• Title/Summary/Keyword: Coating film

Search Result 1,908, Processing Time 0.037 seconds

Synthesis of ITO Nano-Particles by a SAS Method and Preparation of Conductive Film by Coating Them (SAS법을 이용한 ITO 나노입자의 합성과 ITO 도포에 의한 도전필름의 제조)

  • Kim, Moon-Sun;Yun, Sang-Ho;Kim, Byung-Woo
    • Clean Technology
    • /
    • v.13 no.3
    • /
    • pp.180-187
    • /
    • 2007
  • The indium tin oxide(ITO) film on PET was prepared by a wet coating method to obtain the transparent film with a high conductance. ITO nano-particles was synthesized by a SAS method at 15 MPa and $50^{\circ}C$, where optimized rate of In/Sn was 65. Average diameter and resistivity of ITO obtained from SAS are $15{\pm}2\;nm$ and $4{\times}10^4\;{\Omega}{\cdot}cm$. Coating solution was prepared at pH 10. The ITO film was obtained by solution including 0.1 0.5, 1, and 2 ITO wt% on PET. Roughness(Ra) of ITO film with 0.1, 0.5, 1. and 2 ITO wt% is 4, 10, 12, and 16 nm. Resistivity with an increasing ITO concentration is $3.7{\times}10^6,\;2.4{\times}10^6,\;8{\times}10^5,\;and\;2{\times}10^5\;{\Omega}{\cdot}cm$. Transmissivity of ITO film decreased as 89, 88, 86, and 82% with an increasing ITO concentration as 0.1, 0.5, 1, and 2 wt%.

  • PDF

Lubrication of Space Systems by Tribo-coating

  • Kato, Koji
    • Proceedings of the Korean Society of Tribologists and Lubrication Engineers Conference
    • /
    • 2002.10b
    • /
    • pp.7-8
    • /
    • 2002
  • It is a time to introduce a concept of lubrication to space systems. Minimum amount of lubricant should be supplied to a contact interface instead of preparing too much lubricant on surfaces of the earth. In situ controllable lubrication method is wanted to overcome unexpected tribo-troubles in space. Tribo-coating, which forms a thin solid film in nm-scale by vacuum deposition during friction, is a promising lubrication method for space.

  • PDF

Simple Algorithm of Structure Features Extration for Stereo Image Matching (스테레오 영상 정합을 위한 새로운 구조 정보 추출 알고리즘)

  • 최환언
    • Journal of the Korean Graphic Arts Communication Society
    • /
    • v.9 no.1
    • /
    • pp.1-11
    • /
    • 1991
  • In this reseach, double-layered photoconductor consist of the carrier generation layer(CGL) of $\varepsilon$ type copper phthalocyanine thin film by an aqueous coating method and the carrier transport layer(CGL) of polyvinyl carbazol(PVK) by spin coating. We inverstigated effect of the surfactant solution and cathod electrolysis to the crystal type of $\varepsilon$-CuPc in CGL with TEM, SEM and X- ray diffraction spectroscopy and studied the mechanism of an aqueous coating for the preparation of CGL. The effect of the washing of CGL about the electrophotographic characteristics of the $\varepsilon$-CuPc/PVK doublelayered photoconductors is studied also.

  • PDF

Surface Coating and Corrosion Characteristics of Bipolar Plates of PEMFC Application (PEMFC용 분리판 표면코팅 및 부식성 평가)

  • Kang, Kyung-Min;Kim, Dong-Mook;Choi, Jeong-Sik;Cha, In-Soo;Yun, Young-Hoon
    • Transactions of the Korean hydrogen and new energy society
    • /
    • v.22 no.2
    • /
    • pp.199-205
    • /
    • 2011
  • Stainless steel 304 and 316 plates were deposited with the multi-layered coatings of titanium film (0.1 um) and gold film (1-2 um) by an electron beam evaporation method. The XRD patterns of the stainless steel plates modified with the multi-layered coatings showed the crystalline phases of the external gold film and the stainless steel substrate. Surface microstructural morphologies of the stainless steel bipolar plates modified with multi-layered coatings were observed by AFM and FE-SEM images. The external gold films formed on the stainless steel plates showed micro structure of grains of about 100 nm diameter. The grain size of the external surface of the stainless steel plates increased with the gold film thickness. The electrical resistance and water contact angle of the stainless steel bipolar plates covered with multi-layered coatings were examined with the thickness of the external gold film.

Preparation of Ferroelectric PZT Thin Film by Sol-Gel Processing; (I) Synthesis of Stable PZT Sol Using Chelating Agent and Preparation of Its Thin Film (졸-겔법에 의한 강유전성 PZT 박막의 제조;(I) 킬레이팅 에이전트를 이용한 안정화 PZT 졸의 합성 및 박막의 제조)

  • Kim, Byong-Ho;Hong, Kwon;Cho, Hong-Yeon
    • Journal of the Korean Ceramic Society
    • /
    • v.31 no.7
    • /
    • pp.804-812
    • /
    • 1994
  • Stable PZT coating sol was prepared using chelating agent, ethylacetoacetate(EAcAc) by sol-gel processing under ambient atmosphere. Through FT-IR spectrum analysis on solution of each reaction step, formation of metal complex was confirmed and prepared PZT sol was stable over several months. Through TG-DTA, XRD, FT-IR spetrum analysis of PZT gel powder, it was understood that the addition of EAcAc could reduce the transition temperature to ferroelectric phase, due to the increased homogeneity by matching the hydrolysis and condensation rates by chelation. Single perovskite phase was obtained by the heat-treatment at 54$0^{\circ}C$ for 30 min. The film was coated on ITO-coated glass substrate by dip coating method. After heat-treatment, PZT thin film had thickness in the range of 20~130 nm. The maximum dielectric constant of its thin film at room temperature and 1 kHz was 128.

  • PDF

Lubricating Properties on Tribo-Coating of Soft Metals in Ultra High Vacuum (초고진공중에서 연질금속의 Tribo-Coating에 관한 윤활특성)

  • 김형자;전태옥;가등건가
    • Tribology and Lubricants
    • /
    • v.10 no.3
    • /
    • pp.18-28
    • /
    • 1994
  • Sliding friction between a spherical pin of 8mm in diameter and flat (disk) substrates coated with vacuum-deposited thin film was measured under ultra high vacuum pressure for various materials, various rates of film supply (8~210 nm/min), various sliding velocities (1.5~67.0 mm/s). It was found that the most effective lubrication was obtained when the adhesion between $Si_3N_4$ pin and SUS440C disk was high and that between $Si_3N_4$ pin and $Si_3N_4$ disk was low. When In film was used as a lubricant between $Si_3N_4$ pin and stainless steel disk, the friction coefficient had a value as low as 0.04. In this case, the normal load W and the sliding speed V were expressed as 10N and 24 mm/s for $10^{-6}Pa$. The dependence of $\mu$ on the thickness h of the Ag film, which was used as a lubricant between $Si_3N_4$ pin and SUS440C (Q) disk was expressed as $\mu$=0.12 for W=10N and V=24mm/s when the film was thicker than 100nm. A brief discussion on these relations is presented from the viewpoint of the real contact area.

Structural and discharge characteristics of MgO films prepared by Arc Ion Plating (AIP) method

  • Kim, Jong-Kuk;Kim, Do-Geun;Lee, Eun-Sung;Lee, Sung-Hun;Lee, Gun-Hwan
    • 한국정보디스플레이학회:학술대회논문집
    • /
    • 2002.08a
    • /
    • pp.625-627
    • /
    • 2002
  • MgO thin films were deposited on glass and (100) Si substrates by an Arc Ion Plating (AIP) equipment using a magnesium metal target at various oxygen gas flow. In this work, we investigated the relationship between the structural properties and the discharge characteristics of MgO coating layers. X-ray diffraction and AFM have been used to study behaviors of the structure and surface morphology. The optical transmittance and the ion induced secondary electron emission coefficient of the MgO films have been also measured. The resistivity of the deposited MgO films was gradually increased from 0.17 G ohm/${\square}$ to 0.35 G ohm/${\square}$ with the oxygen gas flow. The growth rate of the MgO coating layer was decreased with increasing the oxygen gas flow, while the optical transmittance was improved.

  • PDF

Super Hydrophilic Properties of ZrO2 Thin Film Containing TiO2 Photo-Catalysis (광촉매 TiO2 함유 ZrO2 박막의 초친수성)

  • Jung, Ki-Uk;Lee, Tea-Gu;Mun, Chong-Soo
    • Korean Journal of Materials Research
    • /
    • v.18 no.4
    • /
    • pp.211-217
    • /
    • 2008
  • A $ZrO_2$ coating solution containing $ZrO_2$ photo-catalysis, which is transparent in visible light, was prepared by the hydrolysis of alkoxide, and thin films on the $SiO_2$ glass substrate were formed in a dipcoating method. These thin films were heat-treated at temperatures ranging from $250^{\circ}C-800^{\circ}C$ and their characteristics were subjected to thermal analysis, XRD, spectrometry, SEM, EDS, contact angle measurement, and AFM. Tetragonal $ZrO_2$ phase was found in the thin film heat treated at $450^{\circ}C$, and anatase $TiO_2$ phase was detected in the thin film heat-treated at $600^{\circ}C$ and above. The thickness of the films was approximately 300 nm, and the roughness was 0.66 nm. Thus, the film properties are excellent. The films are super hydrophilic with a contact angle of $4.0^{\circ}$; moreover, they have self-cleaning effect due to the photo catalytic property of anatase $TiO_2$.

Characterization of Electro-Polymerized Polyaniline Film on the Cold Rolled Sheet in the Oxalic acid and Sodium Molybdate Electrolyte (옥살산과 몰리브덴산나트륨 전해액에서 냉연강판에 전해중합된 폴리아닐린 피막의 특성)

  • Lim, Ki-Young;Yoon, Jeong-Mo;Ki, Joon-Seo;Jang, Yong-Seok
    • Korean Journal of Materials Research
    • /
    • v.16 no.6
    • /
    • pp.386-393
    • /
    • 2006
  • Increasing environmental concerns require to solve the problem produced due to the use of heavy metals in coating formulations. Therefore, it is necessary to develop new coating strategy employing inherently conducting polymers such as polyaniline. Polyaniline is a conductive polymer that is synthesized by oxidation polymerization, and the electrochemical and chemical polymerization are possible for the oxidation of aniline. Electrochemical oxidation polymerization produces a fine surface and although voltage control is more convenient, it require electrolytic cells, and elaborate thin film can be acquired with the polymerization. Polyaniline films were electro-polymerized on cold rolled sheets using the galvanostat mode in the oxalic acidaniline-sodium molybdate electrolyte. The structure and properties of polyaniline film were studied using Potentiostat/Galvanostat 263A, FE-SEM,, AFM, SST, Colorimetry. A high corrosion resistance of polyaniline film was observed with an increase of corrosion potential by $500{\sim}600$ mV for the substrate covered with polyaniline.

Study of Multi Anti-Reflection Coating Thin Film of Ferrule Facet Manufacture and Characteristics (광커넥터 패룰 단면의 다층 무반사 코팅 박막 제작 및 특성에 관한 연구)

  • Ki, Hyun-Chul;Yang, Mung-Hark;Kim, Sun-Hoon;Kim, Sang-Taek;Park, Kyung-Hee;Hong, Kyung-Jin
    • Proceedings of the Korean Institute of Electrical and Electronic Material Engineers Conference
    • /
    • 2007.06a
    • /
    • pp.408-409
    • /
    • 2007
  • Ferrule function have connect Optical Communication Cable. But Ferrule have important role that is decided transmission efficiency and information quality. Key-point of detailed drawing of ferrule is Anti-Reflection. In the study Broadband Anti-Reflection coating Film was design for ferrule of optical connector and deposited in low temperature by Ion-Assisted Deposition system. Optical thin film materials($Ta_2O_5$, $SiO_2$) were manufactured Index and Film thickness. $Ta_2O_5$ index is 2.123 ~ 2.125 and $SiO_2$ is 1.44 ~ 1.442. Reflection Loss of film deposited on Ferrule is 30.1[dB].

  • PDF