• Title/Summary/Keyword: Chemical drying

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Changes in Chemical Components and Physical Properties with Freeze Drying and Hot Air-Drying of Dioscorea batatas (동결건조 및 열풍건조 방법에 따른 마의 성분과 물리적 성질 변화)

  • 권중호;이기동;이수정;정신교;최종욱
    • Journal of the Korean Society of Food Science and Nutrition
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    • v.27 no.5
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    • pp.908-913
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    • 1998
  • Chemical components and some physical proeprties of fresh, defrosted and dried yams(Dioscoreab batatas) were determined to obtain basic data for high quality yam processing. Fresh yam showed 81.79% moisture and 15.24% N-free extract. The cohesiveness and adhesiveness of defrosted yam homogenate were significantly higher than those of fresh yam homogenate. Free sugars of yam were mainly composed of sucrose, rhamnose, fructose and glucose, and the contents of fructose and glucose were apparently decreased by hot air drying. Linoleic(45.64%), oleic(8.32%), and arachidic acids(7.40%) were major fatty acids of yam. Hot air drying caused a decrease in unsaturated fatty acids and an increase in saturated acids. Hot air-dried yam powder showed higher gelatinization properties than freeze-dryed yam powder, such asinitial pasting temperature, temperature at maximum viscosity, and viscosity at different parameters. Hot air-dried yam powder showed higher Hunter parameter b and ΔE values and lower L value than freeze-dried one.

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Changes of HwBKP, SwBKP, OCC Handsheets' Drying Behavior and Physical Properties by Refining, Kneading and Wet Pressing (고해, 니딩, 습부압착에 의한 HwBKP, SwBKP, OCC 수초지의 건조 거동 및 물성 변화)

  • Lee, Jin-Ho;Park, Jong-Moon
    • Journal of Korea Technical Association of The Pulp and Paper Industry
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    • v.43 no.5
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    • pp.17-26
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    • 2011
  • Drying behavior and physical properties of HwBKP, SwBKP, and OCC handsheets depending on kneading, refining and wet pressing were analyzed. The maximum drying shrinkage velocity was newly adopted to verify the effect of mechanical treatment of pulps by evaluating drying behavior according to varying the kneading, refining and wet pressing treatments. Those various treatments were changed to evaluate the relationship between the maximum drying shrinkage velocity and handsheets properties. When the drying shrinkage and the maximum drying velocity increased by refining and wet-pressing, handsheets strength was increased. The maximum drying shrinkage velocity showed higher correlation with physical properties of paper than WRV at different refining loads at SwBKP and mixed pulp. At high wet-web dryness, drying shrinkage, the maximum drying shrinkage velocity and strength properties of handsheet were increased. It meant that drying shrinkage behavior was highly affected by not only fibers' shrinkage but also fiber bonding. Kneading pre-treatment for KOCC and SwBKP effectively modified fiber properties and increasing paper strength and drying shrinkage. The effect of kneading pre-treatment was also confirmed by the maximum drying shrinkage velocity. Strength properties of mixed pulp handsheets were not increased by the kneading pre-treatment, although the maximum drying shrinkage velocity and WRV was increased. It meant that fibers network bonding of HwBKP was limited because of ves sels and ray cells' interference for bonding. Therefore in order to improve paper strengths containing HwBKP by mechanical treatments, interference of vessels and ray cells for fiber bondings should be carefully controlled.

Improvement of Paper Bulk and Stiffness by Using Drying Shrinkage Analysis (건조수축 해석을 통한 종이의 벌크 및 강직성 향상)

  • Lee, Jin-Ho;Park, Jong-Moon
    • Journal of Korea Technical Association of The Pulp and Paper Industry
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    • v.43 no.4
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    • pp.49-58
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    • 2011
  • The maximum drying shrinkage velocity was proposed to verify bulk and stiffness improvement mechanism during drying according to papermaking parameters. It was based on the wet-web shrinkage behavior without the restraint of wet-web during drying, so intact drying impact could be measured. Bulking agent reduced the drying shrinkage and the maximum drying shrinkage velocity, so paper bulk increased and paper strength decreased. When adding cationic starch to stock with the bulking agent for strengthening, the bulk was increased further with additional decreasing of the drying shrinkage and the maximum drying shrinkage velocity. Paper strength also increased except tensile stiffness index with decreasing the drying shrinkage and the maximum drying shrinkage velocity. When using additional strength additives for strengthening of fiber interfaces extended by bulking agent and cationic starch, amphoteric strength additive increased paper stiffness without loss of paper bulk. It was considered that the added amphoteric strength additives were cross-linked to the stretched cationic starch and this cross-linking increased elasticity of fiber-polymer-fiber interfaces without changing the drying behavior. Paper bulk could be increased with decreasing the maximum drying shrinkage velocity. The drying shrinkage of paper also could be controlled by fiber-to-fiber bonding interfaces by the bulking agent. In this case, paper strength including stiffness was decreased by reducing fiber-to-fiber bonding but it could be improved by strengthening fiber-to-fiber interfaces with polymer complex without loss of bulk.

Ethanol-pretreated Drying of (+)-dihydromyricetin for Removal of Residual Solvents (잔류 용매 제거를 위한 (+)-dihydromyricetin의 에탄올 전처리 건조)

  • Lee, Hee-Gun;Kim, Jin-Hyun
    • Korean Chemical Engineering Research
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    • v.60 no.2
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    • pp.237-242
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    • 2022
  • In this study, a drying method that can effectively remove residual solvent from (+)-dihydromyricetin was developed. Residual acetone concentration was efficiently removed below ICH-specified value (5,000 ppm) by simple rotary evaporation with ethanol pretreatment. In addition, the residual ethanol met the ICH-specified value (5,000 ppm) by simple rotary evaporation through the addition of water, and the residual moisture also met the specified value (<4%) for active pharmaceutical ingredients. At all the drying temperature (35, 45, and 55 ℃), a large amount of the residual solvent was initially removed during the drying, and the drying efficiency increased when increasing the drying temperature. Removal of residual solvent by ethanol pretreatment was shown to be related to high vapor pressure of acetone-ethanol mixture and hydrogen bonding between acetone and ethanol.

Preparation and Characterization of Stabilized $ZrO_2$ by Wet Chemical Methods (습식화학 방법에 의한 안정화된 $ZrO_2$의 제조 및 특성에 대한 연구)

  • 전승범;변수일
    • Journal of the Korean Ceramic Society
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    • v.16 no.3
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    • pp.155-163
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    • 1979
  • This study was to explore the characteristics of 6 mole% CaO stabilized $ZrO_2$ prepared by wet chemical methods. The results of the experiments were as follows: 1. The powder calcined at 1000$^{\circ}$-110$0^{\circ}C$ was partly agglomerated. The morphology of agglomerate was spherical of 0.5-1$\mu{m}$ in size for Hot Petroleum Drying Method, chain-like of 1-2$\mu{m}$ for Freeze Drying Method, and irreqular of 2-3$\mu{m}$ for Coprecipitation Method. 2. Optimum calcining conditions for powder prepared by wet chemical methods were found: 110$0^{\circ}C$, 2h in air for Hot Petroleum Drying Method and Freeze Drying Method, and 100$0^{\circ}C$, 2h in air for Coprecipitation Method. 3. When specimen was calcined at 1000$^{\circ}$-110$0^{\circ}C$ in air for 2h and then sintered at 1$600^{\circ}C$ in air for 4h, the specimens prepared by wet chemical methods showed a high sintered density (94% of theoretical density) and a low open porosity (<0.8%); however, the sintered density of the specimen prepared by Oxide Wet Mixing Method was 90%. 4. The amount of cubic phase of sintered body prepared by wet chemical methods was observed to be higher than the one prepared by Oxide Wet Mixing Method. 5. It was found that Hot petroleum Drying Method, Freeze Drying Method and Coprecipitation Method were nearly the same in respect of the results of stabilization grade and sintered density of CaO-stabilized $ZrO_2$.

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Drying Characteristics and Content Change of Major Components of Shiitake Mushroom(Lentinus edodes) 2. Changes in Major Components of Shiitake Mushroom by Drying Temperature (표고버섯의 건조 특성 및 주요성분의 변화 2. 건조온도에 따른 표고버섯의 주요성분 변화)

  • Seo, Jae-Sin;Gang, Seong-Gu;Choe, Byeong-Min
    • Food Science and Preservation
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    • v.4 no.3
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    • pp.279-286
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    • 1997
  • The effect of drying temperature (30, 40, 50, 60$^{\circ}C$) on chemical components of Shiitake mushroom(Lentinus edodss) was investigate. When compared proximate composition on pileus and stipe of raw and dried materials, all of them were found to be higher in the stipe part than in the pileus part. The major components of organic acid were oxalic, citric, malic, malonic and pyroglutaric acid. The contents of free and total amino acids in pileus and stipe were 3458.4, 7640.2mg% for pilueus; 2298.0, 6171.5mg% for stipe on dry basis, respectively. On the other hand, there was no significant difference in the changes of crude ash and organic acids content of Shiitake mushroom among drying temperatures. But the amount of crude fats was increased and that of reducing sugars was decreased with increase of drying temperature. The contents of crude proteins of pileus part of dried materials were increased with increased drying temperature, but those of stile part were gradually decreased. The contents of free amino acids decreased with increase in drying temperature, but those of total amino acids were gradually increased.

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Modeling and Simulation of Drying Cylinders in Paper Processes (제지공정 건조 실린더의 모델링 및 모사)

  • Lee, Eun Ho;Kwak, Ki-Young;Yeo, Yeong-Koo
    • Korean Chemical Engineering Research
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    • v.45 no.1
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    • pp.17-24
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    • 2007
  • The purpose of the present study is to identify the drying cylinder model in paper plants and to analyze characteristics of process responses for changes in input variables. The model developed in this work is based on actual plant operation data where the steam pressure applied to the cylinder behaves as the major variable. It is found that heat transfer coefficients from the condensate to the canvas could be represented as empirical relations based on heat conductivities and operation data. The effectiveness of the cylinder model is demonstrated by the measured moisture contents and web temperature. Stability of the drying process is analyzed based on the transfer functions derived from the cylinder model.

Changes of Phenolic Compounds Affected by Different Drying Method in Leaves and Stems of Peony (Paeonia lactiflora Pall.) (작약 잎과 줄기의 건조 방법에 따른 Phenol 화합물의 변화)

  • Kim, Se-Jong;Park, Jun-Hong;Choi, Seong-Yong;Kim, Kil-Ung
    • KOREAN JOURNAL OF CROP SCIENCE
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    • v.51 no.spc1
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    • pp.251-254
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    • 2006
  • This study was conducted to identify changes of chemical components affected by different drying method and temperature conditions in leaves and stems of peony plant. Drying methods were the dried air heated $(50^{\circ}C)$, far-red ray $(50^{\circ}C)$, room temperature and oven dry $(50^{\circ}C)$. Drying temperature were 40, 50, 60, 70 and $80^{\circ}C$ on far-red ray dryer. Among the drying methods, the contents of components were the highest in far-red drying and normal temperature drying as compared with air heated drying and oven drying. Among the drying temperature conditions, the contents of components were the highest in drying temperature at $40^{\circ}C$ and decreased in high temperature of $70^{\circ}C\;and\;80^{\circ}C$.

Drying Characteristics of Succinic acid using the Microwave (마이크로파를 이용한 호박산 건조 특성)

  • Kim, Ji Sun;Ryu, Young Bok;Kim, Myung Hwan;Hong, Seong-Soo;Lee, Man Sig
    • Journal of the Korea Academia-Industrial cooperation Society
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    • v.14 no.11
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    • pp.6023-6028
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    • 2013
  • Recently, biodegradable polymers are gaining more and more attention due to international environmental issues. Succinic acid is synthesised by chemical process of hydrogenation. Succinic acid synthesized has certain amount water content. To remove the water contained in succinic acid is used generally by hot air drying process. But recently, microwave drying process having the advantage of shortening the drying time and uniform drying of product are gaining more attention. In this study, hot air drying and microwave drying efficiency were compared at drying process. In addition, we confirmed commercial applicability in microwave drying process of succinic acid. Microwave drying process has higher efficiency than 70% compared with hot air drying process at thickness of 1cm. Economic efficiency were compared through examination of power consumption for complete drying of succinic acid at microwave and hot air dyring.

Effects of Drying Conditions on the Quality of White Ginseng (백삼건조 조건이 품질에 미치는 영향)

  • 도재호;김상달
    • Journal of Ginseng Research
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    • v.9 no.2
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    • pp.248-255
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    • 1985
  • In order to investigate the optimal drying condition of white ginseng by using bulk air drier(130 x 62 x 65cm), drying curves, diffusion coefficient at various drying temperature, the energy of activation, variation of color intensity and chemical components during drying of white ginseng were studied. Fick's second low of diffusion for diffusion out of spheres was successfully applied to describe the drying of white ginseng. It was found that the diffusion coefficient of water was 2.2x107, 9.0x107 cm2/sec at drying temperature 4$0^{\circ}C$, 55$^{\circ}C$, respectively. An Arrhenius type temperature dependency of moisture diffusivity was found, the energy of activation being 18.8 Kcal/g mol. Color intensity of white ginseng dried at various drying temperature was increased with an increase in drying temperature. The contents of crude protein, reducing sugar and crude saponin during drying of white ginseng were gradually decreased as increasing of drying time. And with the sensory evaluation by multiple comparison difference analysis, the optimal drying temperature of white ginseng was between 45$^{\circ}C$ and 5$0^{\circ}C$.

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