• Title/Summary/Keyword: Constanct current density

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Dielectric breakdown of anodic oxide films formed on AA6061 in 20% H2O4and 8% H2SO4+ 3% C2H2O4 solutions (20% 황산 및 8% 황산 + 3% 옥살산에서 AA6061 합금 표면에 형성된 아노다이징 피막의 내전압 특성)

  • Cheolgi Park;Jaehwak Jang;Yunsuk Hyun;Sungmo Moon
    • Journal of the Korean institute of surface engineering
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    • v.57 no.1
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    • pp.8-13
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    • 2024
  • Anodizing of Al6061 alloy was conducted in two different electrolytes of 20% sulfuric acid and 8% sulfuric acid + 3 % oxalic acid solutions at a constant current or decreasing current density conditions, and its dielectric breakdown voltage was measured. The surface morphology of anodic oxide films was observed by TEM and thermal treatment was carried out at 400 ℃ for 2 h to evaluate the resistance of the anodic oxide films to crack initiation. The anodic oxide film formed in 8% sulfuric acid + 3 % oxalic acid solution showed higher dielectric breakdown voltage and better resistance to crack initiation at 400 ℃ than that formed in 20% sulfuric acid solution. The dielectric breakdown voltage increased 6 ~12% by applying decreasing current density comparing with a constant current density.