• Title/Summary/Keyword: Cryogenic Heat Treatment

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A study on the transient cooling process of a vertical-high temperature tube in an annular flow channel (환상유로에 있어서 수직고온관의 과도적 냉각과정에 관한 연구)

  • 정대인;김경근
    • Journal of Advanced Marine Engineering and Technology
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    • v.10 no.2
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    • pp.156-164
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    • 1986
  • In the case of boiling on high temperature wall, vapor film covers fully or parcially the surface. This phenomenon, film boiling or transition boiling, is very important in the surface heat treatment of metal, design of cryogenic heat exchanger and emergency cooling of nuclear reactor. Mainly supposed hydraulic-thermal accidents in nuclear reactor are LCCA (Loss of Coolant Accident) and PCM (Power-Cooling Mismatch). Recently, world-wide studies on reflooding of high temperature rod bundles after the occurrence of the above accidents focus attention on wall temperature history and required time in transient cooling process, wall superheat at rewet point, heat flux-wall superheat relationship beyond the transition boiling region, and two-phase flow state near the surface. It is considered that the further systematical study in this field will be in need in spite of the previous results in ref. (2), (3), (4). The paper is the study about the fast transient cooling process following the wall temperature excursion under the CHF (Critical Heat Flux) condition in a forced convective subcooled boiling system. The test section is a vertically arranged concentric annulus of 800 mm long and 10 mm hydraulic diameter. The inner tube, SUS 304 of 400 mm long, 8 mm I.D, and 7 mm O.D., is heated uniformly by the low voltage AC power. The wall temperature measurements were performed at the axial distance from the inlet of the heating tube, z=390 mm. 6 chromel- alumel thermocouples of 76 .mu.m were press fitted to the inner surface of the heating tube periphery. To investigate the heat transfer characteristics during the fast transient cooling process, the outer surface (fluid side) temperature and the surface heat flux are computed from the measured inner surface temperature history by means of a numerical method for inverse problems of transient heat conduction. Present cooling (boiling) curve is sufficiently compared with the previous results.

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Microstructure and Electrical Properties of Low Temperature Processed Ohmic Contacts to p-Type GaN

  • Park, Mi-Ran;Song, Young-Joo;Anderson, Wayne A.
    • ETRI Journal
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    • v.24 no.5
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    • pp.349-359
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    • 2002
  • With Ni/Au and Pd/Au metal schemes and low temperature processing, we formed low resistance stable Ohmic contacts to p-type GaN. Our investigation was preceded by conventional cleaning, followed by treatment in boiling $HNO_3$:HCl (1:3). Metallization was by thermally evaporating 30 nm Ni/15 nm Au or 25 nm Pd/15 nm Au. After heat treatment in $O_2$ + $N_2$ at various temperatures, the contacts were subsequently cooled in liquid nitrogen. Cryogenic cooling following heat treatment at $600^{\circ}C$ decreased the specific contact resistance from $9.84{\times}10^{-4}$ ${\Omega}cm^2$ to $2.65{\times}10^{-4}$ ${\Omega}cm^2$ for the Ni/Au contacts, while this increased it from $1.80{\times}10^{-4}$ ${\Omega}cm^2$ to $3.34{\times}10^{-4}$ ${\Omega}cm^2$ for the Pd/Au contacts. The Ni/Au contacts showed slightly higher specific contact resistance than the Pd/Au contacts, although they were more stable than the Pd contacts. X-ray photoelectron spectroscopy depth profiling showed the Ni contacts to be NiO followed by Au at the interface for the Ni/Au contacts, whereas the Pd/Au contacts exhibited a Pd:Au solid solution. The contacts quenched in liquid nitrogen following sintering were much more uniform under atomic force microscopy examination and gave a 3 times lower contact resistance with the Ni/Au design. Current-voltage-temperature analysis revealed that conduction was predominantly by thermionic field emission.

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Process Design and Analysis of BOG Re-liquefaction System with Pre-liquefaction of NGL (NGL 분리식 BOG 재액화 공정 고안 및 해석)

  • Yun, Sang-Kook
    • Journal of the Korean Institute of Gas
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    • v.19 no.3
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    • pp.32-37
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    • 2015
  • The boil-off-gases(BOG) in cryogenic LNG storage tanks are generating continuously due to the heat leakage and need to be re-liquefied by the effective way. As the present method to reliquefy BOG is using LNG cold energy to be supplied after low pressure primary pump, the demand of LNG flow rate should be over 10 times of BOG produced rate to reliquefy it. This research invented new effective re-liquefaction system having only 3~4 times of LNG flow rate against unit BOG, that the pre-liquefaction process of NGL and the use of high pressure LNG cold energy after secondary pump. By the analysis, it could be high efficient reliquefying system for all amount of BOG treatment even during the summer time, and improvement of operation safety and efficiency of LNG terminal.

Microstructure and High Temperature Mechanical Properties of Oxide Dispersion Strengthened Steels Manufactured by Combination Milling Process (복합 밀링 공정으로 제조된 산화물 분산 강화 강의 미세조직 및 고온 기계적 특성)

  • Lee, Jung-Uk;Kim, Young-Kyun;Kim, Jeoung Han;Kim, Hwi-Jin;Lee, Kee-Ahn
    • Journal of Powder Materials
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    • v.28 no.5
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    • pp.389-395
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    • 2021
  • Oxide dispersion-strengthened (ODS) steel has excellent high-temperature properties, corrosion resistance, and oxidation resistance, and is expected to be applicable in various fields. Recently, various studies on mechanical alloying (MA) have been conducted for the dispersion of oxide particles in ODS steel with a high number density. In this study, ODS steel is manufactured by introducing a complex milling process in which planetary ball milling, cryogenic ball milling, and drum ball milling are sequentially performed, and the microstructure and high-temperature mechanical properties of the ODS steel are investigated. The microstructure observation revealed that the structure is stretched in the extrusion direction, even after the heat treatment. In addition, transmission electron microscopy (TEM) analysis confirmed the presence of oxide particles in the range of 5 to 10 nm. As a result of the room-temperature and high-temperature compression tests, the yield strengths were measured as 1430, 1388, 418, and 163 MPa at 25, 500, 700, and 900℃, respectively. Based on these results, the correlation between the microstructure and mechanical properties of ODS steel manufactured using the composite milling process is also discussed.