• Title/Summary/Keyword: Columnar

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Thermal Durability of 4YSZ Thermal Barrier Coating Deposited by Electron Beam PVD (전자빔을 이용한 물리기상증착법으로 제조된 열차폐용 4 mol% YSZ 코팅의 내열특성)

  • Park, Chanyoung;Yang, Younghwan;Kim, Seongwon;Lee, Sungmin;Kim, Hyungtae;Lim, Daesoon;Jang, Byungkoog;Oh, Yoonsuk
    • Journal of Powder Materials
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    • v.20 no.6
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    • pp.460-466
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    • 2013
  • 4 mol% Yttria-stabilized zirconia (4YSZ) coatings with $200{\mu}m$ thick are fabricated by Electron Beam Physical Vapor Deposition (EB-PVD) for thermal barrier coating (TBC). $150{\mu}m$ of NiCrAlY based bond coat is prepared by conventional APS (Air Plasma Spray) method on the NiCrCoAl alloy substrate before deposition of top coating. 4 mol% YSZ top coating shows typical tetragonal phase and columnar structure due to vapor phase deposition process. The adhesion strength of coating is measured about 40 MPa. There is no delamination or cracking of coatings after thermal cyclic fatigue and shock test at $850^{\circ}C$.

The Tissue Distribution of Nesfatin-1/NUCB2 in Mouse

  • Kim, Jinhee;Chung, Yiwa;Kim, Heejeong;Im, Eunji;Lee, Hyojin;Yang, Hyunwon
    • Development and Reproduction
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    • v.18 no.4
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    • pp.301-309
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    • 2014
  • Nesfatin-1, an anorexic nucleobindin-2 (NUCB2)-derived hypothalamic peptide, controls appetite and energy metabolism. Recent studies show that nesfatin-1/NUCB2 is expressed not only in the brain but also in gastric and adipose tissues. Thus, we investigated the distributions of nesfatin-1/NUCB2 in various tissues of male and female mice by real-time PCR, western blotting, and immunohistochemical staining. Real-time PCR analyses showed that NUCB2 mRNA was predominantly expressed in the pituitary and at lower levels in the hypothalamus, spleen, thymus, heart, liver, and muscle of both male and female mice. Expression was much higher in reproductive organs, such as the testis, epididymis, ovary, and uterus, than in the hypothalamus. Western blot analysis of the nesfatin-1 protein level showed similar results to the real-time PCR analyses in both male and female mice. These results suggest that nesfatin-1/NUCB2 have widespread physiological effects in endocrine and non-endocrine organs. In addition, immunohistochemical staining revealed that nesfatin-1 was localized in interstitial cells, including Leydig cells and in the columnar epithelium of the epididymis. Nesfatin-1 was also expressed in theca cells and interstitial cells in the ovary and in epithelial cells of the endometrium and uterine glands in the uterus. These results suggest that nesfatin-1 is a novel potent regulator of steroidogenesis and gonadal function in male and female reproductive organs. Further studies are required to elucidate the functions of nesfatin-1 in various organs of male and female mice.

Effects of Estrogen Receptor $\alpha$-Selective Agonist Propyl Pyrazole Triol on the Morphology of Accessory Genital Glands of Male Mouse (수컷 생쥐 부속 생식샘의 형태에 미치는 에스트로겐 수용체 $\alpha$의 선택적 효능제 propyl pyrazole triol의 영향)

  • Han, Ji-Yeon;Cho, Hyun-Wook
    • Applied Microscopy
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    • v.39 no.1
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    • pp.17-25
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    • 2009
  • This study investigated that exposure of male mice to estrogen receptor $\alpha$-selective agonist, 4,4',4"-(4-propyl-[1H]-pyrazole-1,3,5-triyl)tris-phenol (PPT) induce morphological changes of accessory genital glands. The male reproductive organs were fixed and processed for light microscopy. The PPT induced decreases of ventral prostates, seminal vesicles and preputial glands weights with experimental time. The glandular lumen of ventral prostate was atrophied compared with control group. Type of epithelial tissues in the prostate was changed from simple columnar epithelium to stratified cuboidal or squamous epithelium. Treated group with the agonist showed that increased connective tissue underlying epithelium in the prostate and seminal vesicle. Especially, the glandular lumen of the seminal vesicle was contracted when PPT-treated animals were compared with control group. Secretion cells of preputial gland were smaller than that of control group. On week 8, PPT treatment caused decrease of epithelial cell height lining the lumen of preputial gland. These results provide information useful in researching the physiological function of estrogen mediated by estrogen receptor $\alpha$ in male accessory genital gland.

Effect of the Coating Structure on the Corrosion Resistance of Al-Mg Coated Steel (Al-Mg 코팅층의 구조가 강판 내식성에 미치는 영향)

  • Jung, Jae-Hun;Yang, Ji-Hoon;Kim, Sung-Hwan;Byeon, In-Seop;Jeong, Jae-In;Lee, Myeong-Hoon
    • Journal of Surface Science and Engineering
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    • v.49 no.5
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    • pp.454-460
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    • 2016
  • Double-layered Al-Mg films have been deposited by using an e-beam deposition method on a cold-rolled steel sheet(CR), which the structure of the film was Al/Mg/CR. The micro-structure, alloy phase, and corrosion resistance of the Al-Mg coated CR were investigated before and after heat treatment at $400^{\circ}C$ for 2, 3, and 10 min in a nitrogen atmosphere. Total thickness of Al-Mg films was fixed at $3{\mu}m$ and the thickness ratio of Al and Mg layers(Al:Mg) has been changed from 5:1 to 1:5. The cross-sectional morphology of the films, which had the thickness ratio of 2:1(Al:Mg), 1:1, and 1:2, was changed after heat treatment from columnar to featureless structure. The x-ray diffraction data for as-deposited films showed only pure Al and Mg peaks. Al-Mg alloy peaks such as $Al_3Mg_2$ and $Al_{12}Mg_{17}$ phase appeared after the heat treatment. The Al-Mg coating with the thickness ratio of 1:1(Al:Mg) showed the best corrosion resistance of up to 500 hours by salt spray test.

Palaeomagnetism of Tertiary Basins in Southern Korea: 2. Basaltic Rocks in the Central Part of Pohang Basin (남한 제3기 분지지역에 대한 고자기 연구 : 2. 포항분지 중부의 현무암질암)

  • Son, Moon;Kim, In-Soo
    • Economic and Environmental Geology
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    • v.29 no.3
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    • pp.369-380
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    • 1996
  • In order to determine the emplacement time and stratigraphic position of basaltic rocks in the central part of Pohang basin, palaeomagnetic investigations were conducted on 111 samples collected from 6 sites. Formation mean built from site-mean ChRM directions is $d=340.7^{\circ}$, $i=52.2^{\circ}$ (${\alpha}_{95}=6.0^{\circ}$, k=91) in the geographic coordinates. If "tilt" correction is applied regarding the plane perpendicular to the side walls of columnar joint as palaeohorizon, the formation mean becomes $d=328.7^{\circ}$, $i=43.8^{\circ}$ (${\alpha}_{95}=17.1^{\circ}$, k=13). It is to be noticed that the formation mean is deflected significantly (about $20{\sim}30^{\circ}$) counterclockwise from the Tertiary reference geomagnetic field of Eurasia, independent of "tilt" correction. This situation is very different from that of clockwise rotation of ChRM directions which has been ubiquitously observed in other Tertiary basins of south Korea, and indicates sinistral regional simple-shearing during the emplacement times of the basaltic rocks. Considering previous palaeomagnetic and AMS (anisotropy of magnetic susceptibility) data from other Tertiary regions of south Korea, the time of this sinistral shearing should be 15 Ma or directly thereafter, and this time point represents inversion from extensional to compressional tectonic regime. Magnetic foliation data obtained in this study indicate WNW-ESN compression during or directly after emplacement of the basaltic rocks, while it has known from regional tectonic study that the time of the WNW-ESN compression is about 15 Ma, when SW Honshu was rotated and the Korean strait was narrowed.

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In Situ Observation of Solidification Behavior in Undercooled $Pd_{40}Cu_{30}Ni_{10}P_{20}$ Alloy Melts during Linear Cooling (연속냉각 중 과냉 된 $Pd_{40}Cu_{30}Ni_{10}P_{20}$ 합금 용탕의 실시간 응고거동 관찰)

  • Kim, Ji-Hun
    • Journal of Korea Foundry Society
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    • v.23 no.5
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    • pp.276-285
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    • 2003
  • In the undercooled melt of $Pd_{40}Cu_{30}Ni_{10}P_{20}$ alloy, the solidification behavior including nucleation and growth of crystals at the micrometer level has been observed in-situ by use of a confocal scanning laser microscope combined with an infrared image furnace. The $Pd_{40}Cu_{30}Ni_{10}P_{20}$ alloy specimens were cooled from the liquid state to glass transition temperature. 575 K, at various cooling late under a helium gas flow. According to the cooling rate, the morphologies of the solidification front are changed among various types, irregular jog like front, columnar dendritic front, cellular grain, star like shape jog and fine grain, etc. The velocities of the solid-liquid interface are measured to be $10^{-5}{\sim}10^{-8}$ m/s which are at least two orders higher than the theoretical crystal growth rates. Combining the morphologies observed in terms of cooling rates and their solidification behaviors, we conclude that phase separation takes place in the undercooled molten $Pd_{40}Cu_{30}Ni_{10}P_{20}$ alloy. The continuous cooling transformation (CCT) diagram was constructed from solidification onset time at various linear cooling conditions with different rate. The CCT diagram suggests that the critical cooling rate for glassy solidification is about 1.5 K/s, which is in agreement with the previous calorimetric findings.

Reinforcement Effect of Marine Structure Foundation by Deep Mortar Piling (심층몰탈파일에 의한 호안구조물의 기초보강 효과)

  • Chun, Byung-Sik;Yang, Hyung-Chil;Yang, Jin-Suk
    • Journal of the Korean GEO-environmental Society
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    • v.2 no.2
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    • pp.41-50
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    • 2001
  • In this study, for the stability analysis of marine embankment, the slope stability analysis and possibility of lateral movement with the marine embankment in ${\bigcirc}{\bigcirc}$harbor were carried out. In order to simulate the practical site condition, the expected maximum sea water level and maximum embankment height were assumed for these analyses. For the evaluation of soil properties, field test, laboratory test, and especially chemical composition analysis were performed for the this analysis. Based on these test results, the soil parameters were determined by applying ground improvement concept under columnar stabilized ground condition and also the effect of staged backfilling was considered under the dredged ground condition. For the optimal design, the stability analyses of embankment with changed height and unchanged height were performed under unimproved soil condition. The result showed that both cases were unstable not only with slope stability but also with lateral movement. Therefore, Deep Mortar Piling was applied for stability analysis and this result was safe. As the conclusion, the deep mortar piling method was suggested as reinforced foundation design for this site.

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A Case Report of a Bronchogenic Cyst Misconceived to Lung Cancer (폐암으로 오인된 기관지성 낭종 1례)

  • Kim, Young Wook;Lee, Seong Hee;Hong, Soon Chang;Lee, Ho Hak;Park, Sang-Joon;Lee, Gwon Jun;Kim, Jhin Gook
    • Tuberculosis and Respiratory Diseases
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    • v.55 no.5
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    • pp.526-530
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    • 2003
  • Bronchogenic cysts are generally presented as a well defined mass that have thin and smooth wall in the intrapulmonary or mediastinal area by simple chest radiographs. We present the case of a 20-year-old man with a ill-defined left upper lobe mass, found by chest radiographs. At the preoperative examinations, chest computed tomography showed ill-defined mass with Hounsfield Number 26, and nonspecific findings were shown by the bronchoscopy and percutaneous needle aspiration. The patient was undertaken the left upper lobectomy. The surgical specimen contained a ill-defined mass, measuring $2{\times}3$ cm. On the section of the mass, a cyst containing dark brown thick materials was noted. The cyst was unilocular, and the wall showed a trabeculation. Microscopically, the cystic mass was lined with ciliated pseudostratified columnar epitheliums and surrounded by smooth muscle and cartilage.

Microstructure and Tensile Properties of SS400 Carbon Steel and SUS430 Stainless Steel Butt Joint by Gas Metal Arc Welding

  • Poonnayom, Pramote;Chantasri, Sakchai;Kaewwichit, Jesada;Roybang, Waraporn;Kimapong, Kittipong
    • International Journal of Advanced Culture Technology
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    • v.3 no.1
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    • pp.61-67
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    • 2015
  • The application of SS400 carbon steel and AISI430 ferritic stainless steel joint has been increased in industries because of the advantage of both metals was able to increase the service lifetime of the important structures. Therefore, a fusion welding process that could produce a sound weld and good joint properties should be optimized. This research is aimed to weld a butt joint of SS400 carbon steel and AISI430 ferritic stainless steel using Gas Metal Arc Welding (GMAW) welding process and to study the effects of welding parameters on joint properties. The experimental results were concluded as follows. The optimized welding parameter that produced the tensile strength of 448 MPa was the welding current of 110A, the welding speed of 400 mm/min and the mixed gas of $80%Ar+20%CO_2$. Increase of the welding current affected to increase and decrease the tensile strength of the joint, respectively. Lower welding current produced the incomplete bonding of the metals and indicated the low tensile strength. Microstructure investigation of the welded joint showed a columnar grain in the weld metal and a coarse grain in the heat affected zone (HAZ). The unknown hard precipitated phases were also found at the grain boundaries of the weld metal and HAZ. The hardness profile did not show the difference of the hardness on the joint that was welded by various welding currents but the hardness of the weld metal was higher than that of the other location.

Microstructure and Ferroelectric Properties of Sol-gel Derived $PbTiO_3$ Interlayered PZT Thin Films (졸-겔법으로 제조한 $PbTiO_3$ Interlayered PZT 박막의 미세구조와 강유전 특성)

  • 임동길;최세영;정형진;오영제
    • Journal of the Korean Ceramic Society
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    • v.32 no.12
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    • pp.1408-1416
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    • 1995
  • Microstructure and ferroelectric properties of sol-gel derived PZT(52/48) and PT interlayered PZT(52/48) thin films on Pt/Ti/SiO2/Si substrates were investigated. Films were fabricated using Acetylacetone chelated PT and PZT(52/48) sols. PZT(52/48) thin films annealed at $700^{\circ}C$ for 20 min showed the rosette structure with the size of 1.2~1.6${\mu}{\textrm}{m}$ and the pyrochlore phse was contained. PT interlayered PZT thin films, which is inserted by PbTiO3 thin layer with the thickness of 130 $\AA$ between PZT thin film and electrode, consisted of a single perovskite phase after annealing above 55$0^{\circ}C$. They exhibited the uniform and columnar grains of 0.1~0.16${\mu}{\textrm}{m}$, which are applicable for microelectronic device including non-volatile memory. Typical P-E hysteresis loops could be obtained from PT interlayered PZT thin film at as low as the annealing temperature of 50$0^{\circ}C$. Ferroelectric properties of PT interlayered PZT thin films were improved as increasing annealing temperature up to $700^{\circ}C$, and then deteriorated at 75$0^{\circ}C$. PZT(52/48) and PT interlayered PZT(52/48) thin film annealed at $700^{\circ}C$ for 20 min displayed Ps=38.8$\mu$C/$\textrm{cm}^2$, Pr=10.0$\mu$C/$\textrm{cm}^2$, Ec=65.3 kV/cm and Ps=28.5$\mu$C/$\textrm{cm}^2$, Pr=9.8$\mu$C/$\textrm{cm}^2$, Ec=76.1 kV/cm, respectively.

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