• 한국정밀공학회지
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• 제28권10호
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• pp.1210-1216
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• 2011

The purpose of this study is to establish the analysis method for prediction of temperature during cryogenic heat treatment. Experimental cryogenic heat treatment is conducted to observe the phenomena such as boiling of fluid, ice layer on the material surface and to measure the temperature distribution of Al6061 tube. The CFD analysis considering the observed phenomena in the experiment is performed to predict the temperature distribution and convection heat transfer coefficient at each stage of cryogenic heat treatment, in which the boiling of fluid is considered as the multi-phase condition of vapour and liquid. The formation of ice layer on the tube surface is also modeled between material and fluid. The predicted results are in good agreement with the experimental ones. From the results, it is shown that the analysis method can predict the temperature distribution and convection heat transfer coefficient during cryogenic heat treatment.

• 한국초전도ㆍ저온공학회논문지
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• 제26권2호
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• pp.24-30
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• 2024

Metal 3D printing is utilized in various industrial fields due to its advantages, such as fewer restrictions on production shape and reduced production time and cost. Existing research on 3D printing metal materials focused on changes in material properties depending on manufacturing conditions and was mainly conducted in a room temperature environment. In order to apply metal 3D printing products to cryogenic applications, research on the properties of materials in cryogenic environments is necessary but still insufficient. In this study, we evaluate the properties of stainless steel (STS) 316L and CuCr1Zr manufactured by Laser Powder Bed Fusion (LPBF) in a cryogenic environment. CuCr1Zr is a precipitation hardening alloy, and changes in material properties were compared by applying various heat treatment conditions. The mechanical properties of materials manufactured using the LBPF method are evaluated through tensile tests at room temperature and cryogenic temperature (77 K), and the thermal properties are evaluated by deriving the thermal conductivity of CuCr1Zr according to various heat treatment conditions. In a cryogenic environment, the mechanical strength of STS 316L and CuCr1Zr increased by about 150% compared to room temperature, and the thermal conductivity of CuCr1Zr after heat treatment increased by about 6 to 10 times compared to before heat treatment at 40 K.

• 열처리공학회지
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• 제16권3호
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• pp.134-140
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• 2003

Effects of cryogenic treatment and tempering temperature on the amount of retained austenite, hardness and wear properties has been investigated using alloy tool steel, STD 11. Cryogenic treatments were performed at the temperatures of $-100^{\circ}C$, $-150^{\circ}C$ and $-196^{\circ}C$, and tempering were performed at $200^{\circ}C$ and $530^{\circ}C$. It was shown that lower hardness value was obtained on high temperature ($530^{\circ}C$) tempering even after cryogenic treatment. And retained austenite was not entirely transformed to martensite after cryogenic treatment even at $-196^{\circ}C$, which was not consistent with the belief that $-80^{\circ}C$ was sufficient to entirely transform any austenite retained in the quenched microstructure. Austenite retained in cryogenic treated condition was completely transformed to martensite only after tempering at $530^{\circ}C$. As far as wear test conditions in this investigation, it was found that cryogenic treatments improved the sliding wear resistance, but improvement of wear resistance was not directly related with retained austenite contents. And it was found that predominent wear mechanisms of STD 11 steel were oxidation wear and adhesive wear In sliding wear conditions.

• 대한기계학회논문집A
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• 제22권2호
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• pp.343-351
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• 1998

This paper was investigated degradation of the fracture toughness caused by sensitizing heat-treatment of the cryogenic structural material JN1 base metal using unloading compliance method reported as useful a method in evaluating the elastic-plastic fracture toughness at cryogenic temperature. The specimens used in this paper were 20% side-grooved 0.5T-CT specimens which were machined in the JN1 base metal. Also, to investigate cryogenic fracture toughness of the fusion line region in the JN1 GTA weldments, it was also used 20% side-grooved 0.5T-CT specimens that was machined fusion line to located in the middle of the specimen. The cryogenic fracture toughness values of the JN1 base metal were significantly decreased with increasing the time and temperature of the heat treatment. The fracture toughness value obtained from the fusion line specimen was invalid, but it was lower value than that of the JN1 base metal. Especially, this value was approximately equal with that obtained from the JN1 650.deg. C-5h heat-treated material.

• 대한기계학회논문집A
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• 제22권2호
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• pp.311-320
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• 1998

The cryogenic fracture behaviors of austenitic stainless steel HN2 developed for nuclear fusion reactor were evaluated quantitatively by using the small punch(SP) test. The electrochemical polarization test was applied to study thermal aging degradation of HN2 steel. The X-ray diffraction(XRD) analysis was conducted to detect carbides and nitrides precipitated on the grain boundary of the heat treated HN2 steel. The mechanical properties of the HN2 steel significantly decreased with increasing time and temperature of heat treatment or with decreasing testing temperature. The integrated charge(Q) obtained from electrochemical polarization test showed a good correlation with the SP energy(ESP) obtained by means of SP tests. From the results observed in the x-ray diffraction and anodic polarization curve, it was known that the material the grain boundary. Combining SP test and electrochemical polarization test, it could be useful tools to non-destructively evaluate the cryogenic fracture behaviors and the aging degradation for cryogenic structural material.

• 열처리공학회지
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• 제28권3호
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• pp.139-145
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• 2015

Effects of austenitizing, cryogenic treatment and tempering conditions on the phase change, microstructure and Vickers hardness value have been studied in STD11 steel for tool and die. The volume fraction of retained austenite increased with a rise in austenitizing temperature, while the volume fraction of eutectoid $M_7C_3$ carbides decreased. The retained austenite could be reduced by cryogenic treatment i.e., maintaining at $LN_2$ temperature ($-196^{\circ}C$) for 12hrs but a little amount of retained austenite did not transform to martensite further although holding time increased to 24 hrs or more. The microstructure of the quenched and then cryogenictreated specimen showed nano-sized and needle-shaped carbides in matrix due to the decomposition of martensite by tempering, but that of the one without cryogenic treatment still revealed retained austenite by tempering even at $500^{\circ}C$.

• 열처리공학회지
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• 제18권2호
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• pp.134-138
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• 2005

• 열처리공학회지
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• 제18권3호
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• pp.202-207
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• 2005

• 열처리공학회지
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• 제18권1호
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• pp.54-57
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• 2005

• 열처리공학회지
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• 제18권4호
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• pp.261-264
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• 2005