 ∼ 수십 나노 급의 선폭을 가지는 스탬프(stamp)를 전자빔 리소그래피(electron beam lithography)를 이용하여 제작한 후 스탬프에 형성된 패턴과 동일한 형상을 원하는 곳에 모사하는 기술이다. 이 기술은 크게 열을 가하는 방식과 UV 경화성 수지를 이용한 방식으로 나뉜다. 열을 가하는 나노임프린트 리소그래피 방식의 경우는 열 경화성 수지를 이용하여 고온 조건에서 스탬프를 고압으로 눌러 원래의 형상을 모사하며, UV 나노임프린트는 광경화 반응을 이용하여 수지를 경화 시켜 모사하는 차이점이 있다.(중략)

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반응성노화방지제(反應性老化防止劑)의 가황특성(加黃特性)에 관(關)한 연구(硏究) (Studies on the Vulcanization Characteristics of Rubber-Bound Antioxidants)

  • 백남철
    • Elastomers and Composites
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    • 제14권2호
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    • pp.83-102
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    • 1979
  • The purpose of this dissertation is to study some of the vulcanization characteristics of rubber-bound antioxidants such as G-1, [N-(3-methacryloyloxy-2-hydroxypropyl)-N'-phenyl-p-phenylene diamine] and acryl, acrylamide & acrylester substituted hindered phenols. The influence of these antioxidants upon vulcanization characteristics in NR and SBR compounds in the presence of vulcanizing accelerators such as MSA, TT, DM, M & D was evaluated by means of Oscillationg Disk Cure Meter. The comparison was also made between the influence of rubber-bound antioxidants and that of conventional non-reactive antioxidants such as N-alkyl substituted PADA series. Regarding the influence of reactive type antioxidant G-1 mixed with accelerator TT upon vulcanization characteristics, rapid onset of vulcanization and higher degree of cross-linking were discovered, whereas in the case of accelerator M and DM, the result was slow onset of vulcanization and lesser degree of cross-linking. The comparison of vulcanizing characteristics among acrylic substituted hindered phenols as antioxidants was made under several vulcanization accelerator systems. Under such systems, MSA-S combined accelerator caused the onset of vulcanization to slow down and lowered the degree of cross-linking. Finally in the case of hindered phenol derivatives containing longer substituent, the delayed onset of vulcanization and the lowered degree of cross-linking could be discerned.

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대구지역 일부 초등학교 교사의 구강보건인식도에 대한 견해 (Views about the degree of recognition of dental hygiene of elementary school teachers - The object of study: elementary school teachers in city of Daegu -)

  • 정은경;이가령
    • 한국치위생학회지
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    • 제6권2호
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    • pp.165-174
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    • 2006
  • In order to establish basic data before deciding on the ways to manage school dental hygiene project, this study polled 165 elementary school teachers. Collected data was used SPSS 12.0 statistics program and got the technical statistics and This research and analysis came to the following conclusion by using Fridmen rank test, Pearson's correlation. 1. To the question about how they acquire the knowledge of dental hygiene, 60.6 percent of elementary school teachers turned out to learn about it through mass media(TV, Internet, magazines). 2. Regarding the purpose to maintain dental hygiene, "the prevention of dental diseases" ranked highest, and next "the prevention of cavity" and "the cure of halitosis" appeared at the similar level, and "to become a good model of children" and "to serve the esthetic purpose" ranked lowest. 3. As to the ways to prevent cavity, regular visits to dental clinic and daily brushing turned out to be more effective preventation method. 4. As for the degree of recognition of fluoride, the correct answer about fluoride that is recovered slight caries is appeared 11.8%, that was lowest correct answer ratio.

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Preblending Effect of Biblends on Properties of the Carbon Black-Filled Rubber Compounds

  • Park, Sung-Seen
    • Macromolecular Research
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    • 제9권1호
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    • pp.37-44
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    • 2001
  • A premixing effect for the properties of carbon black-filled rubber compounds was investigated using biblends of natural rubber (NR), styrene-butadiene rubber (SBR), and butadiene rubber (BR). Degree of mixing of the biblends was controlled by preblending time of 0.0, 2.5, and 5.0 min. Mooney viscosities of the compounds decreased by increasing the preblending time. Of three carbon black-filled compounds of NR/SBR, NR/BR, and SBR/BR compounds, only the SBR/BR blends showed a specific cure characteristics depending on the preblending time. For the bound rubber composition, the NR content was higher than SBR and BR. The difference in the rubber composition ratio of the bound rubber became smaller with increasing the preblending time. Physical properties of the vulcanizates such as hardness, modulus, tensile property, abrasion loss, and tans were also compared. Differences in properties of the compounds were discussed with miscibility of the dissimilar rubbers and degree of mixing.

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Functional Finishing of Cotton Fabrics by Treatment with Chitosan

  • Shin, Youn-Sook;Min, Kyung-Hye;Jang, Jeong-In
    • 한국가정과학회:학술대회논문집
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    • 한국가정과학회 1997년도 가정과학회 총회 및 학술대회
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    • pp.33-37
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    • 1997
  • Cotton fabric was treated with chitosan solution by pad-dry(-cure) method to impart antimicrobial properties. Four chitosans of different degree of deacetylation(DAC: 65~95%) with similar molecular weight(ca. 50, 000) and one chitosan oligomer(MW 1, 800, DAC 86%) were used. Antimicribial activity against Staphylococcus aureus was evaluated by the Shake Flask Method. Treated fabrics were laundered up to 20 times according to AATCC Test Method 60-1986 and antimicrobial activity of laundered fabrics was evaluated. The antimicrobial activity was increased with the concentration and DAC of chitosan used. And the cured samples showed better durability to laundering than not-cured samples. Crosslinker and binder decreased the antimicrobial activity of fabrics treated with chitosan oligomer and were not effective to improve the durability to washing.

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8체질의학에 대한 환자 인식 조사 (Recognition Surrey of Patients about Eight Constitution Medicine)

  • 박재성;박영재;민재영;신용섭;이상철;박영배;김민용
    • 대한한의진단학회지
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    • 제11권1호
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    • pp.130-145
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    • 2007
  • Background and purpose: The purpose of this study is to search recognition patients in Eight constitution Oriental Medical Clinic. And we compare Eight constitution acupuncture methods with the another acupuncture methods. Methods: The subjects were comprised of 200 volunteers. In 3 Eight constitution Oriental Medical Clinic participants were chosen through questionnaire. Finishing answer participants put in their lacked name questionnaire to gathering box. DecisionTree (AnswerTree 3.0 Ver.) statistical software was used for statistical analysis. Results and Conclusion: As a result of the analysis of cognition to Eight constitution acupuncture methods was influenced to patients health, dietetic therapy is best influenced. Next influenced acupuncture reflex degree, age, job, constitution, cure periods, sex distinction, cure degree, diagnosed participant's Constitution by pulse diagnosis in 8 Constitution Medicine.

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Highly Reliable Solder ACFs FOB (Flex-on-Board) Interconnection Using Ultrasonic Bonding

  • Kim, Yoo-Sun;Zhang, Shuye;Paik, Kyung-Wook
    • 마이크로전자및패키징학회지
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    • 제22권1호
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    • pp.35-41
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    • 2015
  • In this study, in order to improve the reliability of ACF interconnections, solder ACF joints were investigated interms of solder joint morphology and solder wetting areas, and evaluated the electrical properties of Flex-on-Board (FOB) interconncections. Solder ACF joints with the ultrasonic bonding method showed excellent solder wetting by broken solder oxide layers on solder surfaces compared with solder joints with remaining solder oxide layer bonded by the conventional thermo-compression (TC) bonding method. When higher target temperature was used, Sn58Bi solder joints showed concave shape due to lower degree of cure of resin at solder MP by higher heating rate. ACFs with epoxy resins and SAC305 solders showed lower degree of resin cure at solder MP due to the slow curing rate resulting in concave shaped solder joints. In terms of solder wetting area, solder ACFs with $25-32{\mu}m$ diameters and 30-40 wt% showed highest wetted solder areas. Solder ACF joints with the concave shape and the highest wetting area showed lower contact resistances and higher reliability in PCT results than conventional ACF joints. These results indicate that solder morphologies and wetting areas of solder ACF joints can be controlled by adjustment of bonding conditions and material properties of solder and polymer resin to improve reliability of ACF joints.

자율신경계를 통한 한약약성의 해석 (Interpretation on the Four-Properties of the Traditional Korean Drugs by the Effects on the Autonomic Nervous System)

  • 김호철;박찬웅
    • 대한한의학회지
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    • 제18권2호
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    • pp.148-154
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    • 1997
  • In the pharmacology of traditional Korean medicine, each drug has its own specific characters. The different characters of drugs are employed to treat diseases, rectify the hyperactivity or hypoactivity of yin or yang, and help the body restore its normal physiological functions, consequently curing the diseases and restoring health. The various characters and functions of these drugs concerning medical treatment include drugs' properties, flavours, actions of lifting, lowering, floating and sinking, channel tropism, toxicity, etc. Among these theories, theory of properties and flavours of drugs provides the basis for drug analysis and application. 'Property' refers to the cold, hot, warm or cool nature of a drug. These properties of drugs are so sorted out according to the different actions of the drugs on the human body and thier therapeutic effects. Drugs which cure heat syndrome(yang syndrome) have a cold or cool property, whereas drugs which cure cold syndrome (yin syndrome) have hot or warm property Drugs of cold and cool-natured and drugs of warm and hot natures are of opposite properties. A cold-natured drug is different from a cool-natured on only in degree, and so is a warm-natured drug from a hot-natured drug. Most of the cool- or cold- natured drugs have the effects of clearing heat, purging fire, removing toxic substances, and nourishing yin, and are uese to cure heat syndromes. On the contrary, drugs of warm or hot nature usually have the effects of dispersing cold, warming up the interior, supporting yang, and treating collapse, and are therefore used to treat cold syndromes. We thought that the property of drug may be related to the autonomic nervous system in western medicine. In other words, drugs of warm or hot nature increase heart rate or acts like sympathomimetics, and drugs of cool or cold nature decrease heart rate or acts like para sympathomimetics . According to this hypothesis, we administrated some drugs to isolated rat right atrium in magnus tube. But there is no correlation between 'property' in traditional Korean medicine and autonomic nervous system in western medicine.

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