• Title/Summary/Keyword: Coercive force

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Influences of Plating Conditions on Magnetic Properties of Co-P Thin Films by Electroless Plating (무전해도금에 의한 코발트- 인 박막의 자성에 미치는 도금조건의 영향)

  • Choi, Byoung-Ik;Yeo, Woon-Kwan;Lee, Ju-Seong
    • Journal of the Korean institute of surface engineering
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    • v.19 no.1
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    • pp.3-12
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    • 1986
  • Influences of pH, temperature, and composition of bath on the deposition rate and the magnetic properties were studied for two kinds of electroless Co-P plating bath. The results obtained are as follows. Ammonia alkaline citrate bath was more stable than ammonia alkaline tartrate bath, and the film deposited from citrate bath gave a higher squareness. The magnetic properties of the film obtained from citrate bath greatly depended upon pH. Under the optimum conditions, the film deposited from citrate bath had coercive force of 330 Oe and squareness of 0.67. However the films deposited from tartrate bath had coercive force of 300 Oe and squareness of 0.58.

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Physical Properties of Polycrystalline Zinc-Substituted Lithium Ferrite (ZnO가 Lithium ferrite의 물리적 특성에 미치는 영향에 관한 연구)

  • 고재귀
    • Journal of the Korean Magnetics Society
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    • v.9 no.5
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    • pp.234-238
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    • 1999
  • Lithium ferrites are prominent in the element of microwave frequency communication core and high frequency memory core because of their low coercivity and the high squareness ratio. This paper reports primarily the development of lithium ferrites with the low coercivity and high squareness ratio. The materials with $Li_{0.48-0.5x}Bi_{0.02}Ni_{0.04}Zn_xFe_{2.46-0.5x}O_4$ (x = 0,0.01, 0.02, 0.03) have been prepared to investigate the physical properties. The addition of ZnO gave raised maximum induction $(B_m)$ and decreased coercive force $(H_c)$, but the squareness ratio $(R\;=\;B_m/B_r)$ was decreased. The specimen of squareness ratio R=0.82, coercive force $H_c=\;1.80\;Oe$ was obtained for $Li_{0.48-0.5x}Bi_{0.02}Ni_{0.04}Zn_xFe_{2.46-0.5x}O_4$ (X=0) sintered at 105$0^{\circ}C$. Also the sample of squareness ratio R = 0.75, coercive force $H_c=\;1.70\;Oe$ for $Li_{0.48-0.5x}Bi_{0.02}Ni_{0.04}Zn_xFe_{2.46-0.5x}O_4$ (X = 0) sintered at 110$0^{\circ}C$ was measured. The Tc was obtained 463$^{\circ}C$ and the Br of environmental temperature variation was stable.

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A Study on the Effects of first and second additives Magnetic Characteristics of Anisotropic $SrO-5.7Fe_2O_3$. (1,2차 첨가제가 이방성 $SrO-5.7Fe_2O_3$의 자기적 특성에 미치는 효과)

  • Song, Joon-Tae;Shin, Yeong-Duck;Jeong, In-Young;Jin, Hong-Bum
    • Proceedings of the KIEE Conference
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    • 1990.07a
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    • pp.239-242
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    • 1990
  • The effect of $CaCo_3$, $SrCo_3$, $SiO_2$ and $H_3BO_3$ in the range of 0.1-1.0 wt% on strontium ferrites consisting of the magnetoplumbite phase $SrO-5.7Fe_2O_3$ were investigated. The hysteresis loop, density, demagnetization curve and the intrinsic coercive force were measured on anisotropic ferrite. The particle diameter and 0.5(wt%) of second additive $CaCo_3$ is particularly important for the properties of anisotropic ferrite. When the particle diameter is decreased from 1.98(${\mu}m$) to 1.07(${\mu}m$), the remance is increased from 2900 to 4010(G) and the coercive force from 2150 to 2850(Oe) at a sintering temperature 1230 ($^{\circ}C$). Remance Br(G), coercleve force(Oe) and maximum energy product of sample A-16 are87(%), 56(%), 67(%) of S-W model theoretical value.

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A Study on Physical Properties Of Co3O4-added Ni- Zn Ferrite at High Frequency (Co3O4첨가에 따른 고주파용 Ni-Zn계 ferrite의 물리적 특성 연구)

  • Koh, Jae-Gui
    • Korean Journal of Materials Research
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    • v.12 no.10
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    • pp.791-795
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    • 2002
  • We studied the physical properties of $Co_3$$O_4$-added Ni-Zn ferrite which were sintered at 1050~110$0^{\circ}C$ for 2 hours. X-ray diffraction showed a spinel structure, and optical microscopy showed grain sizes of 5 to 10 $\mu\textrm{m}$. As the sintering temperature was increased from $1050^{\circ}C$ to $1070^{\circ}C$, the initial permeability and magnetic induction increased, and both of the loss factor and the coercive force decreased. The Curie temperatures were about $^234~245{\circ}C$ with added $Co_3$$O_4$. The initial permeability was 350 to 420 and maximum magnetic induction density and coercive force 4870G to 4980G and 0.15 Oe to 0.21 Oe, respectively which were similar to those of Ni-Zn ferrite synthesized in the conventional process. The frequency of specimen was in the range of 1MHz to 300MHz. In the plot of initial permeability vs. frequencies, a $180^{\circ}C$ rotation of the magnetic domain could be perceived in a broad band of microwave before and after the resonance frequency.

Crystalline Behavior and Microstructure Analysis in Fe73.28Si13.43B8.72Cu0.94Nb3.63 Alloy

  • Oh, Young Hwa;Kim, Yoon Bae;Seok, Hyun Kwang;Kim, Young-Woon
    • Applied Microscopy
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    • v.47 no.1
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    • pp.50-54
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    • 2017
  • The microstructure, the crystallization behavior, and magnetic properties of FeSi-based soft magnetic alloys (FINEMET) were investigated using transmission electron microscopy, X-ray diffraction, and coercive force measurements. The amorphous $Fe_{73.28}Si_{13.43}B_{8.72}Cu_{0.94}Nb_{3.63}$ alloys particles, prepared in $10^{-4}$ torr by gas atomization process, were heat treated at $530^{\circ}C$, $600^{\circ}C$, and $670^{\circ}C$ for 1 hour in a vacuum of $10^{-2}$ torr. Nanocrystalline Fe precipitation was first formed followed by the grain growth. Phase formation and crystallite sizes was compared linked to its magnetic behavior, which showed that excellent soft magnetic property can directly be correlated with its microstructure.

Characterization and Preparation of Glass-Ceramics in the System Fe_2O_3-CaO-SiO_2$ (I) (Fe_2O_3-CaO-SiO_2$계 결정화 유리의 제조 및 특성(I))

  • 이용근;최세영;김경남
    • Journal of the Korean Ceramic Society
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    • v.31 no.6
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    • pp.629-636
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    • 1994
  • The ferrimagnetic glass-ceramics in the system Fe2O3-CaO-SiO2 for hyperthermia were investigated. Glasses could be prepared up to the content of 40 wt% of Fe2O3 and below the weight ratio of 1.0 of CaO/SiO2. The maximum saturation magnetization and the maximum coercive force were 29.85 emu/g and 340.1 Oe respectively, for a glass 40Fe2O3.20CaO.40SiO2 composition heat-treated at 95$0^{\circ}C$ for 8 hours. And for a glass 40Fe2O3.30CaO.30SiO2 composition the maximum saturation magnetization and the maximum coercive force were 18.47 emu/g and 374.4 Oe heat-treated at 1,00$0^{\circ}C$ and 90$0^{\circ}C$ for 8 hours respectively. The maximum hysteresis loss was 1,726.3 cal/g for a glass 40Fe2O3.20CaO.40SiO2 composition heat-treated at 95$0^{\circ}C$ for 8 hours. It was found that the ferrimagnetic Fe2O3.CaO.SiO2 glass-ceramics was little injurious to human body as results of biocompatibility test and biotoxicity test.

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Evaluation of 1Cr-1Mo-0.25V Steel Degradation Using Magnetic Barkhausen Noise (Magnetic Barkhausen Noise를 이용한 1Cr-1Mo-0.25V강의 열화도 평가)

  • Lee, J.M.;Ahn, B.Y.;Nam, Y.H.;Nahm, S.H.;Lee, S.S.;Lee, O.S.
    • Proceedings of the KSME Conference
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    • 2001.06a
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    • pp.250-255
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    • 2001
  • It is inevitable to evaluate the life of turbine rotor because the operating periods of power plants need to be extended. The magnetic methods utilizing Magnetic Barkhausen noise curve were applied to detect the degradation caused by thermal aging. The Magnetic property of material depends on the domain dynamics and it is affected by the microstructure of material. Therefore the magnetic property is very sensitive to the microstructure change of the material. It is, thus, very useful to detect the state of degradation of varying materials. The test specimen made of 1Cr-1Mo-0.25V steel was used widely for turbine rotor material, and seven kinds of specimens with different degradation levels were prepared by the isothermal heat treatment at $630^{\circ}C$. With the increase of degradation, BHN was decreased. The result was compared with coercive force and vickers hardness.

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Fabrication of Barium Oxide Ferrite Magnet-II (바리움 훼라이트 자석의 시작 - II)

  • 백용현
    • 전기의세계
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    • v.21 no.6
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    • pp.17-20
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    • 1972
  • The magnetic properties of Ba-Ferrite ( $M^{+2}$O.nF $e_{2}$ $O_{3}$ is highly improved under the condition of composition ratio n=4.4 when B $i_{2}$ $O_{3}$ is added to Ferrite, the adding amount and sintering temperature which affect the magnetic properties were investigated and the following results; were obtained; 1. Magnetic properties are varied with B $i_{2}$ $O_{3}$ content and singering temperature, and coercive force and residual induction can be improved with B $i_{2}$ $O_{3}$. 2. The optimal content of B $i_{2}$ $O_{3}$ amount is about 4 mol %, 3. Without the addition of B $i_{2}$ $O_{3}$, the optimal sintering temperature is about 1300.deg. C, but when 4 mol % of B $i_{2}$ $O_{3}$ is added, the optimal sintering temperature falls to the range of 900.deg. C to 1100.deg. C and it also improves magnetic properties. 4. Residual induction increases as the singering temperature is raised to 1100.deg. C. Coercive force also increased as the sintering temperature is raised to 1000.deg. C, but it rapidly decreases when sintering temperature goes beyond 1000.deg. C. 5. Only a negligible change may be noticed in the decrease of Curie temperature by the addition of about 4 mol % of B $i_{2}$ $O_{3}$.

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High-frequency Magnetic Properties of Ni-Zn-Co Ferrites Used for Mangetic Shielding in NFC (NFC의 자기 차폐용 Ni-Zn-Co 페라이트 자성체의 고주파 자기특성)

  • Ryu, Yo-Han;Kim, Sung-Soo
    • Journal of Powder Materials
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    • v.21 no.6
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    • pp.429-433
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    • 2014
  • This study investigated the magnetic properties and frequency dispersion of complex permeability of Ni-Zn-Co ferrites used for magnetic shielding in near field communication (NFC) system. The sintered specimens of $(Ni_{0.7}Zn_{0.3})_{1-x}Co_xFe_2O_4$ composition were prepared by the conventional ceramic processing. The coercive force and saturation magnetization were measured by vibrating sample magnetometer. The complex permeability was measured by RF impedance analyzer in the range of 1 MHz~1.8 GHz. The coercive force increased and saturation magnetization decreased with increasing the Co substitution. The real and imaginary parts of complex permeability decreased and the resonance frequency increased with Co substitution, which was attributed to the increase in crystal anisotropy field and reduction in saturation magnetization. The effect of Co substitution could be found in reducing the magnetic loss to nearly zero at the operating frequency of NFC (13.56 MHz).