• Title/Summary/Keyword: CoreOnto

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Determination of meloxicam in human plasma by semi-micro high-performance liqiud chromatography.

  • Park, Chang-Hun;Kim, Ho-Hyun;Lee, Hee-Joo;Beom, Han-Sang
    • Proceedings of the PSK Conference
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    • 2003.04a
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    • pp.276.1-276.1
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    • 2003
  • This study describes a simple and sensitive semi-micro HPLC method with UV detection and direct deproteinization. The plasma protein was precipitated using perchloric acid (60%) and the supernatant was directly injected onto the semi-micro HPLC system. The separation was achieved on a C18 (25 mm ${\times}$ 2.0 mm I.D) analytical column with a mobile phase of sodium acetate buffer (pH 3.5, 50 mmol) - acetonitrile (60:40, V/V). (omitted)

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Synthesis of well-aligned thin multiwalled carbon nanotubes on the silicon substrate and their field emission properties

  • Yuan, Huajun;Shin, Dong-Hoon;Kim, Bawl;Lee, Cheol-Jin
    • Carbon letters
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    • v.12 no.4
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    • pp.218-222
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    • 2011
  • Well-aligned multi-walled carbon nanotubes (MWCNTs) were successfully synthesized by catalytic chemical vapor deposition using a hydrogen sulfide ($H_2S$) additive onto Al/Fe thin film deposited on Si wafers. Transmission electron microscopy images indicated that the as-grown carbon products were thin MWCNTs with small outer diameters of less than 10 nm. $H_2S$ plays a key role in synthesizing thin MWCNTs with a large inside hollow core. The well-aligned thin MWCNTs showed a low turn-on voltage of about 1.1 V/${\mu}m$ at a current density of 0.1 ${\mu}A/cm^2$ and a high emission current of about 1.0 mA/$cm^2$ at a bias field of 2.3 V/${\mu}m$. We suggest a possible growth mechanism for the well-aligned thin MWCNTs with a large inside hollow core.

PIV Measurements of the Pressure Driven Flow Inside a T-Shaped Microchannel (T형 마이크로채널 내부 압력구동 유동의 PIV 계측)

  • Choi Jayho;Lee In-Seop
    • Proceedings of the KSME Conference
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    • 2002.08a
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    • pp.423-426
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    • 2002
  • A custom micro-PIV optics assembly has been used to measure the flow field inside a T-shaped microchannel. The micro-PIV system consists of microscope objectives of various magnifications, a dichroic cube, and an 8-bit CCD camera. Fluorescent particles of diameters 620nm have been used with a Nd:YAG laser and color filters. A programmable syringe pump with Teflon tubings were used to inject particle-seeded distilled water into the channel at flow rates of $420,\;40,\;60{\mu}L/hr$. The microchannels are fabricated with PDMS with a silicon mold, then $O_2-ion$ bonded onto a slide glass. Results show differences in flow characteristics and resolution according to fluid injection rates, and magnifications, respectively. The results show PIV results with vector-to-vector distances of $2{\mu}m$ with 32 pixel-square interrogation windows at $50{\%}$ overlap.

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Chemical Doping of Graphene by Altretamine(2,4,6-Tris [dimethylamino]-1,3,5-Triazine)

  • Park, Sun-Min;Yang, Se-Na;Lim, Hee-Seon;Lee, Han-Gil
    • Bulletin of the Korean Chemical Society
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    • v.32 no.7
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    • pp.2199-2202
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    • 2011
  • The electronic properties of altretamine(2,4,6-tris [dimethylamino]-1,3,5-triazine) adsorbed on epitaxial graphene (EG) were investigated by core-level photoemission spectroscopy (CLPES) in conjunction with low energy electron diffraction (LEED). We found that altretamine molecule adsorbed onto interface layer (S1) of graphene as we confirm decrement of S1 peak using CLPES and haziness of LEED pattern. Moreover, the measured work function changes verified that increased adsorption of the altretamine on graphene layer showed n-type doping characteristics due to charge transfer from altretamine to graphene through the nitrogens. Two distinct nitrogen bonding feature associated with the N 1s peak was clearly observed in the core-level spectra indicating two different chemical environments.

Monodisperse Micrometer-Ranged Poly(methyl methacrylate) Hybrid Particles Coated with a Uniform Silica Layer

  • Han, Seung-Jin;Shin, Kyo-Min;Suh, Kyung-Do;Ryu, Jee-Hyun
    • Macromolecular Research
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    • v.16 no.5
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    • pp.399-403
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    • 2008
  • Monodisperse, micron-sized, hybrid particles having a core-shell structure were prepared by coating the surface of poly(methyl methacrylate)(PMMA) microspheres with silica and by copolymerizing acrylamide (AAm) to supply the hydrogen bonding effect by means of the amide groups. Tetraethoxysilane (TEOS) was then slowly dropped onto the medium under certain conditions. Because of the hydrogen bonding between the amide of the PMMA particles and the hydroxyl group of the hydrolyzed silanol, a silica shell was generated on the PMMA core particles. The morphology of the hybrid particles was investigated with transmission (TEM) and scanning (SEM) electron microscopy as a function of the medium conditions and the amount of TEOS. Improved thermal properties were observed by TGA analysis.

Structural Safety Evaluation of Hydraulic Steering System for Ship (선박용 유압 조타 시스템의 구조적 안전성 평가)

  • Lee, Moonhee;Son, Insoo;Yang, Changgun
    • Journal of the Korean Society of Industry Convergence
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    • v.23 no.4_2
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    • pp.661-667
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    • 2020
  • The optimal shape modeling of core parts through 3D modeling and structural analysis for the development of small and medium-sized ships. The goal is to improve the efficient structure of the hydraulic system for controlling the rudder among the core steering parts in small and medium-sized ships. Through 3D modeling and structural analysis, a new concept of tiller parts and a double-acting hydraulic cylinder control system were proposed and operational structural stability was evaluated. Structural analysis of the three different tiller designs that can be replaceable onto existing fishing vessels was conducted to derive the final shapes. The emphasis was placed on evaluating the structural stability of the key drive components, the tiller, pin, and cylinder rodin the maximum torque condition of the hydraulic cylinder.

Growth and Electronic Properties of Ag Overlayers on Stepped Pt(211) Surface

  • 김유권;김정원;김세훈
    • Bulletin of the Korean Chemical Society
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    • v.17 no.12
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    • pp.1154-1157
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    • 1996
  • The growth and electronic properties of ultrathin silver films deposited onto Pt(211) surface were studied using Auger electron spectroscopy (AES), low-energy electron diffraction (LEED), and x-ray photoelectron spectroscopy. The AES and LEED results indicate that the silver grows by a layer by layer growth followed by three dimensional islands growth. The XPS results show that the Ag 3d core-level binding energy of Ag overlayers on Pt(211) shifts toward lower binding energy relative to the bulk value at lower Ag coverage. This negative binding energy shift of the Ag 3d core level is explained by the reduced coordination number of the overlayer atoms and the resulting initial state band narrowing effect suggested by Wertheim and Citrin [Phys. Rev. Lett. 1978, 41, 1425].

Dynamic Stability Effect of Applicable Core and Neuromuscular Training for 12 Weeks (12주간 적용 가능한 코어, 신경근 훈련의 동적 안정성 효과)

  • Kim, Kyoung-Hun;Lee, Sung-Cheol
    • Korean Journal of Applied Biomechanics
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    • v.20 no.1
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    • pp.101-108
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    • 2010
  • Recently, core and neuromuscular training(CNT) is emerging as a clinically relevant tool to improve neuromuscular control and to prevent sports injuries. The purpose of this study was to examine the effect of a 12 weeks CNT program on the dynamic stability after drop landing. The subjects attempted drop landing onto the force platform on single foot from a 40 cm height distance. The collected data was used to calculate the dynamic stability index. The Dynamic stability index was derived by measuring the medial-lateral stability index(MLSI), anterior-posterior stability index(APSI), and the vertical stability index(VSI). In comparison to the control group, the MLSI and APSI showed no difference, yet, it resulted in higher VSI. The results of this study suggest that CNT is worthwhile to be considered as a way to improve neuromuscular control and to prevent traumatic injuries. However, the results are taking into consideration to discuss the limitations of CNT and suggested future approaches.

The Fabrication of PVA Polymer Coated on the Surface of B4C Nanocomposite by High Energy Ball Mill (고에너지볼밀을 이용한 PVA 고분자가 표면 코팅된 B4C 나노복합재 제조)

  • Uhm, Young-Rang;Kim, Jae-Woo;Jung, Jin-Woo;Rhee, Chang-Kyu
    • Journal of Powder Materials
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    • v.16 no.2
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    • pp.110-114
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    • 2009
  • Mechanical coating process was applied to form 89 %-hydrolyzed poly vinyl alcohol (PVA) onto boron carbide ($B_4C$) nanopowder using one step high energy ball mill method. The polymer layer coated on the surface of B4C was changed to glass-like phase. The average particle size of core/shell structured $B_4C$/PVA was about 50 nm. The core/shell structured $B_4C$/PVA was formed by dry milling. However, the hydrolyzed PVA of $98{\sim}99%$ with high glass transition temperature ($T_g$) was rarely coated on the powder. The $T_g$ of polymer materials was one of keys for guest polymer coating on to the host powder by solvent free milling.

Properties of Friction Coefficient with Re-Ir Coating Surface (Re-Ir 코팅에 따른 표면 마찰 계수 특성 연구)

  • Lee, Ho-Shik;Cheon, Min-Woo;Park, Yong-Pil
    • Proceedings of the Korean Institute of Information and Commucation Sciences Conference
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    • 2011.05a
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    • pp.676-677
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    • 2011
  • Rhenium-Iridium(Re-Ir) thin films were deposited onto the tungsten carbide(WC) molding core by sputtering system. The Re-Ir thin films on tungsten carbide molding core were analyzed by scanning electron microscope(SEM) and surface roughness. The Re-Ir coating technique has been intensive efforts in the field of coating process because the coating technique and process have been their feature, like hardness, high elasticity, adrasion resistance and mechanical stability and also have been applied widely the industrial and biomedical areas. In this report, tungsten carbide(WC) molding core was manufactures using high performance precision machining and the efforts of Re-Ir coating on the surface roughness.

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