• Title/Summary/Keyword: DMA (differential mobility analyzer)

Search Result 22, Processing Time 0.038 seconds

Particle path and performance evaluation of differential mobility analyzer (Differential Mobility Analyzer(DMA)내의 입자운동 및 특성 분석)

  • An, Gang-Ho;Kim, Nam-Hyo;Lee, Jong-Ho;Bae, Gwi-Nam
    • Transactions of the Korean Society of Mechanical Engineers B
    • /
    • v.20 no.6
    • /
    • pp.2005-2013
    • /
    • 1996
  • Particle paths and flow fields in a prototype differential mobility analyzer (DMA) were numerically analyzed solving Navier-Stokes equation, electric field equation and particle motion considering viscous drag force, Coulomb force and polarization force. Analytically predicted particle diameters for the prototype DMA are in good agreement with the measured particle diameters within $\pm$1%. And the analytically predicted particle diameters are also in good agreement with numerical results for the prototype DMA.

Calibration and Uncertainty Measurement of Differential Mobility Analyzer Using 100 nm NIST SRM 1963 (100 nm NIST 표준입자를 이용한 미분형 전기 이동도 분석기의 교정 및 불확실도 측정)

  • Lee, Snag-Jin;Ahn, Jin-Hong;Ahn, Kang-Ho
    • Transactions of the Korean Society of Mechanical Engineers B
    • /
    • v.27 no.12
    • /
    • pp.1766-1771
    • /
    • 2003
  • House made differential mobility analyzer(DMA) is calibrated with NIST SRM 1691(300 nm PSL). Then the particle size and uncertainty for differential mobility analyzer(DMA) using the NIST SRM 1963(100 nm PSL). In result, calibration of prototype DMA is measured using 300 nm NIST SRM 1691, then sheath air flow was corrected 126.67 ㎤/s. Corrected sheath air flow is used in uncertainty measurement of prototype DMA. Uncertainty analysis is performed using NIST SRM 1963(100 nm PSL). The experimental result shows that NIST SRM 1963 is measured as 102.17 nm with a type A uncertainty of 0.33 nm.

Understanding Size Selection of Nanoparticles Using a Differential Mobility Analyzer (DMA) and Its Performance Enhancement (DMA를 이용한 나노 입자의 크기 분류법에 대한 이해와 성능개선)

  • Kim, Seok-Hwan;Kim, Sang-Wook;Lee, Donggeun
    • Particle and aerosol research
    • /
    • v.10 no.1
    • /
    • pp.33-43
    • /
    • 2014
  • A differential mobility analyzer (DMA) has been widely used as a standard tool for classifying nanoparticles with a certain size. More recently, several new types of DMA have been tested in an attempt to produce size-monodisperse nanoparticles. It is a bit surprise to see how simple the working theory of the DMA is. Although the theory was demonstrated quite successful, no one can guarantee whether the theory still works in another geometry of the DMA. In this regard, we first investigated the validity of the theory under various working conditions and then moved to check the validity upon minor change in its design. For the valid test, we compared the results with those obtained from a computational fluid dynamics.

Study on the Contribution of Mixing Effects in Sampling Tube and Condensation Nuclei Counter(CNC) to the measurement of size distribution obtained using Differential Mobility Analyzer and CNC (Differential Mobility Analyzer(DMA)와 Condensation Nuclei Counter(CNC)를 이용한 입자크기 분포 측정에서 샘플링 튜브와 CNC에서의 혼합 효과가 입자 크기 분포 측정에 미치는 영향에 관한 연구)

  • Lee, Youn-Soo;Ahn, Kang-Ho
    • Proceedings of the KSME Conference
    • /
    • 2001.06d
    • /
    • pp.104-109
    • /
    • 2001
  • The time to measure the size distribution using Condensation Nuclei Counter(CNC) and Differential Mobility Analyzer(DMA) can be shortened by classifying particles ramping the DMA voltage exponentially and continuously. In measurement, particles sampled at different time are mixed together going through sampling tube and CNC. Because the size distribution is inversed by using detector responses to sampling time intervals in this accelerated method, the mixing effects give inversion errors to the size distribution. The mixing effects can be considered by appling the transfer function with mixing effects to the data inversion. The inversion considering this effects gives birth to the size distribution shifted to the opposite direction of the size scanning.

  • PDF

Recent Development of Differential Mobility Analyzers For Size-Classification of Nanoparticles and Their Applications to Nanotechnologies

  • Seol, Kwang-Soo;Yoshimichi Ohki;Kazuo Takeuchi
    • KIEE International Transactions on Electrophysics and Applications
    • /
    • v.4C no.2
    • /
    • pp.39-44
    • /
    • 2004
  • The present paper gives a review of the recent development of a differential mobility analyzer (DMA) available for both particle size measurements and production of monodisperse particles in the nanometer range. Operating principles of a general DMA are introduced as well as characteristics of highly functional DMAs such as those capable of classifying particles in a measurement range as broad as 1-1000nm at low pressures. Some examples of DMA applications are also described.

Morphological control and electrostatic deposition of silver nanoparticles produced by condensation-evaporation method (증발-응축법에 의해 발생된 은(silver) 나노입자의 구조제어 및 전기적 부착 특성 연구)

  • Kim, Whidong;Ahn, Ji Young;Kim, Soo Hyung
    • Particle and aerosol research
    • /
    • v.5 no.2
    • /
    • pp.83-90
    • /
    • 2009
  • This paper describes a condensation-evaporation method (CEM) to produce size-controlled spherical silver nanoparticles by perturbing coagulation and coalescence processes in the gas phase. Polydisperse silver nanoparticles generated by the CEM were first introduced into a differential mobility analyzer (DMA) to select a group of silver nanoparticles with same electrical mobility, which also enables to make a group of nanoparticles with elongated structures and same projected area. These silver nanoparticles selected by the DMA were then in-situ sintered at ${\sim}600^{\circ}C$, and then they were observed to turn into spherical shaped nanoparticles by the rapid coalescence process. With the assistance of modified converging-typed quartz reactor, we can also produce the 10 times higher number concentration of silver nanoparticles compared with a general quartz reactor with uniform diameter. Finally, the spherical silver nanoparticles with 30 nm were electrostatically deposited on the surface of silicon substrate with the coverage rate of ~4%/hr. This useful preparation method of size-controlled monodisperse silver nanoparticles developed in this work can be applied to the various studies for characterizing the physical, chemical, optical, and biological properties of nanoparticles as a function of their size.

  • PDF

Study on the real-time measurement equipment for nanoparticle in low-pressure processes (저압공정 중 발생하는 나노입자 실시간 측정장비에 관한 연구)

  • Na, Jeong-Gil;Cho, Dae-Geun;Choi, Jae-Boong;Kim, Young-Gin;Kim, Tae-Sung
    • Journal of the Korean Vacuum Society
    • /
    • v.16 no.6
    • /
    • pp.468-473
    • /
    • 2007
  • In this paper, we discussed about the development of the PBMS(Particle Beam Mass Spectrometer) that can measure the nanoparticles on real-time in low-pressure processes. To calibrate this equipment, a DMA(Differential Mobility Analyzer) was used to generate NaCl particles which are charged to +1. Total aerosols flow rate was 1 lpm and 0.086 lpm of that was introduced into the PBMS through the pressure-reducing critical orifice. Transport efficiency through PBMS was 50$\sim$60 % compared to particle current for DMA and PBMS according to the particle size. Results of mesurements are in good agreement with size distributions obtained by DMA.

An Experimental Study on Composition Characteristics of $SiO_2/TiO_2$ Multicomponent Particle in Coflow Diffusion Flame (화염중 발생하는 $SiO_2/TiO_2$ 다성분입자의 조성특성에 관한 실험적 연구)

  • Kim, Tae-Oh;Suh, Jeong-Soo;Choi, Man-Soo
    • Proceedings of the KSME Conference
    • /
    • 2000.04b
    • /
    • pp.441-446
    • /
    • 2000
  • Chemical compositions of monodisperse $SiO_2/TiO_2$ multicomponent aggregates were measured for different heights from the burner surface and different mobility diameters of aggregates. $SiO_2/TiO_2$ multicomponent particles were generated in a hydrogen/oxygen coflow diffusion flame from two sets of precursors: TTIP (titanium tetraisopropoxide), TEOS(tetraethylorthosilicate). To maintain 1:1 mole ratio of TTIP:TEOS vapor theoretically, flow rate of carrier gas $N_2$ was fixed at 0.61pm for TTIP, at 0.11pm for TEOS. In situ sampling probe was used to supply particles into differential mobility analyzer(DMA) which was calibrated with using commercial DMA(TSI 3071A) and classifying monodisperse multicomponent particles. Classified particles were collected with electrophoretic collector. The distributions of composition from particle to particle were determined using EDS (energy dispersive spectrometry) coupled with TEM (transmission electron microscope). The chemical (atomic) compositions of classified monodisperse particle were obtained for different heights; z=40mm, 60mm, 80mm. The results suggested that the atomic composition of $SiO_2$ decreased with the height from burner surface and the composition of $SiO_2$ and $TiO_2$ approached to the value of 1 to 1 in far downstream. It is also found that the composition of $SiO_2$ decreases as the mobility diameter of aggregate increases.

  • PDF

Investigation of the Optical and Cloud Forming Properties of Pollution, Biomass Burning, and Mineral Dust Aerosol

  • Lee Yong-Seop
    • Proceedings of the Korea Air Pollution Research Association Conference
    • /
    • 2006.04a
    • /
    • pp.55-56
    • /
    • 2006
  • This thesis describes the use of measured aerosol size distributions and size-resolved hygroscopic growth to examine the physical and chemical properties of several particle classes. The primary objective of this work was to investigate the optical and cloud forming properties of a range of ambient aerosol types measured in a number of different locations. The tool used for most of these analyses is a differential mobility analyzer / tandem differential mobility analyzer (DMA / TDMA) system developed in our research group. To collect the data described in two of the chapters of this thesis, an aircraft-based version of the DMA / TDMA was deployed to Japan and California. The data described in two other chapters were conveniently collected during a period when the aerosol of interest came to us. The unique aspect of this analysis is the use of these data to isolate the size distributions of distinct aerosol types in order to quantify their optical and cloud forming properties. I used collected data during the Asian Aerosol Characterization Experiment (ACE-Asia) to examine the composition and homogeneity of a complex aerosol generated in the deserts and urban regions of China and other Asian countries. An aircraft-based tandem differential mobility analyzer was used for the first time during this campaign to examine the size-resolved hygroscopic properties of particles having diameters between 40 and 586 nm. Asian Dust Above Monterey (ADAM-2003) study was designed both to evaluate the degree to which models can predict the long-range transport of Asian dust, and to examine the physical and optical properties of that aged dust upon reaching the California coast. Aerosol size distributions and hygroscopic growth are measured in College Station, TX to investigate the cloud nucleating and optical properties of a biomass burning aerosol generated from fires on the Yucatan Peninsula. Measured aerosol size distributions and size-resolved hygroscopicity and volatility were used to infer critical supersaturation distributions of the distinct particle types that were observed during this period. The predicted CCN concentrations were used in a cloud model to determine the impact of the different aerosol types on the expected cloud droplet concentration. RH-dependent aerosol extinction coefficients are calculated at a wavelength of 550 nm.

  • PDF