• 제목/요약/키워드: Coarsening

검색결과 268건 처리시간 0.031초

Al-Li-Cu-Mg-Zr 합금에 있어서 δ'상 조대화를 위한 Lithium의 확산계수 평가 (The Evaluation of Diffusivity of Lithium for Coarsening of δ' Precipitate in AI-Li-Cu-Mg-Zr Alloy)

  • 정동석;김은호;조현기
    • 열처리공학회지
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    • 제7권1호
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    • pp.17-24
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    • 1994
  • The evaluation and analysis of diffusivity of lithium for coarsening and coarsening kinetics of ${\delta}^{\prime}$ precipitate in Al-Li-Cu-Mg-Zr alloy aged at $170^{\circ}C$ have been investigated by transmission electron microscopy. With ageing time, ${\delta}^{\prime}$ precipitate coaesened to followed $\bar{\gamma}{\propto}t^{1/3}$ and coarsening kinetics was found to be obeyed to the Lifshitz-Slyozov-Wagner(LSW) theory and diffusivity of lithium for coarsening of ${\delta}^{\prime}$ precipitate in Al-Li-Cu-Mg-Zr alloy was obtained to be $5.85{\times}10^{-17}{\sim}1.53{\times}10^{-16}$ by experimental coarsening rate constant and various coarsening kinetic theory. Diffusivity of lithium measured by using various model but MLSW and Tsumuraya (VI) et al. model in Al-Li-Cu-Mg-Zr alloy is similar to that calculated by the Costas's diffusivity equation. It was, therefore, suggested that additing to the Cu, Mg and Zr element in Al-Li system have no great effect on diiffusivity of lithium for coarsening of ${\delta}^{\prime}$ This suggest that in matrix.

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3.5Ni-Cr-Mo-V 강의 크리프 수명예측에 재질열화 및 오스테나이트 결정립 조대화가 미치는 영향 (Effect of Material Degradation and Austenite Grain Coarsening on the Creep life Prediction in 3.5 Ni-Cr-Mo-V Steel)

  • 홍성호;조현춘
    • 대한기계학회논문집
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    • 제18권11호
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    • pp.2837-2845
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    • 1994
  • Several methods have been developed to predict on the remaining life of the old power plants. However, Larson-Miller parameter, one of existing creep life prediction methods, has not reflected the effect of material degradatioin and grain size. So this study has been carried out to research the effects of material degradation and austenite grain coarsening on the life prediction of 3.5Ni-Cr-Mo-V steel. An experimental result shows that carbide coarsening has no significant effects on the creep rupture life and the Larson-Miller parameter, but grain coarsening has an important influence on the creep ruptrure life and the Larson-Miller parameter. Therefore Larson-Miller constant, K should be determined to consider on the chemical composition and the grain size of materials.

기계적 합금화된 ODS NiAl에서 분산상 및 기지상의 조대화 거동 (Coarsening of Dispersoid and Matrix Phase in Mechanically Alloyed ODS NiAl)

  • 어순철
    • 한국분말재료학회지
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    • 제4권1호
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    • pp.48-54
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    • 1997
  • NiAl powders containing oxide dispersoids have been produced by mechanical alloying process in a controlled atmosphere using high energy attrition mill. The powders have been consolidated by hot extrusion and hot pressing followed by isothermal annealing to induce microstructure coarsening to improve high temperature properties. Grain growth and dispersoid coarsening kinetics have been investigated as functions of annealing time and temperature. Coarsening of dispersion strengthen NiAl and dispersoid has been discussed. Some clues of secondary recrystallization have been investigated. Mechanical property measurements have been also made and correlated with the microstructures.

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고분자 용액에서의 Coarsening 현상 (Coarsening Phenomena in Polymer-Solvent Systems-A Review)

  • 송승원
    • 멤브레인
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    • 제7권2호
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    • pp.49-56
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    • 1997
  • In order to understand the formation of polymeric membranes or microcellular foams, phase separation phenomena in polymer solutions should be understood. The present review examines the progress made in the understanding of these phenomena, with emphasis on selected polymer-solvent systems. In the case of polymer-solvent systems, coarsening is of particular importance as it may come to dominate or overshadow spinodal decomposition effects within the first minute or few minutes of phase separation. In this article, some of the most important theoretical models of late stage of phase separation are reviewed, and recent experimental studies on coarsening in polymer-solvent systems are studied.

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Coarsening Effects on the Formation of Microporous Membranes

  • Song, Seung-Won
    • 한국막학회:학술대회논문집
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    • 한국막학회 1995년도 춘계 총회 및 학술발표회
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    • pp.1-4
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    • 1995
  • The microstructure of polymer membranes produced via thermally induced phase separation (TIPS) of polymer solutions is a strong function of both the early-stage (by spinodal decomposition or nucleation & growth) and the late-stage phase separation (referred to in general as coarsening). In the case of early stage effects, the membrane morphology resulting from a nucleation & growth mechanism is either a poorly interconnecsed, stringy, beady structure which is mechanically fragile or a well interconnected structure with highly nonuniform pore sizes. In contrast, spinodal decomposition results in a well interconnected, mechanically strong membrane with highly uniform pore sizes. Here I describe recent quantitative studies of the coarsening effects on the microstructure of membranes produced via TIPS process. The dependence of microstructure on coarsening time, quench depth, solution viscosity, and polymer molecular weight was investigated in order to distinguish among three possible coarsening mechanisms, Ostwald ripening, coalescence, and hydrodynamic flow, which may be responsible for structural evolution after the early-stage phase Separation (spinodal decomposition or nucleation & growth).

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항공기용 Al 합금 단조품의 특성 향상을 위한 단조 공정 설계 (Forging Process Design to Improve the Properties of Al Alloy Forged Part for Aerospace)

  • 이영선;이정환
    • 한국소성가공학회:학술대회논문집
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    • 한국소성가공학회 2001년도 추계학술대회 논문집
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    • pp.228-232
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    • 2001
  • Fatigue strength, electrical conductivity and stress-corrosion-cracking resistance are considered as important factors at aircraft Al alloys, therefore Al7050 alloy has been developed to improve such properties. However, hammer-forged Al7050 parts showed the undesirable structures such as severe local grain coarsening and inhomogeneous material flow, resulted in the degraded mechanical properties. In this paper, process conditions are investigated for elimination of the grain coarsening and improved material flow during forging process by both of experiments and FEM analysis. Particular interest has been given to understand role of preform shape on the grain coarsening behavior and magnitude of the hammer forging load The use of preform has been beneficial for reduction of the forging load and elimination of the grain coarsening. However, in the cases of as received bar and the round bar, which was machined to 2.5mm thickness in surface layer, some degree of local grain coarsening behavior has been observed. The optimized preform shape could be properly designed by applying the FEM simulation.

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용접 열영향부 미세조직 및 재질 예측 모델링: IV. Ti-첨가 저합금강에서의 임계 석출물 크기의 영향을 고려한 용접 열영향부 석출물 조대화 예측 모델 (Prediction Model for the Microstructure and Properties in Weld Heat Affected Zone : IV. Critical Particle Size for the Particle Coarsening Kinetics in Weld HAZ of Ti Added Low Alloyed Seel)

  • 문준오;김상훈;정홍철;이종봉;이창희
    • Journal of Welding and Joining
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    • 제25권2호
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    • pp.62-69
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    • 2007
  • A kinetic model fur the particle coarsening behavior was developed. The proposed model considered the critical particle size which can be derived from Gibbs-Thomson equation unlike the conventional approach. In this study, the proposed particle coarsening model was applied to study the coarsening behavior of titanium nitride (TiN particle) in microalloyed steel weld HAZ. Particle size distributions and mean particle size by the proposed model were in agreement with the experimental results. Meanwhile, using additivity rule, the isothermal model was extended to predict particle coarsening behavior during continuous thermal cycle.

Modeling of Pore Coarsening in the Rim Region of High Burn-up UO2 Fuel

  • Xiao, Hongxing;Long, Chongsheng
    • Nuclear Engineering and Technology
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    • 제48권4호
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    • pp.1002-1008
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    • 2016
  • An understanding of the coarsening process of the large fission gas pores in the high burn-up structure (HBS) of irradiated $UO_2$ fuel is very necessary for analyzing the safety and reliability of fuel rods in a reactor. A numerical model for the description of pore coarsening in the HBS based on the Ostwald ripening mechanism, which has successfully explained the coarsening process of precipitates in solids is developed. In this model, the fission gas atoms are treated as the special precipitates in the irradiated $UO_2$ fuel matrix. The calculated results indicate that the significant pore coarsening and mean pore density decrease in the HBS occur upon surpassing a local burn-up of 100 GWd/tM. The capability of this model is successfully validated against irradiation experiments of $UO_2$ fuel, in which the average pore radius, pore density, and porosity are directly measured as functions of local burn-up. Comparisons with experimental data show that, when the local burn-up exceeds 100 GWd/tM, the calculated results agree well with the measured data.

Nb의 첨가에 따른 Ti 첨가 저합금강 용접열영향부에서의 석출물 거동 변화 (Precipitation and Precipitate Coarsening Behavior According to Nb Addition in the Weld HAZ of a Ti-containing Steel)

  • 문준오;이창희
    • Journal of Welding and Joining
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    • 제26권1호
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    • pp.76-82
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    • 2008
  • The effect of Nb addition on the precipitation and precipitate coarsening behavior was investigated in Ti and Ti + Nb steel weld HAZ. A dilatometer equipped with a He-quenching system was used to simulate the weld thermal cycle. Compared to $TiC_yN_{1-y}$ precipitate in a Ti containing steel, $Ti_xNb_{1-x}C_yN_{1-y}$ complex particle with addition of Nb is precipitated in a Ti + Nb containing steel. Meanwhile, precipitate coarsening occurred more easily in Ti + Nb steel, which may be because the high temperature stability of $Ti_xNb_{1-x}C_yN_{1-y}$ complex particle is deteriorated by the Nb addition.

Coarsening Advantage of Twinned BaTiO3 Seed Particle

  • Jin, Hong-Ri;Jo, Wook;Hwang, Nong-Moon;Kim, Doh-Yeon
    • 한국세라믹학회지
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    • 제42권9호
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    • pp.599-601
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    • 2005
  • The coarsening process of two different $BaTiO_3$ single crystal seeds, one with a (111) double twin and the other without it, was investigated. Due to the presence of Twin Plane Reentrant Edge (TPRE), the coarsening rate of the twinned seed crystal was significantly higher than that without a twin. For the coarsening by the 2-dimensional nucleation and lateral growth, the energy barrier for nucleation at the TPRE was analyzed to be about a half compared with that at the terrace planes.