• 대한조선학회논문집
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• 제49권5호
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• pp.433-439
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• 2012

Anticorrosive paint is the most widely used in shipbuilding and the dry film thickness is very important in terms of productivity and assurance of anticorrosive performance. However, it is difficult to achieve the recommended target film thickness because the dry film thickness depends on labor's skill in practice and is affected by a number of parameters, such as spray pressure, paint flow rate, tip size, spray distance, SVR(Solid Volume Ratio), etc. Present paper derives an empirical equation through the correlation analysis of parameters selected by spray experiments of anti corrosive painting in order to predict the coated status. Comparing the calculated results with practical data, we show that the empirical equation can successfully expect DFT(Dry Film Thickness).

• 한국표면공학회:학술대회논문집
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• 한국표면공학회 2017년도 춘계학술대회 논문집
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• pp.77-77
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• 2017

Titanium and its alloys offer attractive properties in a variety of applications. These are widely used for the field of biomedical implants because of its good biocompatibility and high corrosion resistance. Titanium anodizing is often used in the metal finishing of products, especially those can be used in the medical devices with dense oxide surface. Based on SAE/AMS (Society of Automotive Engineers/Aerospace Material Specification) 2488D, it has the specification for industrial titanium anodizing that have three different types of titanium anodization as following: Type I is used as a coating for elevated temperature forming; Type II is used as an anti-galling coating without additional lubrication or as a pre-treatment for improving adherence of film lubricants; Type III is used as a treatment to produce a spectrum of surface colours on titanium. In this study, we have focused on Type II anodization for the medical (dental and orthopedic) application, the anodized surface was modified with gray color under alkaline electrolyte. The surface characteristics were analyzed with Focused Ion Beam (FIB), Scanning Electron Microscopy (SEM), surface roughness, Vickers hardness, three point bending test, biocompatibility, and corrosion (potentiodynamic) test. The Ti-6Al-4V alloy was used for specimen, the anodizing procedure was conducted in alkaline solution (NaOH based, pH>13). Applied voltage was range between 20 V to 40 V until the ampere to be zero. As results, the surface characteristics of anodic oxide layer were analyzed with SEM, the dissecting layer was fabricated with FIB method prior to analyze surface. The surface roughness was measured by arithmetic mean deviation of the roughness profile (Ra). The Vickers hardness was obtained with Vickers hardness tester, indentation was repeated for 5 times on each sample, and the three point bending property was verified by yield load values. In order to determine the corrosion resistance for the corrosion rate, the potentiodynamic test was performed for each specimen. The biological safety assessment was analyzed by cytotoxic and pyrogen test. Through FIB feature of anodic surfaces, the thickness of oxide layer was 1.1 um. The surface roughness, Vickers hardness, bending yield, and corrosion resistance of the anodized specimen were shown higher value than those of non-treated specimen. Also we could verify that there was no significant issues from cytotoxicity and pyrogen test.

• 한국산학기술학회논문지
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• 제20권6호
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• pp.272-277
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• 2019

본 논문에서는 옥외용 디스플레이의 눈부심 방지 강화유리 생산 방법을 제안하였다. 일반적으로 옥외용 디스플레이를 위한 커버글라스의 주요 사양은 내강도와 눈부심 방지이다. 내강도는 커버글라스를 고온로에서 열처리한 강화유리를 사용하여 그 요구 사양을 만족시키고 눈부심 방지를 위해서는 AG(Anti-Glare)필름을 강화 유리에 접착하여 주로 사용한다. 그러나 필름 형태의 눈부심 방지기술은 PET 필름자체의 내마모성이 3H정도로 취약하여 AG 성능이 지속적으로 유지되기 어렵다. 따라서 본 논문에서는 AG 필름이 가지는 내구성의 단점을 보완하고 기존 강화유리 생산 공정을 이용하는 눈부심 방지 기술을 제안하였다. 제안된 눈부심 방지 코팅은 ZBS ($ZnO-B_2O_3-SiO_2$) 분말을 유리 표면에 도포하고 강화공정을 수행하여 내구 강도와 눈부심 방지 성능을 높일 수 있도록 하였다. ZBS 분말을 유리 표면에 도포하기 위해서는 스크린 프린팅 공정을 이용하여 분말이 유리표면에 균일하게 도포되도록 하였다. 스크린 프린팅 시 고려되어야 하는 주요 변수는 분말을 희석하기 위한 오일의 농도와 메쉬 오프닝 사이즈이다. 이 두 변수의 설정에 따라 스크린 프린팅 공정에서 도포되는 ZBS 분말의 양이 조절되므로 이에 대한 상관관계를 실험을 통해 규명하였다. 제안된 제조 방법의 성능을 평가하기 위해 상업용 시장에서 널리 사용되는 haze, 표면 거칠기 및 투과도를 성능 지표로 선정하였고 눈부심 방지를 위해 일반적으로 사용되는 AG필름과 비교하여 그 성능을 검증하였다. 비교 결과 제안된 제조 방법에 의한 강화유리의 투과도는 AG필름의 89.5%보다 다소 감소한 83.1%이지만 막강도는 7H로 두배 이상 향상됨을 확인하였다.