• Applied Chemistry for Engineering
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• v.29 no.3
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• pp.356-361
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• 2018

It is common to analyze volatile organic compound (VOC) or semi-VOC (SVOC) in a sample composed of a complex matrix consisting of multiple components such as bloods through a separation process. Adsorption is a physical phenomenon in which certain components accumulate on the surface of other phases. In order to overcome difficulties in the pretreatment process, an adsorption is frequently used. Solid phase microextraction (SPME) equipment with porous carbon carboxen (CAR) is an example of adsorption application. In this study, the adsorption of 4-octylphenol to carboxen was examined. To do so, the extraction efficiency for such solvents as dichloromethane ($CH_2Cl_2$, DCM), ethylacetate ($CH_3COOC_2H_5$, EA) and diethylether ($C_2H_5OC_2H_5$, $Et_2O$) was studied and also the derivatization reaction for 4-octylphenol with reagents of bistrimethylsilyltrifluoroacetamide (BSTFA), methylchloroformate (MCF) and pentafluorobenzylbromide (PFBBr) was compared. The combination of DCM and BSTFA showed good performance thus they were adopted for this study. Thermodynamic adsorption experiments showed that the adsorption process was endothermic and Freundlich isotherm equation was more suitable than Langmuir isotherm. It was also found that the adsorption followed a pseudo-$2^{nd}$ order kinetic model.

• Analytical Science and Technology
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• v.15 no.5
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• pp.466-474
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• 2002

The analytical method of 14 kinds of coplanar - PCBs was established and applied the soil sample. The three kinds of extraction solvents (toluene, acetone: n-hexane, dichloromethane) were selected to apply the soil sample. The silica gel, florisil and alumina column cleanup also performed to compare the elution recovery. The average recovery of selected solvents in soil A, B and C was surveyed the 84.25%, 56.09% and 44.69% for toluene, 52.56%, 81.42% and 58.53% for acetone : n - hexane and 55.94%, 71.33% and 61.05% for dichloromethane. The average recovery is represented 49.99% for silica gel (n - hexane 100 mL), 69.65% for florisil (6% ether/n - hexane 100 mL), and 65.23% for alumina (2% DCM : n - hexane 100 mL, 50% DCM: n-hexane 150 mL). In silica gel (n - hexane) and florisil (6% ether : n - hexane) cleanup, the 14 kinds of coplanar PCBs eluted until 40 mL. In the silica gel and florisil columns cleanup, the amounts of elution solvent can be reduced from these results, but the researcher has to confirm the elution amounts before performing the experiments. In alumina cleanup process, the result was obtained to the 100 mL of elution solvents (2% DCM: n-hexane 100 mL and 50% DCM: n-hexane 40 mL), therefore the change of elution solvent is necessary to develop the simple procedure.

• Journal of the Korean Institute of Illuminating and Electrical Installation Engineers
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• v.20 no.2
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• pp.16-23
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• 2006

This paper presents a novel single-stage high frequency resonant inverter link type DC-DC converter using zero voltage switching with high power-factor. The proposed topology is integrated half-bridge boost rectifier as power factor corrector(PFC) and half-bridge high frequency resonant converter into a single-stage. The input stage of the half-bridge boost rectifier works in discontinuous conduction mode(DCM) with constant duty cycle and variable switching frequency. So that a boost converter makes the line current follow naturally the sinusoidal line voltage waveform. Simulation results have demonstrated the feasibility of the proposed high frequency resonant converter. Characteristics values based on characteristics analysis through circuit analysis is given as basis data in design procedure. Also, experimental results are presented to verify theoretical discussion. This proposed inverter will be able to be practically used as a power supply in various fields as induction heating applications, fluorescent lamp and DC-DC converter etc.

• KSCE Journal of Civil and Environmental Engineering Research
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• v.26 no.4A
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• pp.659-675
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• 2006

Recently, significant progress has been made in performance-based engineering methods that rely mainly on nonlinear static seismic analysis procedures. The Capacity Spectrum Method (CSM) and the Displacement Coefficient Method (DCM) are the representative nonlinear static seismic analysis procedures. In order to evaluate the applicability of the procedures to the seismic evaluation and design process of new and existing structures, the accuracy of both CSM and DCM should be evaluated in advance. The accuracy of seismic responses by the nonlinear static procedures is evaluated in comparison with the shaking table test results for the structural wall specimen subjected to the far field and near field earthquakes. Also conducted are comparative studies where the shaking table test results are compared with those from nonlinear dynamic analysis procedures, i.e., Single-Degree-of-Freedom (SDOF), equivalent SDOF and Multi-Degree-of-Freedom (MDOF) systems.

• Journal of Power Electronics
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• v.14 no.5
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• pp.908-917
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• 2014

For the purpose of designing an intrinsic safety Flyback converter with minimal output voltage ripple based on a specified output current, this paper first classified the energy transmission modes of the system into three sorts, namely, the Complete Inductor Supply Mode-CCM (CISM-CCM), the Incomplete Inductor Supply Mode-CCM (IISM-CCM) and the Incomplete Inductor Supply Mode-DCM (IISM-DCM). Then, the critical secondary self-inductance assorting the three modes are deduced and expressions of the output voltage ripples (OVR) are presented. For a Flyback converter with constant loads and switching frequency, it is shown that the output voltage ripple in the CISM-CCM is the smallest and that it has no relationship with the secondary self-inductance. Otherwise, the OVR of the other two modes are bigger than the previously mentioned one. It is concluded that the critical inductance between the CISM-CCM and the IISM-CCM is the minimal secondary self-inductance to ensure the smallest output voltage ripple. At last, a design method to guarantee the minimum OVR within the scales of the input voltage and load are analyzed, and the minimum secondary self-inductance is proposed to minimize the OVR. Simulations and experiments are given to verify the results.

• KSCE Journal of Civil and Environmental Engineering Research
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• v.32 no.4C
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• pp.159-167
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• 2012

In this study, laboratory model pile-load test and finite element analysis were carried out to compare and analyze the strain behaviour around the model pile tip. In order to simulate the pile load, both the LCM(load control method)and DCM(displacement control method) were introduced to determine which one is appropriate for the FE simulation. In contrast to the previous simulation method, two interface elements around the model pile were used to consider the slip effect in the finite element analysis and its results were compared to the model test. Through this study it was found that the degree of non-associated flow was a dominant factor in terms of numerical solution convergence. In addition, an improved FE mesh was required to obtain the symmetric distribution of the maximum shear strain contour.

• Proceedings of the KIEE Conference
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• 2009.07a
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• pp.1035_1036
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• 2009

본 논문에서는 연료전지에 적용될 수 있는 다상부스트의 동작과 전류 불연속 모드에서 입력전류의 발생 추이를 수식적으로 제시하였다. 제시한 방법은 입력전류의 구간을 나눈 뒤 구간마다 입력 전류의 상태 방정식을 각각 유도 하였으며 이를 바탕으로 리플크기를 나타내었다.

• Journal of the Korean Geotechnical Society
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• v.34 no.12
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• pp.71-82
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• 2018

This study presents a reasonable and economical DCM reinforcement length for the various factors (the embankment height, the distance from the embankment to the underground structure, the depth of the soft ground, and the compression index and the swelling index of the soft ground) that affect the stability of the structure due to lateral movement. Based on these results, we analyzed each factor's degree of influence and figured out which factor influenced the lateral movement most. The cross section of the embankment on the soft ground was modeled by using the Finite Element Program and reinforced with DCM. The results show that the increase rate of the reinforcement length with the increase of the embankment height is about 9~50%, the increase rate of the reinforcement length with the depth of soft ground is about 13~30%, and the increase rate of the reinforcement length with increasing compression index is about 3~25%. In addition, the influence of each factor on each other was analyzed. As a result, among the separation distance, the compressive index and the maximum to minimum slope ratio of the reinforcement length of the embankment height, the separation distance was the largest for the depth of soft ground. As the depth of the soft ground increases, the ratio of the maximum to minimum slope of the reinforcement length according to the embankment height is 3.75, the ratio of the maximum to minimum slope of the reinforcement length according to the spacing distance is 4.3, and the ratio of maximum to minimum slope according to compression index is 2.5. From these results, it is confirmed that the three factors are greatly affected by the depth of soft ground.

• The Transactions of the Korean Institute of Power Electronics
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• v.24 no.3
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• pp.207-214
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• 2019

In this study, discrete-time domain analysis is proposed to investigate the input current of a buck AC/DC light-emitting diode (LED) driver. The buck power factor correction converter can operate in both discontinuous conduction mode (DCM) and continuous conduction mode (CCM). Two discontinuous and two continuous conduction operating modes are possible depending on which event terminates the conduction of the main switch in a switching cycle. All four operating modes are considered in the discrete-time domain analysis. The peak current-mode control with slope compensation is used to design a low-cost AC/DC LED driver. A slope compensation design of the buck AC/DC LED driver is described on the basis of a discrete-time domain analysis. Experimental results are presented to confirm the usefulness of the proposed analysis.

• Proceedings of the Korea Concrete Institute Conference
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• 2000.10a
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• pp.63-68
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• 2000

Concrete is popular as a building material, however it is inherently brittle and performs poorly during earthquakes if nor reinforced properly. Traditional retrofit design techniques assume that buildings respond elastically to earthquakes. This assumption simplifies the analysis procedure but can lead to an erroneous conclusion. The complete nonlinear time history analysis is considered overly complex and impractical for general use. Simplified nonlinear analysis methods, referred to as nonlinear static analysis procedures, include the capacity spectrum method(CSM) developed in detail at ATC-40 and the displacement coefficient method(DCM) utilized at FEMA-273. In this study wall APT system. The results were compared and analyzed. The program used was neaMAX-3D to express nonlinear material.