• Proceedings of KOSOMES biannual meeting
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• 2017.04a
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• pp.207-207
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• 2017

• YAKHAK HOEJI
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• v.37 no.1
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• pp.76-83
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• 1993

The changes in discharge current, emission and/or oscillation frequency of the electric oscillation of a glow discharge are the potential sensitive measure of the concentration of an impurity in the argon plasma supporting gas. A single jet enhanced glow discharge has been interfaced with the gas chromatograph via 1/8" O.D. tube with a heating pad to study the changes in discharge current. To investigate the optimum operating conditions of the glow discharge system as detector for gas chromatography, pressure, gas flow rate, discharge current, distance between the anode and the cathode have been studied.

• Bulletin of the Korean Chemical Society
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• v.14 no.1
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• pp.127-131
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• 1993

Laser optoacoustic technique has been employed to obtain the gas phase absorption spectra of 1-chloronaphthalene, 3-chlorobiphenyl, and 2,5,2'-trichlorobiphenyl in conjunction with a gas chromatograph and a Helmholtz resonator at the various $CO_2$ laser wavelengths. Raman spectra of 1-chloronaphthalene, 4-chlorobiphenyl, and 4,4'-dichlorobiphenyl in condensed phase have been also obtained. The optoacoustic measurement of the infrared absorption in gas phase has been shown to be of value in monitoring the environmental pollutants.

• The Journal of Internal Korean Medicine
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• v.35 no.4
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• pp.532-545
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• 2014

Objectives: The purpose of this study was to evaluate the clinical effect of Korean medical treatments such as herbal medicine, acupuncture, and electroacupuncture by using the portable gas chromatograph OralChroma$^{TM}$ (Abimedical, Japan) in halitosis patients. Methods: We surveyed 30 halitosis patients who had visited the Oral Diseases Clinic in the Korean Medical Hospital of Kyunghee University from October, 2013 to November, 2014. Before starting Korean medical treatment, the subjects were evaluated on sociodemographic characteristics, severity of discomfort using visual analogue scale (VAS), unstimulated salivary flow rate (USFR), and halitosis associated life-quality test (HALT) score. To evaluate the therapeutic effect, we measured the volatile sulfur compounds (VSCs) in breath by using OralChroma$^{TM}$ before and after 3 weeks treatment. Results: The concentration of total VSCs measured by OralChroma$^{TM}$ significantly decreased (p=0.001). Furthermore, the level of hydrogen sulfide and methyl mercaptan also significantly decreased (p<0.05). However, although the level of dimethyl sulfide decreased as well, there was no significance(p>0.05). Conclusions: Korean medical treatment was effective in treating halitosis by decreasing VSCs. Further study, with well-designed randomized controlled trials with larger number of cases will be needed in the future.

• Applied Biological Chemistry
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• v.15 no.1
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• pp.7-17
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• 1972

Samples of 13 vegetables were collected, between 14 July and 6 August, 1971, from 15 markets located in 12 different cities and analyzed for Heptachlor residues by gas liquid chromatograph. The residue concentrations of Heptachlor and its epoxide were estimated separately, at a sensitivity level of 0.001 p.p.m., to produce Heptachlor residues on the fresh weight basis. The Heptachlor residues in or on the crops analyzed, including three staple vegetables, potatoe, radish and chinese cabbage, were found fairly low and are far lower than the residue tolerences for respective vegetables recommended jointly by FAO and WHO of the United Nations.

• Applied Chemistry for Engineering
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• v.10 no.1
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• pp.30-34
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• 1999

Photolysis behavoirs of pesticides(Chlorothalonil and Endosulfan) over UV irradiation UV irradiation with pH 3.0 and irradiation with 3.5% salt were studied. The analyses of pesticides were carried out using gas chromatograph with an electron-capture detector, total organic carbon, and Ion chromatograph, respectively. The reactions were conducted in a alumium annular reactor equipped with a low pressure mercury multilamp ($8W{\times}6$) and initial concentration was 10 ppm. Chlorothalonil was almost photodegraded by UV irradiation, UV irradiation with pH 3.0 and 3.5% salt within 30 min of reaction time. Endosulfan-${\alpha}$,${\beta}$(100%) were photodegraded to 38% of Endosulfan-${\alpha}$ and 25% of Endisulfan-${\beta}$ by UV irradiation. Endosulfan-${\alpha}$(83%) was photodegraded to 66% by UV irradiation, 70% by UV irradiation and pH 3.0 and 75% by UV irradiation and 3.5% salt. Endosulfan-${\beta}$(16%) was photodegraded to 80% by UV irradiation, 98% by UV irradiation and pH 3.0 and 90% by UV irradiation and 3.5% salt.

• Fire Science and Engineering
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• v.28 no.4
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• pp.64-72
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• 2014

Flammable liquids residues in fire debris and pyrolysis products of flammable materials were analyzed by using Gas detecting tube, Gas Chromatograph/Mass Spectrometers (GC/MS), and Pyrolyzer. Comparison studies between chemical components detected in debris fired with and without Flammable liquids were performed. Though Flammable liquids were not present in debris, Gas detecting tube colors were also changed. Chemical components produced from conventional combustions were different from those produced from pyrolysis. Due to the difference of the reaction conditions between combustions and pyrolysis, different chemical products were produced. Petrochemical products of PVC wood-linoleum block could produce ignitable chemicals, such as toluene, ethylbenzene, undecane, and dodecane. So, for better fire investigation more consideration of those chemicals will be porformed.

• Korean Journal of Food Science and Technology
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• v.25 no.2
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• pp.136-141
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• 1993

A curd yogurt was prepared from milk added with skim milk powder or four kinds of cereal. The effect of cereals at 2%(w/v) level on the pattern of volatile aroma compounds in curd yogurt was investigated. Acetaldehyde, acetone, ethanol, diacetyl, butanol and acetoin in curd yogurt were detected by gas chromatographic analysis. Among these compounds, acetaldehyde, ethanol, diacetyl and acetoin were produced during fermentation by Lactobacillus acidophilus (KCTC 2182). The addition of cereals did not affect markedly general pattern of volatile aroma compounds in curd yogurt. The amount of acetoin and ethanol markedly increased until the first 6 hours of fermentation, and then increased mildly until 24 hours. The amount of diacetyl markedly increased until the first 6 hours and then decreased slightly. Acetaldehyde was first detected by gas chromatograph after 18 hours of fermentation.

• Journal of Korean Society for Atmospheric Environment
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• v.18 no.1
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• pp.39-49
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• 2002

In this study, limits of detection (LOD), accuracy and precision of four sampling/ analytical methods were evaluated and compared for the determination of airborne hexavalent chromium, Cr (VI). The methods include : (1) a combination of the National Institute for Occupational Safety and Health (NIOSH) Method 7600/U. S. Environmental Protection Agency (EPA) Method 218.6 (NIOSH/EPA Method) proposed by Shin and Paik, 2) two impinger methods using 2% NaOH/3% Na$_2$CO$_3$. (3) same as (2) but with 0.02 N NaHCO$_3$absorbing solution, and (4) the Occupational Safety and Health (OSHA) Method ID-215. An ion chromatograph/visible absorbance detector was used for the analysis of Cr (VI) in sample solution. Limit of detection (LOD) , analytical accuracy, and precision were also tested using Cr (VI) spike samples. Recoveries (as index of accuracy) and coefficient of variation (CV) (as a index of precision) were determined. Two-way ANOVA and Turkey's test were performed to test the significance in differences among recoveries and CVs of the methods. In all the methods, the peaks of Cr (VI) were separated sharply on chromatograms and exhibited a strong linearity with Cr (VI) concentrations in solution. The correlation coefficients of calibration curves typically ranged from 0.9997 to 0.9999, and the analytical LODs from 0.025 to 0.1$\mu\textrm{g}$/sample. All the method had good sensitivities and linearities between Cr (VI) levels and peak areas. The accuracies (% mean recoveries) of the methods ranged from 80.1 to 104.2%, while the precisions (pooled coefficient of variation) ranged from 3.16 to 4.43%. The impinger methods showed higher recoveries ( > 95%) than those of the PVC filter methods (the OSHA Method and the NIOSH/EPA Method). It was assumed that Cr (VI) on PVC filter was exposed to air and reduced to trivalent chromium, Cr (III), whereas it was stabilized in alkali solution contained in impinger. Thus, a special treatment of Cr (VI) samples collected on PVC filters may be required.

• Korean journal of applied entomology
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• v.42 no.1
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• pp.9-13
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• 2003

Cuticular hydrocarbons of antenna, legs and wings from two species of honeybee worker of Apis mellifera L. and Apis cerana F. can be analyzed directly with gas chromatograph and GC/MS without solvent extraction. The saturated hydrocarbons identified in selected part of both species were nC22, nC23, nC25-nC3O, nC32 and nC34 except nC24. Two saturated hydrocarbons, nC26 (23.0-42.6%) and nC28 (16.8-54.8%), were major compounds in both species and others were minor compounds. A. mellifera can be distinguished from A. cerana F. by having higher proportion of nC30, nC32 and nC34 by having lower proportion of nC25 from three selected part of both species.