• Journal of the Korean Applied Science and Technology
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• v.33 no.1
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• pp.23-29
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• 2016

Zinc oxide of hexagonal wurzite, is known as n-type semiconductor. It has a wide band gap energy of 3.37 eV and large exciton binding energy of 60 meV. It can be widely applied to gas sensors, laser diodes, dye-sensitized solar cells and degradation of dye waste. The use of microwave hydrothermal synthesis brings a rapid reaction rate, high yield, and energy saving. Amine additives control the different particle shapes because of the chelate effect and formation of hydroxide ion. In this study, zinc nitrate hexahydrate was used as zinc precursor. In addition, ethanolamine, ethylenediamine, diethylenetriamine, and hexamethylenetetramine are used as shape control agent. The pH value was controlled as 11 by NaOH. The shapes of zinc oxide are star-like, rod, flower-like, and circular cone. In order to analyze physical, chemical, and optical properties of ZnO with diverse amine additives, we used XRD, SEM, EDS, FT-IR, UV-Vis spectroscopy, and PL spectroscopy.

• Journal of the Korean Wood Science and Technology
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• v.38 no.3
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• pp.170-177
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• 2010

Finite element numerical analysis was conducted with using the knot data which has a strong influence on the prediction of capacity for the structural wood member. Wood is a orthotropic property unlike other structural materials, so orthotropic property was applied. Knot was modelled as a cylinder shape, cone shape, and cubic shape. Compressive test was carried out to investigate the failure types and to calculate ultimate strengths for the wood members. Numerical model which can reflect the member size, number of knot, location of knot, size of knot was created and analyzed. By the numerical analysis using the ultimate compressive strength, numerical stress distribution types of each specimen was compared to real failure types for the test specimen. Cylinder shape modelling might be most reasonable, according to the necessary time for the analysis, the difficulty of element meshing, and the similarity of stress transfer around knot. Moreover, according to the stress and deformation distribution for the numerical analysis, failures or cracks of real specimen were developed in the vicinity of stress concentrated section and most transformed section. Based on the those results, numerical analysis could be utilized as a useful method to analyze the performance of bending member and tensile member, if only orthotropic property and knot modelling were properly applied.

• Journal of Industrial Technology
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• v.20 no.A
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• pp.101-111
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• 2000

This research is results of experimental and numerical works on characteristic of strength increase and bearing capacity in dredged and reclaimed soil due to desiccation shrinkage. For a soil sampled from southern coastal area in Korea, basic soil property tests and standard consolidation test with falling head permeability tests were carried out to obtain consolidational characteristics of soil. Double cone penetration test, laboratory vane test and unconfined compression test were also performed to investigate the change of shear strength with degree of desiccation. Model tests were performed in 1G environment and 30G level artificially accelerated condition by using the centrifuge model test facilities to investigate the bearing capacity of desiccated ground. Test results were analyzed by using the theoretical and load-settlement characteristics method proposed by Meyehof & Hanna(1978). On the other hands, the numerical technique, using the finite strain consolidation theory considering the effect of desiccation was used to estimate the appropriate time of using heavy construction equipments in field with respect to strength increase due to desiccation.

• Proceedings of the Korean Vacuum Society Conference
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• 2016.02a
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• pp.282.2-282.2
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• 2016

중적외선 물질에는 Ge, ZnS, ZnSe, Si 등이 있으나 고굴절율이므로 반사가 매우 크게 발생을 한다. 이를 줄이기 위해 다층 박막 무반사 코팅을 일반적으로 사용하지만 열에 취약함, 적합한 물질을 찾는 것이 매우 어려움, 다층 박막으로 제작 시 두께가 매우 두꺼워짐의 단점이 있다. 또한 Ge, ZnS, ZnSe 의 소재는 가격이 Silicon에 비해 매우 비싸다. 그러므로 RCWA(Rigorous Coupled Wavelength Analysis) 시뮬레이션을 이용하여 상대적으로 저렴한 소재임에도 고투과성을 지닌 중적외선용 무반사 실리콘 서브파장구조(Subwavelength Structures, SWSs)를 제안한다. 본 연구에서는 원기둥, 원뿔, 파라볼라, 잘린 원뿔(truncated cone) 등의 형태에 따른 투과율 특성을 파악하여 최적구조가 파라볼라 형태임을 증명하였다. 또한 서브파장구조의 주기, 높이의 특성을 조절하여 공정 시의 종횡비(Aspect ratio)를 고려한 최적형태를 제안하였다. 중적외선 영역($3{\mu}m{\sim}5{\mu}m$)에서 일반 Silicon의 적외선 영역에서 평균 55%의 낮은 투과율을 보이나, 양면에 무반사 구조를 설계 하였을 때 평균 94%의 높은 투과율을 확인할 수 있다. 다양한 형태를 가진 무반사 실리콘 서브파장 구조물을 RCWA 방식으로 계산함으로서 특성을 파악하며 최적구조를 설계 할 수 있다. 또한 단면에 비하여 양면으로 SWSs 구조를 제작할 시 매우 두드러지는 투과특성을 확인할 수 있다. 고굴절율이지만 뛰어난 투과특성을 이용하여 초소형 적외선 카메라 렌즈 뿐만 아니라 적외선 광검출기, 광학 필터 등에 이용 가능할 것으로 예상된다.

• Journal of Ocean Engineering and Technology
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• v.29 no.1
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• pp.85-93
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• 2015

In this study, tensile tests were performed on aluminum alloys (AA6061 and AA6082) to investigate their mechanical behaviors at cryogenic temperatures. The temperature was varied from 110 K up to 293 K, and quasi-static strain rates of 10⁻⁴ s⁻¹ −10⁻² s⁻¹ were taken into account for the tests. The experimental results were analyzed to find the dependence on the temperature, strain rate, and fractured surfaces. As a result, it was found that the strength and elongation of the aluminum alloys were improved when the temperature was decreased. In addition, it was confirmed that the mechanical behaviors of the aluminum alloys were not dependant on the strain rate. Under a tensile load, two types of fractures were seen in the aluminum alloys: cup-cone (AA6061) and shear (AA6082).

• Journal of the Korean Applied Science and Technology
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• v.15 no.3
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• pp.61-66
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• 1998

Cyclodextrin are obtained from starch by enzymatic degradation. The three best characterize forms are ${\alpha}$, ${\beta}$, ${\gamma}$ cyclodextrin consisting of 6, 7, and 8 D-glucose units, respectively. Each of the glucose units are in the rigid C1 chair conformation and are linked by ${\alpha}$ 1,4 bonds. This geometry gives the cyclodextrin the shape of a hollow truncated cone with the wider side formed by the secondary 2- and 3-hydroxy groups and the narrower side by the primary 6-hydroxy group. The most characteristics property of the cyclodextrin is their ability to form inclusion complexes with a wide range of guest moleculars. We syntheses per-6-substituted ${\beta}$-cyclodextrin derivatives and investigate structures, spectrospcopic properties. The substituted materials are piperidine, piperazin, morphorine. The synthetic compound showed a good solubility than natural ${\beta}$ cyclodextrin in organic solvents such as methylene chloride, methanol, ethanol, etc.

• Journal of Oral Medicine and Pain
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• v.15 no.1
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• pp.9-25
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• 1991

타액의 유동학적 성질은 타액의 윤활작용 및 구강내 경조직, 연조직 보호작용에 영향을 미친다. 그러므로 타액의 유동성을 잘 이해하면, 구강내 기능적 불편감의 평가와 인공타액의 개발에 필요한 중요한 정보를 얻을 수 있다. 저자는 전단율 변화에 따른 타액점도 변화의 연령 및 성별에 따른 차이를 알고자, 각 연령층별로 구강건조증으로 고통받은 병력이 없으며 타액채취시 약물을 복용하고 있지 않은 남녀 각 20명씩 총 240명을 대상으로 자극시 분비된 타액의 점도를 cone-and-plate 형태의 점도계를 이용하여 전단율 11.3에서부터 450.0(/sec )사이에서 측정하였다. 또, 20대 남녀 각각 20명의 경우, 자극시 분비 된 전타액의 점도와 함께 비자극시 분비된 전타액, 자극시 분비된 이하선 타액, 자극시 분비된 악하선 설하선 혼합타액의 점도를 같은 방법으로 측정한 결과 다음과 같은 결론을 얻었다. 1. 타액은 점탄성의 성질을 가지는 non-Newtonian 유체로서 점도와 전단율 사이의 관계는 점근선으로 표시될 수 있었다. 2. 자극시 분비된 전타액의 점도는 연령이 높을수록 증가된 양상을 보였으나, 남자의 경우 50대 이상에서 가장 높고 여자의 경우 30대에서 가장 높았다. 3. 자극시 분비된 전타액의 점도는 20대, 30대, 40대에서 여자가 남자보다 높았다. 4. 타액 점도는 자극시 분비된 악하선 설하선 혼합타액에서 가장 높았으며, 비자극시 분비된 전타액, 자극시 분비된 전타액, 자극시 분비된 이하선 타액 순이었다.

• Geotechnical Engineering
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• v.14 no.2
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• pp.79-92
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• 1998

Parametric studies based on laboratory pilot tests were performed to investigate the relationships between electrical resistivity and properties of contaminated soils. Three kinds of sandy soils sampled and leachate from an industrial waste landfill were mired to model the contaminated soils. Electrical resistivity of soils was measured by using a simulated resistivity cone penetrometer probe. In the experiments. the electrical resistivity was observed by changing the water content, void ratio, unit weight, degree of saturation, and concentration of the leachate. The test results show that the electrical resistivity of soils depends largely on the water content and the electrical property of pore water rather than unit weight and types of soils.

• Applied Chemistry for Engineering
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• v.18 no.2
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• pp.194-198
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• 2007

Veneer plate was painted by the treatment with ammonium salts such as ammonium chloride (AMCR), ammonium sulfate (AMSF), monoammonium phosphate (MAPP), and diammonium phosphate (DAPP) at room temperature. The physical property and flammability of painted veneer plate were investigated. In order to evaluate flammability of the treated veneer with ammonium salts, heat release rate (HRR) of the veneer was measured by a cone calorimeter according to ISO 5660-1 standard. The flammability painted veneener plate with ammonium salts was reduced compared to virgin veneer plate. The flashover possibility of veneer plates treated with these ammonium salts was examined by R. V. Petrella's classification using time to ignition and peak heat release rate. The specific gravities of veneer plates treated with only ammonium sulfate were higher than that of virgin veneer plate. Also, the veneer plates treated with ammonium salts showed lower equilibrium moisture contents over virgin veneer.

• Restorative Dentistry and Endodontics
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• v.11 no.1
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• pp.27-32
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• 1985

The purpose of this study was to examine the influence of canal irrigants and smear layer on the property of apical seal. Fourty-five canals from human teeth were randomly selected and divided into 5 groups according to the irrigants used in conjunction with instrumentation. The irrigants were RC-prep in combination with Naocl, Citric acid, Naocl, Naocl in combination with $H_2O_2$, and normal saline solution. After instrumention and dry the canal with paper point, the canals were obturated by lateral condensation of Zinc-oxide eugenol sealer and gutta percha cone. All the specimens were immersed in 2% methylene blue dye solution for 7 days and the depth of dye penetration into the canals was evaluated by macros cope. The following results were obtained. 1. All the canals experimented showed varying degree of dye penetration. 2. There was no significant difference in depth of dye penetration between the groups known to be effective and ineffective in the removal of the smear layer. 3. The canals irrigated with NaOCl alone showed the highest dye penetration and mean leakage was 7.7 mm. 4. In the canals irrigated with RC-prep in combination with Naocl and citric acid, the mean dye penetration was 5.5 mm and 4.8 mm respectively, and the canals irrigated with NaOCl in combination with $H_2O_2$ and normal saline solution revealed mean dye penetration of 3.9 mm.