• Applied Microscopy
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• 제27권3호
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• pp.235-241
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• 1997

(001) GaAs 기판 위에 성장된 (ZnSe/FeSe) 초격자의 구성층 사이에 상호확산으로 형성된 $Zn_{1-x}Fe_xSe$ 의 미세구조가 고분해능 투과전자현미경과 컴퓨터 이미지 시뮬레이션에 의해 연구되었다. 컴퓨터 이미지 시뮬레이션은 multislice 방법으로 여러 시편 두께와 초점 거리에서 실시되었다. 컴퓨터 시뮬레이션에 의해 얻은 이미지는 실험에 의해 얻은 이미지와 비교되었다. 또한, CuAu-I 형태 규칙화가 $Zn_{1-x}Fe_xSe$ 상호화산층에서 일어났다. 이 CuAu-I 형태 규칙격자는 <100>과 <110> 방향에 따라서 ZnSe와 FeSe 층이 교대로 구성되어 있다.

• 대한치과기공학회지
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• 제34권4호
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• pp.345-352
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• 2012

Purpose: The age-hardening mechanism of an Au-Ag-Cu-Pt-Zn alloy for crown and bridge fabrication was investigated by means of hardness test, X-ray diffraction study and field emission scanning electron microscopic observation. Methods: Before hardness testing, the specimens were solution treated and then were rapidly quenched into ice brine, and were subsequently aged isothermally at $400-450^{\circ}C$ for various periods of time in a molten salt bath and then quenched into ice brain. Hardness measurements were made using a Vickers microhardness tester. The specimens were examined at 15 kV using a field emission scanning electron microscope. Results: By the isothermal aging of the solution-treated specimen at $450^{\circ}C$, the hardness increased rapidly in the early stage of aging process and reached a maximum hardness value. After that, the hardness decreased slowly with prolonged aging. However, the relatively high hardness value was obtained even with 20,000 min aging. By aging the solution-treated specimen, the f.c.c. Au-Ag-rich ${\alpha}_0$ phase was transformed into the Au-Ag-rich ${\alpha}_1$ phase and the AuCu I ordered phase. Conclusion: The hardness increase in the early stage of aging process was attributed to the formation of lattice strains by the precipitation of the Cu-rich phase and then subsequent ordering into the AuCu I-type phase. The decrease in hardness in the later stage of aging process was due to the release of coherency strains by the coarsening of tweed structure in the grain interior and by the growth and coarsening of the lamellar structure in the grain boundary. The increase of inter-lamellar space contributed slightly to the softening compared to the growth of lamellar structure toward the grain interior.